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1. 发明授权

US09414547B2 Methods to grow, deliver, and plant young trees in a removable tubular container 有权
标题翻译：在可移除的管状容器中生长，输送和种植幼树的方法
公开(公告)号：US09414547B2
公开(公告)日：2016-08-16
申请号：US13754847
申请日：2013-01-30
申请人： Thomas Link Guggenheim , Roy Ray Odle
发明人： Thomas Link Guggenheim , Roy Ray Odle
IPC分类号： A01G9/02 , A01G1/00 , A01G13/00 , A01G9/10
CPC分类号： A01G1/001 , A01G9/026 , A01G9/0299 , A01G13/0243 , A01G22/00
摘要： Methods to grow, provide and plant a young tree using a novel removable tubular container are disclosed. The container promotes the growth of a well formed protected root structure that minimizes transplant shock at the time the young tree is moved and permanently planted. The removable container and methods described provide for a fast growing inexpensive tree that is easily planted by a single person.
摘要翻译：公开了使用新型可移除管状容器生长，提供和种植幼树的方法。该容器促进形成良好形成的保护根结构的生长，使幼树移动和永久种植时的移植冲击最小化。所描述的可移动容器和方法提供了一种快速增长的便宜的树，其容易由单个人种植。

2. 发明授权

US09040651B2 Poly(aryl ether sulfone) composition, and method of making 有权
标题翻译：聚（芳基醚砜）组合物及其制备方法
公开(公告)号：US09040651B2
公开(公告)日：2015-05-26
申请号：US13285043
申请日：2011-10-31
申请人： Eric Lee Lutz , William Hoy Heath , Roy Ray Odle , Thomas Link Guggenheim , Juan Justino Rodriguez Ordonez , Jose Roman Galdamez Pena
发明人： Eric Lee Lutz , William Hoy Heath , Roy Ray Odle , Thomas Link Guggenheim , Juan Justino Rodriguez Ordonez , Jose Roman Galdamez Pena
IPC分类号： C08G75/00 , C08G75/23 , C08G65/40 , C08G65/00
CPC分类号： C08G75/23 , C08G65/00 , C08G65/40 , C08G65/4056
摘要： A poly(aryl ether sulfone) comprises units of formula (I): wherein Ar1 is a divalent C6-C15 aromatic group, Ar2 is a divalent C6-C15 aromatic group, Ar3 is a divalent C6-C15 aromatic group, and n is greater than 1; and a terminal group of formula (II) derived from a monofunctional phenoxide wherein is X is a hydrogen atom or an organic substituent having from 1 to 20 carbon atoms; wherein the poly(aryl ether sulfone) has a hydroxyl group content greater than 0 and less than 50 parts per million (ppm), based on the poly(aryl ether sulfone) weight, a glass transition temperature of 180 to 290° C., a weight average molecular weight of 20,000 to 100,000, a halogen content of greater than 0 and less than 3000 ppm based on the poly(aryl ether sulfone) weight. The poly(aryl ether sulfone) is free of methoxy groups.
摘要翻译：聚（芳基醚砜）包括式（I）的单元：其中Ar1是二价C 6 -C 15芳族基团，Ar 2是二价C 6 -C 15芳族基团，Ar 3是二价C 6 -C 15芳族基团，n大于比1; 和衍生自单官能酚盐的式（II）的末端基团，其中X为氢原子或具有1至20个碳原子的有机取代基; 其中聚（芳基醚砜）的羟基含量大于0且小于50ppm（ppm），基于聚（芳基醚砜）重量，玻璃化转变温度为180-290℃，重均分子量为20,000至100,000，卤素含量大于0且小于3000ppm，基于聚（芳基醚砜）重量。聚（芳基醚砜）不含甲氧基。

3. 发明申请

US20140208645A1 Methods to Grow, Deliver, and Plant Young Trees in a Removable Tubular Container 审中-公开
标题翻译：在可移动管状容器中种植，输送和种植幼树的方法
公开(公告)号：US20140208645A1
公开(公告)日：2014-07-31
申请号：US13754847
申请日：2013-01-30
申请人： Thomas Link Guggenheim , Roy Ray Odle
发明人： Thomas Link Guggenheim , Roy Ray Odle
IPC分类号： A01G1/00 , A01G9/02
CPC分类号： A01G1/001 , A01G9/026 , A01G9/0299 , A01G13/0243 , A01G22/00
摘要： Methods to grow, provide and plant a young tree using a novel removable tubular container are disclosed. The container promotes the growth of a well formed protected root structure that minimizes transplant shock at the time the young tree is moved and permanently planted. The removable container and methods described provide for a fast growing inexpensive tree that is easily planted by a single person.
摘要翻译：公开了使用新型可移除管状容器生长，提供和种植幼树的方法。该容器促进形成良好形成的保护根结构的生长，使幼树移动和永久种植时的移植冲击最小化。所描述的可移动容器和方法提供了一种快速增长的便宜的树，其容易由单个人种植。

