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    • 1. 发明授权
    • Headspace sampling and monitoring systems and methods
    • 顶空采样和监测系统和方法
    • US06436710B1
    • 2002-08-20
    • US09556287
    • 2000-04-24
    • Timothy Mark SivavecSunita Singh BaghelDon Royall HoustonAngelo Anthony Bracco
    • Timothy Mark SivavecSunita Singh BaghelDon Royall HoustonAngelo Anthony Bracco
    • G01N118
    • G01N33/0047G01N1/2226G01N33/18G01N2001/2229Y10T436/25375Y10T436/25875
    • A headspace sampling system monitors materials in wastewater. The headspace sampling system comprises a sample receptacle that can contain a wastewater sample; a sparger chamber vapor column; a sample receptacle cover assembly that connects the sparger chamber vapor column to the sample receptacle; a sparger tube; at least one sensing device; and at least one analytic device. The sparger tube and the sample receptacle define a headspace. The sparger chamber vapor column is in communication with the sample receptacle and is closed by a sparger chamber vapor column cover at a second end that is opposed to the sample receptacle. The sparger tube extends into the sample receptacle and the wastewater sample in the sample receptacle. The sparger tube is connected to a source of inert gas at a first end opposed to the sample receptacle and comprises a dispersion device at an end opposed to the first end. The sensing device is disposed in the headspace sampling system in the headspace. The analytic device in communication with the least one sensing device. Inert gas can flow through the sparger tube into the wastewater sample to separate materials from the wastewater, the sparged materials entering the headspace of the headspace sampling system. The sparged materials are sensed by the sensing device thus providing material signal characteristics, which can be analyzed by the analytic device to determine characteristics of the material from the material signal characteristics and provide information about the characteristics of the material.
    • 顶空采样系统监测废水中的物质。 顶空采样系统包括可容纳废水样品的样品容器; 分配器室蒸气柱; 将所述分布器室蒸气柱连接到所述样品容器的样品容器盖组件; 分布管; 至少一个感测装置; 和至少一个分析设备。 分布器管和样品容器定义了顶部空间。 分布器室蒸气柱与样品容器连通,并在与样品容器相对的第二端处由分布器室蒸气柱盖封闭。 分布器管延伸到样品容器和样品容器中的废水样品。 喷射管在与样品容器相对的第一端处连接到惰性气体源,并且在与第一端相对的端部包括分散装置。 感测装置设置在顶部空间采样系统中。 与至少一个感测装置通信的分析装置。 惰性气体可以通过分布管流入废水样品,从废水中分离出材料,喷射材料进入顶空采样系统的顶部空间。 所述感光装置感测到所述喷射材料,从而提供材料信号特性,所述材料信号特性可由所述分析装置分析,以根据所述材料信号特性确定所述材料的特性并提供关于所述材料的特性的信息。
    • 7. 发明授权
    • On-line sparging sampling and monitoring systems and methods
    • 在线喷射取样和监测系统和方法
    • US06485688B1
    • 2002-11-26
    • US09556288
    • 2000-04-24
    • Timothy Mark SivavecSunita Singh BaghelAngelo Anthony BraccoDon Royall Houston
    • Timothy Mark SivavecSunita Singh BaghelAngelo Anthony BraccoDon Royall Houston
    • G01N700
    • G01N33/18G01N1/2226G01N33/0047G01N2001/2229
    • An on-line sparging sampling system and method sparges polar and non-polar volatile organic compounds from aqueous discharge. The system comprises a network of tubular members that are interconnected to each other to define a fluid passage, in which the network of tubular members comprises an inlet for influent aqueous discharge into the network of tubular members and an outlet for discharge of aqueous discharge from the on-line sparging sampling and monitoring system; a sparger disposed in the network of tubular members, in which the sparger is disposed between the inlet and the outlet of the aqueous discharge so that aqueous discharge flows by the sparger, the sparger providing inert non-reactive gas to the on-line sparging sampling and monitoring system; and at least one analytic device connected to the on-line sparging sampling and monitoring system for analyzing volatile organic compounds in the aqueous discharge. The aqueous discharge forms an aqueous discharge portion and a headspace during flow through the network of tubular members. The sparger provides the inert non-reactive gas to flow through the aqueous discharge portion. The inert non-reactive gas partitions volatile organic compounds from the aqueous discharge portion to the headspace. Thus, polar and non-polar volatile organic compounds can be analyzed by the at least one analytic device.
    • 在线喷射取样系统和方法从水性排放物喷射极性和非极性挥发性有机化合物。 该系统包括彼此互连以限定流体通道的管状构件的网络,其中管状构件的网络包括用于从管状构件的网络中进水的排水入口和用于从 在线喷射采样和监测系统; 分布器布置在管状构件的网络中,其中分布器布置在水性排出口的入口和出口之间,使得水分离器由分布器流动,分布器向在线喷射取样提供惰性非反应性气体 监控系统; 以及连接到在线喷射取样和监测系统上的至少一个分析装置,用于分析含水排放物中的挥发性有机化合物。 在通过管状构件的网络的流动期间,水性排出物形成水性排出部分和顶部空间。 喷射器提供惰性非反应性气体流过含水排放部分。 惰性非反应性气体将挥发性有机化合物从含水排放部分分隔成顶部空间。 因此,极性和非极性挥发性有机化合物可以通过至少一种分析装置来分析。