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    • 6. 发明申请
    • PROCESS FOR PRODUCING POLYSILICON
    • 多晶硅生产工艺
    • US20130011558A1
    • 2013-01-10
    • US13533441
    • 2012-06-26
    • Walter HAECKLBarbara MUELLERRobert RING
    • Walter HAECKLBarbara MUELLERRobert RING
    • C23C16/24
    • C23C16/24C01B33/03C01B33/035C01B33/10778
    • A process for producing polysilicon, includes a) depositing polycrystalline silicon on filaments using reaction gas containing silicon-containing component (SCC) containing trichlorosilane, and hydrogen, wherein molar saturation of SCC based on hydrogen is at least 25%; b) feeding offgas from the deposition into a cooling apparatus, i) wherein condensed offgas components containing SiCl4 are conducted to an apparatus which enables distillative purification of the condensate, and ii) non-condensing components are conducted to an adsorption or desorption unit; c) obtaining a first stream of non-condensing components purified by adsorption and containing hydrogen; and d) obtaining, during adsorption unit regeneration, a second stream of non-condensing components, containing SiCl4 which is then preferably supplied to a converter for conversion of SiCl4 to trichlorosilane. A process for depositing polysilicon on filaments with a reaction gas includes a SCC and hydrogen, wherein molar saturation of SCC based on hydrogen is at least 25%.
    • 一种生产多晶硅的方法,包括:a)使用含有含三氯硅烷的含硅组分(SCC)和氢气的氢气沉积多晶硅,其中基于氢的SCC的摩尔饱和度至少为25%; b)将沉淀物中的废气进料到冷却装置中,i)其中含有SiCl 4的浓缩废气组分被导入能够对冷凝物进行蒸馏净化的装置,以及ii)将非冷凝组分导入吸附或解吸装置; c)获得通过吸附纯化并含有氢的第一个非冷凝组分物流; 和d)在吸附单元再生期间获得含有SiCl 4的第二非冷凝组分流,然后优选将其供应到用于将SiCl 4转化为三氯硅烷的转化器。 用反应气体在长丝上沉积多晶硅的方法包括SCC和氢,其中基于氢的SCC的摩尔饱和度为至少25%。