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1. 发明授权

US08431202B2 Aluminum/alkaline or alkali/titanium containing polyesters having improved reheat, color and clarity 有权
标题翻译：具有改善的再热，颜色和透明度的铝/碱性或碱/含钛聚酯
公开(公告)号：US08431202B2
公开(公告)日：2013-04-30
申请号：US11229238
申请日：2005-09-16
申请人： Donna Rice Quillen , Rodney Scott Armentrout , Mary Therese Jernigan , Steven Lee Stafford , Zhiyong Xia
发明人： Donna Rice Quillen , Rodney Scott Armentrout , Mary Therese Jernigan , Steven Lee Stafford , Zhiyong Xia
IPC分类号： B29D22/00 , B29D23/00 , B32B1/08
CPC分类号： C08G63/83 , B29C47/0004 , B29C47/0016 , B29C47/0021 , C08G63/183 , C08G63/84 , Y10T428/1352 , Y10T428/1355 , Y10T428/139 , Y10T428/1397
摘要： A polyester composition containing: a) aluminum atoms; and b) alkaline earth atoms or alkali metal atoms or alkali compound residues such as lithium atoms; and c) particles comprising titanium, zirconium, vanadium, niobium, hafnium, tantalum, chromium, tungsten, molybdenum, iron, or nickel atoms or combinations thereof, where the particles improve the reheat rate of the polyester composition. The polyester polymer compositions may also contain phosphorus catalyst deactivators/stabilizers. The polyester compositions and the articles made from the compositions such as bottle preforms and stretch blow molded bottles have improved reheat rate while maintaining low haze, high L*, a b* below 3, and have low levels of acetaldehyde. In the process for making the polyester polymer, the polymer melt is polycondensed in the presence of a) and b), with the particles c) added in a melt phase process or added to the polymer in an injection molding machine or extruder. The polyester polymer composition can be made to high IV from the melt phase while avoiding solid state polymerization.
摘要翻译：一种聚酯组合物，其含有：a）铝原子; 和b）碱土金属原子或碱金属原子或碱金属化合物残基如锂原子; 和c）包含钛，锆，钒，铌，铪，钽，铬，钨，钼，铁或镍原子或其组合的颗粒，其中颗粒改善了聚酯组合物的再热速率。聚酯聚合物组合物还可以含有磷催化剂失活剂/稳定剂。聚酯组合物和由诸如瓶子预成型件和拉伸吹塑成型瓶的组合物制成的制品具有改善的再加热速率，同时保持低雾度，高L *，低于3的b *，并且具有低水平的乙醛。在制备聚酯聚合物的方法中，聚合物熔体在a）和b）存在下缩聚，颗粒c）在熔融相中加入或在注塑机或挤出机中加入到聚合物中。聚酯聚合物组合物可以从熔融相制成高IV，同时避免固态聚合。

2. 发明授权

US08791187B2 Aluminum/alkyline or alkali/titanium containing polyesters having improved reheat, color and clarity 有权
标题翻译：铝/烷基或含碱/钛的聚酯具有改善的再热，颜色和透明度
公开(公告)号：US08791187B2
公开(公告)日：2014-07-29
申请号：US13149248
申请日：2011-05-31
申请人： Donna Rice Quillen , Rodney Scott Armentrout , Mary Therese Jernigan , Steven Lee Stafford , Zhiyong Xia
发明人： Donna Rice Quillen , Rodney Scott Armentrout , Mary Therese Jernigan , Steven Lee Stafford , Zhiyong Xia
IPC分类号： B32B27/18
CPC分类号： C08G63/83 , B29C47/0004 , B29C47/0016 , B29C47/0021 , C08G63/183 , C08G63/84 , Y10T428/1352 , Y10T428/1355 , Y10T428/139 , Y10T428/1397
摘要： A polyester composition containing: a) aluminum atoms; and b) alkaline earth atoms or alkali metal atoms or alkali compound residues such as lithium atoms; and c) particles comprising titanium, zirconium, vanadium, niobium, hafnium, tantalum, chromium, tungsten, molybdenum, iron, or nickel atoms or combinations thereof, where the particles improve the reheat rate of the polyester composition. The polyester polymer compositions may also contain phosphorus catalyst deactivators/stabilizers. The polyester compositions and the articles made from the compositions such as bottle preforms and stretch blow molded bottles have improved reheat rate while maintaining low haze, high L*, a b* below 3, and have low levels of acetaldehyde. In the process for making the polyester polymer, the polymer melt is polycondensed in the presence of a) and b), with the particles c) added in a melt phase process or added to the polymer in an injection molding machine or extruder. The polyester polymer composition can be made to high IV from the melt phase while avoiding solid state polymerization.
摘要翻译：一种聚酯组合物，其含有：a）铝原子; 和b）碱土金属原子或碱金属原子或碱金属化合物残基如锂原子; 和c）包含钛，锆，钒，铌，铪，钽，铬，钨，钼，铁或镍原子或其组合的颗粒，其中颗粒改善了聚酯组合物的再热速率。聚酯聚合物组合物还可以含有磷催化剂失活剂/稳定剂。聚酯组合物和由诸如瓶子预成型件和拉伸吹塑成型瓶的组合物制成的制品具有改善的再加热速率，同时保持低雾度，高L *，低于3的b *，并且具有低水平的乙醛。在制备聚酯聚合物的过程中，聚合物熔体在a）和b）存在下缩聚，颗粒c）以熔融相方式加入，或者在注射成型机或挤出机中加入到聚合物中。聚酯聚合物组合物可以从熔融相制成高IV，同时避免固态聚合。