4. 发明授权

US07902407B2 Method for preparation of salts of hydroxy-substituted aromatic compounds 有权
标题翻译：羟基取代芳族化合物的盐的制备方法
公开(公告)号：US07902407B2
公开(公告)日：2011-03-08
申请号：US11095200
申请日：2005-03-30
申请人： James Manio Silva , Thomas Link Guggenheim , David Winfield Woodruff
发明人： James Manio Silva , Thomas Link Guggenheim , David Winfield Woodruff
IPC分类号： C07C39/12 , C07C39/16
CPC分类号： C07C37/66 , C07C39/235
摘要： A method for preparing a metal salt of a hydroxy-substituted aromatic compound is described. The method comprises contacting in an aqueous medium at least one hydroxy-substituted aromatic compound with a base comprising a metal cation to provide a mixture comprising water and a metal salt of said hydroxy-substituted aromatic compound. The aqueous metal salt is then contacted with a substantially water-immiscible solvent at a temperature greater than the boiling point of water at the prevailing pressure to provide a slurry comprising the metal salt of the hydroxy-substituted aromatic compound and a vapor stream comprising the water-immiscible solvent and water. The components of the vapor stream are separated using a vapor handling system comprising a partial reflux condenser to provide a water-rich component and a water immiscible solvent-rich component.
摘要翻译：描述了制备羟基取代的芳族化合物的金属盐的方法。该方法包括在含水介质中使至少一种羟基取代的芳族化合物与包含金属阳离子的碱接触以提供包含水和所述羟基取代的芳族化合物的金属盐的混合物。然后在主要压力下，在大于沸点的温度下，将水性金属盐与基本上与水不混溶的溶剂接触，以提供包含羟基取代的芳族化合物的金属盐和包含水的蒸汽流的浆料可混溶的溶剂和水。使用包含部分回流冷凝器的蒸汽处理系统分离蒸气流的组分以提供富含水的组分和与水不混溶的富含溶剂的组分。

5. 发明授权

US07842188B2 Method for removal of guanidine compound from aqueous media 失效
标题翻译：从水性介质中除去胍化合物的方法
公开(公告)号：US07842188B2
公开(公告)日：2010-11-30
申请号：US11684882
申请日：2007-03-12
申请人： David Bruce Hall , Thomas Link Guggenheim , James Manio Silva , Farid Fouad Khouri , Matthew Hal Littlejohn , Balakrishnan Ganesan , Ashok Shankrappa Shyadligeri , Pradeep Jeevaji Nadkarni
发明人： David Bruce Hall , Thomas Link Guggenheim , James Manio Silva , Farid Fouad Khouri , Matthew Hal Littlejohn , Balakrishnan Ganesan , Ashok Shankrappa Shyadligeri , Pradeep Jeevaji Nadkarni
IPC分类号： B01D61/00 , B01D63/00
CPC分类号： C02F9/00 , B01D61/027 , C02F1/281 , C02F1/283 , C02F1/44 , C02F2101/38 , C07C277/06 , C07C279/04
摘要： Disclosed is a method for removing a neutral or an ionic guanidine compound from aqueous media optionally comprising an alkali metal halide, wherein the method is selected from the group consisting of (a) adsorption onto a carbonaceous adsorbent, (b) adsorption onto a clay adsorbent, (c) filtration through a nanofiltration membrane, and (d) removal of water and calcination.
摘要翻译：公开了一种从任选地包含碱金属卤化物的水性介质中除去中性或离子胍化合物的方法，其中所述方法选自（a）吸附到含碳吸附剂上，（b）吸附到粘土吸附剂上，（c）通过纳滤膜过滤，和（d）去除水和煅烧。