3. 发明申请

US20110281049A1 ALUMINUM/ALKYLINE OR ALKALI/TITANIUM CONTAINING POLYESTERS HAVING IMPROVED REHEAT, COLOR AND CLARITY 有权
标题翻译：含有改进的REHEAT，COLOR和CLARITY的聚酯的ALUMINUM / ALKYLINE或ALKALI / TITANIUM
公开(公告)号：US20110281049A1
公开(公告)日：2011-11-17
申请号：US13149248
申请日：2011-05-31
申请人： Donna Rice Quillen , Rodney Scott Armentrout , Mary Therese Jernigan , Steven Lee Stafford , Zhiyong Xia
发明人： Donna Rice Quillen , Rodney Scott Armentrout , Mary Therese Jernigan , Steven Lee Stafford , Zhiyong Xia
IPC分类号： B32B27/18 , B32B27/36 , B32B1/02 , C08K3/28 , C08K5/521
CPC分类号： C08G63/83 , B29C47/0004 , B29C47/0016 , B29C47/0021 , C08G63/183 , C08G63/84 , Y10T428/1352 , Y10T428/1355 , Y10T428/139 , Y10T428/1397
摘要： A polyester composition containing: a) aluminum atoms; and b) alkaline earth atoms or alkali metal atoms or alkali compound residues such as lithium atoms; and c) particles comprising titanium, zirconium, vanadium, niobium, hafnium, tantalum, chromium, tungsten, molybdenum, iron, or nickel atoms or combinations thereof, where the particles improve the reheat rate of the polyester composition. The polyester polymer compositions may also contain phosphorus catalyst deactivators/stabilizers. The polyester compositions and the articles made from the compositions such as bottle preforms and stretch blow molded bottles have improved reheat rate while maintaining low haze, high L*, a b* below 3, and have low levels of acetaldehyde. In the process for making the polyester polymer, the polymer melt is polycondensed in the presence of a) and b), with the particles c) added in a melt phase process or added to the polymer in an injection molding machine or extruder. The polyester polymer composition can be made to high IV from the melt phase while avoiding solid state polymerization.
摘要翻译：一种聚酯组合物，其含有：a）铝原子; 和b）碱土金属原子或碱金属原子或碱金属化合物残基如锂原子; 和c）包含钛，锆，钒，铌，铪，钽，铬，钨，钼，铁或镍原子或其组合的颗粒，其中颗粒改善了聚酯组合物的再热速率。聚酯聚合物组合物还可以含有磷催化剂失活剂/稳定剂。聚酯组合物和由诸如瓶子预成型件和拉伸吹塑成型瓶的组合物制成的制品具有改善的再加热速率，同时保持低雾度，高L *，低于3的b *，并且具有低水平的乙醛。在制备聚酯聚合物的过程中，聚合物熔体在a）和b）存在下缩聚，颗粒c）以熔融相方式加入，或者在注射成型机或挤出机中加入到聚合物中。聚酯聚合物组合物可以从熔融相制成高IV，同时避免固态聚合。