6. 发明授权

US06881815B2 Method for the preparation poly(etherimide)s 失效
标题翻译：制备聚（醚酰亚胺）的方法
公开(公告)号：US06881815B2
公开(公告)日：2005-04-19
申请号：US10065197
申请日：2002-09-25
申请人： Roy Ray Odle , Thomas Link Guggenheim
发明人： Roy Ray Odle , Thomas Link Guggenheim
IPC分类号： C07B61/00 , C07D209/48 , C07D401/04 , C07D401/14 , C08G73/10 , C08G69/26 , C08G69/28
CPC分类号： C07D209/48 , C07D401/04 , C07D401/14
摘要： A method for the synthesis of poly(etherimide)s comprises the reaction of 4-halotetrahydrophthalic anhydride with an activating primary amine to yield an activated 4-halotetrahydrophthalimide. Activated 4-halotetrahydrophthalimide may then be aromatized and treated with the disodium salt of a bis(phenol) to yield an activated bisimide. The activated bisimide may then be directly treated with a diamine to yield poly(etherimide)s.
摘要翻译：用于合成聚（醚酰亚胺）的方法包括4-卤代四氢邻苯二甲酸酐与活化伯胺的反应，得到活化的4-卤代四氢邻苯二甲酰亚胺。然后将活化的4-卤代四氢邻苯二甲酰亚胺芳构化并用双（苯酚）的二钠盐处理，得到活化的双酰亚胺。然后可以用二胺直接处理活化的双酰亚胺以产生聚（醚酰亚胺）。

7. 发明授权

US06710187B2 Process to isolate dianhydrides 有权
标题翻译：分离二酸酐的方法
公开(公告)号：US06710187B2
公开(公告)日：2004-03-23
申请号：US10063795
申请日：2002-05-14
申请人： Thomas Link Guggenheim , David Anthony Mongilio
发明人： Thomas Link Guggenheim , David Anthony Mongilio
IPC分类号： C07D30789
CPC分类号： C07C51/573 , Y10S159/901 , C07C65/24
摘要： A process to isolate dianhydride from an exchange reaction comprises extracting a bisimide/anhydride exchange reaction aqueous phase with an organic solution comprising an exchange catalyst at a first temperature and pressure to form an extracted aqueous phase comprising water, exchange catalyst and a dianhydride precursor; removing water from the extracted aqueous phase at a second temperature and pressure to form a molten phase, wherein the second pressure is less than the first pressure; removing water and exchange catalyst from the molten phase at a third temperature and pressure to form an isolation mixture; and converting the dianhydride precursor in the isolation mixture to dianhydride at a fourth temperature and pressure, wherein the fourth temperature is greater than the second and third temperatures and the fourth pressure is less than the second and third pressures.
摘要翻译：从交换反应中分离二酐的方法包括在第一温度和压力下用包含交换催化剂的有机溶液萃取双酰亚胺/酸酐交换反应水相以形成包含水，交换催化剂和二酐前体的萃取水相; 在第二温度和压力下从提取的水相中除去水以形成熔融相，其中第二压力小于第一压力; 在第三温度和压力下除去水并从熔融相中交换催化剂以形成分离混合物; 以及在第四温度和压力下将分离混合物中的二酐前体转化为二酐，其中第四温度大于第二和第三温度，第四压力小于第二和第三压力。

8. 发明授权

US06528663B1 Methods for the preparation of 4-chlorophthalic anhydride 失效
标题翻译：制备4-氯邻苯二甲酸酐的方法
公开(公告)号：US06528663B1
公开(公告)日：2003-03-04
申请号：US09683256
申请日：2001-12-05
申请人： Roy Ray Odle , Thomas Link Guggenheim
发明人： Roy Ray Odle , Thomas Link Guggenheim
IPC分类号： C07D30789
CPC分类号： C07C51/00 , C07D209/48 , C07C63/70
摘要： A method for the synthesis of substituted phthalic anhydrides (IV) wherein R′ is a halogen, aromatic or aliphatic group comprising 1-18 carbons, hydrogen or nitro group is the transimidation between a substituted N-alkyl phthalimide (V) wherein R is an alkyl having from 1 to 18 carbons, and a substituted tetrahydrophthalic anhydride (VI): The by-product of this reaction, a substituted N-alkyl tetrahydrophthalimide (VII), may be converted by aromatization to the substituted N-alkyl phthalimide (V).
摘要翻译：用于合成取代的邻苯二甲酸酐（Ⅳ）的方法，其中R'是卤素，包含1-18个碳原子的芳族或脂族基团，氢或硝基是取代的N-烷基邻苯二甲酰亚胺（Ⅴ）之间的转移，其中R是具有1至18个碳原子的烷基和取代的四氢邻苯二甲酸酐（VI）：该反应的副产物 - 取代的N-烷基四氢邻苯二甲酰亚胺（VII）可通过芳构化转化为取代的N-烷基邻苯二甲酰亚胺（V）。