4. 发明授权

US06777048B2 Polyester compositions containing silicon carbide 有权
标题翻译：含有碳化硅的聚酯组合物
公开(公告)号：US06777048B2
公开(公告)日：2004-08-17
申请号：US10323058
申请日：2002-12-18
申请人： Donna Rice Quillen , Earl Edmondson Howell, Jr. , Steven Lee Stafford
发明人： Donna Rice Quillen , Earl Edmondson Howell, Jr. , Steven Lee Stafford
IPC分类号： B29D2200
CPC分类号： C08J3/226 , C08J2367/02 , C08J2467/00 , C08K3/14 , Y10T428/1314 , Y10T428/1352 , Y10T428/2991 , C08L67/02
摘要： A polyester pellet composition, a preform, and a bottle, each comprising a polyester polymer and silicon carbide. A polyester, and in particular a polyethylene terephthalate polyester, bottle containing silicon carbide has a low coefficient of static friction and a low bottle sidewall haze.
摘要翻译：聚酯颗粒组合物，预成型体和瓶子，各自包含聚酯聚合物和碳化硅。聚酯，特别是聚对苯二甲酸乙二醇酯聚酯，含有碳化硅的瓶具有低的静摩擦系数和低的瓶侧壁雾度。

5. 发明授权

US07662880B2 Polyester polymer and copolymer compositions containing metallic nickel particles 有权
标题翻译：含有金属镍颗粒的聚酯聚合物和共聚物组合物
公开(公告)号：US07662880B2
公开(公告)日：2010-02-16
申请号：US10996924
申请日：2004-11-24
申请人： Zhiyong Xia , Donna Rice Quillen
发明人： Zhiyong Xia , Donna Rice Quillen
IPC分类号： B65D81/24
CPC分类号： C08K3/08 , B29B2911/1402 , B29B2911/14026 , B29B2911/14033 , B29B2911/1404 , B29B2911/14106 , B29B2911/14133 , B29C49/0005 , B29C49/06 , B29C51/00 , B29K2105/005 , B29K2105/065 , B29K2705/00 , C08K2003/0862 , Y10S428/913 , Y10T428/1355 , Y10T428/1372 , Y10T428/256 , C08L67/02
摘要： Polyester compositions are disclosed that include polyester polymers or copolymers having incorporated therein metallic nickel particles that improve the reheat properties of the compositions. Processes for making such compositions are also disclosed. The nickel particles may be incorporated in the polyester by melt compounding, or may be added at any stage of the polymerization, such as during the melt-phase of the polymerization. A range of particle sizes may be used, as well as a range of particle size distributions. The polyester compositions are suitable for use in packaging made from processes in which a reheat step is desirable.
摘要翻译：公开了聚酯组合物，其包括其中掺入金属镍颗粒的聚酯聚合物或共聚物，其改善组合物的再加热性能。还公开了制备这种组合物的方法。镍颗粒可以通过熔融混合而引入聚酯中，或者可以在聚合的任何阶段，例如在聚合的熔融相期间加入。可以使用一定范围的粒度，以及一定范围的粒度分布。聚酯组合物适用于由需要再热步骤的方法制成的包装。

6. 发明申请

US20080058495A1 Polyester polymer and copolymer compositions containing titanium and yellow colorants 审中-公开
标题翻译：含有钛和黄色着色剂的聚酯聚合物和共聚物组合物
公开(公告)号：US20080058495A1
公开(公告)日：2008-03-06
申请号：US11594282
申请日：2006-11-08
申请人： Donna Rice Quillen , Robert Joseph Maleski , Max Allen Weaver , James Christopher Scanlan , Emily Fraser , Colin Milton , Wim Hoenderdaal
发明人： Donna Rice Quillen , Robert Joseph Maleski , Max Allen Weaver , James Christopher Scanlan , Emily Fraser , Colin Milton , Wim Hoenderdaal
IPC分类号： C08G63/02
CPC分类号： C08K5/0041 , C08L67/02
摘要： There is provided a process for increasing the yellowness of polyester polymer particles, preforms, bottles, and concentrates, containing a polyester polymer such as polyethylene terephthalate and copolymers by adding a yellow colorant and reheat agent particles comprising titanium, alloys of titanium, titanium nitride, titanium boride, titanium carbide, or combinations thereof to a melt phase polymerization process for making the polyester polymer to adding any one of the colorant or particles to a polyester polymer.
摘要翻译：提供了通过添加黄色着色剂和包含钛的再热剂颗粒，钛，氮化钛的合金，增加聚酯聚合物颗粒，预成型体，瓶子和浓缩物的黄色度的方法，其包含聚对苯二甲酸乙二醇酯等聚酯聚合物和共聚物，硼化钛，碳化钛或其组合，用于制备聚酯聚合物以将任何一种着色剂或颗粒添加到聚酯聚合物中的熔融相聚合方法。

7. 发明申请

US20080027208A1 Non-precipitating alkali/alkaline earth metal and aluminum solutions made with polyhydroxyl ether solvents 有权
标题翻译：用多羟基醚溶剂制成的非沉淀碱/碱土金属和铝溶液
公开(公告)号：US20080027208A1
公开(公告)日：2008-01-31
申请号：US11495870
申请日：2006-07-28
申请人： Donna Rice Quillen , Barry Glen Pearcy , Michael Duane Cliffton , Aaron Nathaniel Edens
发明人： Donna Rice Quillen , Barry Glen Pearcy , Michael Duane Cliffton , Aaron Nathaniel Edens
IPC分类号： C08G63/00
CPC分类号： C08G63/84 , C08G63/83 , Y10T428/13 , Y10T428/1352
摘要： A stable catalyst solution suitable for catalyzing the polycondensation of reactants to make polyester polymers comprising: (i) M, wherein M is represented by an alkaline earth metal or alkali metal and (ii) aluminum metal and (iii) a polyhydroxyl ether solvent, wherein the molar ratio of M:Al ranges from 0.2:1 to 4:1 or less. The catalyst solution is desirably a solution which does not precipitate upon standing over a period of at least one week at room temperature (25° C.-40° C.), even at molar ratios of M:Al approaching 1:1. There is also provided a method for the manufacture of the solution, its feed to and use in the manufacture of a polyester polymer, and polyester polymers obtained by combining certain ingredients or containing the residues of these ingredients in the composition.
摘要翻译：一种稳定的催化剂溶液，其适用于催化反应物的缩聚以制备聚酯聚合物，其包含：（i）M，其中M由碱土金属或碱金属代表，和（ii）铝金属和（iii）多羟基醚溶剂，其中 M：Al的摩尔比范围为0.2:1至4:1或更低。催化剂溶液理想地是即使在接近1：1的M:Al的摩尔比下，在室温（25℃-40℃）下在至少一周的时间内静置时也不沉淀的溶液。还提供了一种用于制造溶液，其用于制造聚酯聚合物的原料和通过组合某些成分或将组合物中含有这些成分的残余物而获得的聚酯聚合物的方法。

8. 发明授权

US06458915B1 Process for producing poly(1,4-cyclohexylenedimethylene 1,4-cyclohexanedicarboxylate) and the reactor grade polyester therefrom 有权
标题翻译：聚（1,4-环己烯二亚甲基1,4-环己烷二羧酸酯）和反应器级聚酯的方法
公开(公告)号：US06458915B1
公开(公告)日：2002-10-01
申请号：US09764931
申请日：2001-01-18
申请人： Donna Rice Quillen
发明人： Donna Rice Quillen
IPC分类号： C08G6400
CPC分类号： C08G63/82 , C08G63/199 , C08G63/78
摘要： In a process for producing a reactor grade polyester, a poly(1,4-cyclohexylenedimethylene 1,4-cyclohexanedicarboxylate) has a reduced amount of isomerization of the trans-isomer to the cis-isomer of 1,4-dimethylcyclohexanedicarboxylate and an increased polymerization rate by the addition of a phosphorus-containing compound to the reaction process. In step (a) of the process, a diacid comprising at least 80 mole percent 1,4-cyclohexanedicarboxylic acid or an ester derivative of the diacid comprising at least 80 mole percent 1,4-dimethylcyclohexanedicarboxylate is reacted with a glycol comprising at least 80 mole percent 1,4-cyclohexanedimethanol at a temperature sufficient to effect esterification for the diacid or transesterification for the ester derivative. In step (b), the product of step (a) is subjected to temperatures and pressures in the presence of a suitable catalyst to effect polycondensation. Phosphorus in an amount of 1 to 800 ppm is added in the form of a phosphorus-containing compound during the process.
摘要翻译：在制备反应器级聚酯的方法中，聚（1,4-环己烯二亚甲基1,4-环己烷二羧酸酯）具有减少的反式异构体向1,4-二甲基环己烷二羧酸酯的顺式异构体的量和增加的聚合通过向反应过程中加入含磷化合物的速率。在该方法的步骤（a）中，将包含至少80摩尔％1,4-环己烷二羧酸的二酸或包含至少80摩尔％1,4-二甲基环己烷二羧酸酯的二酸的酯衍生物与包含至少80 摩尔百分比的1,4-环己烷二甲醇在足以实现酯衍生物的二酸或酯交换的酯化反应的温度下进行。在步骤（b）中，步骤（a）的产物在合适的催化剂存在下进行温度和压力以进行缩聚反应。在该过程中以含磷化合物的形式加入1至800ppm的量的磷。