9. 发明授权

US06251354B1 Process for recovering sodium nitrite 失效
标题翻译：回收亚硝酸钠的方法
公开(公告)号：US06251354B1
公开(公告)日：2001-06-26
申请号：US09285927
申请日：1999-04-02
申请人： Robert E. Greenwell , Thomas Link Guggenheim , Norman Enoch Johnson , Roy Ray Odle , Jimmy Lynn Webb
发明人： Robert E. Greenwell , Thomas Link Guggenheim , Norman Enoch Johnson , Roy Ray Odle , Jimmy Lynn Webb
IPC分类号： C01B2120
CPC分类号： C01B21/50
摘要： The present invention provides a process for recovering a metal nitrite, e.g., sodium nitrite, from a reaction mixture formed from an aromatic displacement reaction such as the synthesis of an aromatic bis(ether phthalimide) in an organic non-polar solvent. The process comprises forming a reaction mixture from the synthesis of an aromatic bis(ether phthalimide) comprising a recoverable amount of metal nitrite; treating the reaction mixture with an amount of water effective to produce an aqueous solution phase of metal nitrite and an organic non-polar phase; and separating the aqueous solution phase of metal nitrite from the organic non-polar phase.
摘要翻译：本发明提供了从由有机非极性溶剂中的芳族双（醚邻苯二甲酰亚胺）的合成等芳香置换反应形成的反应混合物中回收亚硝酸金属亚硝酸盐的方法。该方法包括从合成包含可回收量的金属亚硝酸盐的芳族双（醚邻苯二甲酰亚胺）形成反应混合物; 用有效量的水处理反应混合物以产生金属亚硝酸盐和有机非极性相的水溶液相; 并从有机非极性相分离金属亚硝酸盐的水溶液相。

10. 发明申请

US20150337461A1 Crystallizable Polyetherimides, Method of Manufacture, and Articles Derived Therefrom 审中-公开
标题翻译：可结晶聚醚酰亚胺，制造方法及其衍生物
公开(公告)号：US20150337461A1
公开(公告)日：2015-11-26
申请号：US14643859
申请日：2015-03-10
申请人： Amitabh Bansal , Thomas Link Guggenheim , Erik C Hagberg , Ganesh Kailasam , Roy Ray Odle , Prameela Susarla , Karthik Venkataraman , Xiaolan Wei
发明人： Amitabh Bansal , Thomas Link Guggenheim , Erik C Hagberg , Ganesh Kailasam , Roy Ray Odle , Prameela Susarla , Karthik Venkataraman , Xiaolan Wei
IPC分类号： D01F6/74 , D01D10/02 , D04H3/005 , D01D5/12
CPC分类号： C08G73/1053 , C08L79/08 , D01D5/12 , D01D10/02 , D01F6/74 , D04H3/005 , D10B2331/06 , Y10T442/30 , Y10T442/3984 , Y10T442/60 , Y10T442/696
摘要： A composition is described, which comprises a crystallizable polyetherimide derived from the polymerization of: (a) a dianhydride component, comprising more than 96.8 mole % of 4,4′-bisphenol A dianhydride or a chemical equivalent thereof; and (b) a diamine component comprising a diamine or a chemical equivalent thereof, wherein the crystallizable polyetherimide has a Tm ranging from 250° C. to 400° C. and the difference between the Tm and Tg of the composition is more than 50° C. Further described are articles, such as fibers, made from the composition, methods for making the composition, methods for making the articles, and methods for using the articles.
摘要翻译：描述了一种组合物，其包含衍生自以下聚合的可结晶聚醚酰亚胺：（a）二酐组分，其包含大于96.8摩尔％的4,4'-双酚A二酐或其化学等价物; 和（b）包含二胺或其化学等价物的二胺组分，其中可结晶聚醚酰亚胺的Tm为250℃至400℃，组合物的Tm和Tg之间的差值大于50℃ 进一步描述了由组合物制成的制品，例如纤维，用于制备组合物的方法，制造制品的方法以及使用制品的方法。

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