9. 发明授权

US07709595B2 Non-precipitating alkali/alkaline earth metal and aluminum solutions made with polyhydroxyl ether solvents 有权
标题翻译：用多羟基醚溶剂制成的非沉淀碱/碱土金属和铝溶液
公开(公告)号：US07709595B2
公开(公告)日：2010-05-04
申请号：US11495870
申请日：2006-07-28
申请人： Donna Rice Quillen , Barry Glen Pearcy , Michael Duane Cliffton , Aaron Nathaniel Edens
发明人： Donna Rice Quillen , Barry Glen Pearcy , Michael Duane Cliffton , Aaron Nathaniel Edens
IPC分类号： C08G63/00 , C08G64/02
CPC分类号： C08G63/84 , C08G63/83 , Y10T428/13 , Y10T428/1352
摘要： A stable catalyst solution suitable for catalyzing the polycondensation of reactants to make polyester polymers comprising: (i) M, wherein M is represented by an alkaline earth metal or alkali metal and (ii) aluminum metal and (iii) a polyhydroxyl ether solvent, wherein the molar ratio of M:Al ranges from 0.2:1 to 4:1 or less. The catalyst solution is desirably a solution which does not precipitate upon standing over a period of at least one week at room temperature (25° C.-40° C.), even at molar ratios of M:Al approaching 1:1. There is also provided a method for the manufacture of the solution, its feed to and use in the manufacture of a polyester polymer, and polyester polymers obtained by combining certain ingredients or containing the residues of these ingredients in the composition.
摘要翻译：一种稳定的催化剂溶液，其适用于催化反应物的缩聚以制备聚酯聚合物，其包含：（i）M，其中M由碱土金属或碱金属代表，和（ii）铝金属和（iii）多羟基醚溶剂，其中 M：Al的摩尔比范围为0.2:1至4:1或更低。催化剂溶液理想地是即使在接近1：1的M:Al的摩尔比下，在室温（25℃-40℃）下在至少一周的时间内静置时也不沉淀的溶液。还提供了一种用于制造溶液，其用于制造聚酯聚合物的原料和通过组合某些成分或将组合物中含有这些成分的残余物而获得的聚酯聚合物的方法。

10. 发明授权

US5856424A Process for making polyesters containing low concentrations of diethylene glycol 失效
标题翻译：制备含低浓度二甘醇的聚酯的方法
公开(公告)号：US5856424A
公开(公告)日：1999-01-05
申请号：US950210
申请日：1997-10-14
申请人： David Taylor Bowers , Ronnie Jay Jones , Michael Duane Cliffton , Joseph Franklin Knight , Donna Rice Quillen
发明人： David Taylor Bowers , Ronnie Jay Jones , Michael Duane Cliffton , Joseph Franklin Knight , Donna Rice Quillen
IPC分类号： C08G63/183 , C08G63/189 , C08G63/78 , C08G63/02
CPC分类号： C08G63/183 , C08G63/189 , C08G63/78
摘要： The present invention relates to a process for producing a high molecular weight polyester having less than about 0.5 weight % diethylene glycol comprising adding at least one carbonate compound to the ester exchange reaction product produced from reaction of a glycol component comprising ethylene glycol and an ester component comprising dimethylterephthalate, dimethylnaphthalenedicarboxylate and mixtures thereof wherein said reaction product is formed without a Ti catalyst.
摘要翻译：本发明涉及一种生产具有小于约0.5重量％二甘醇的高分子量聚酯的方法，其包括向由乙二醇和酯组分的二醇组分的反应产生的酯交换反应产物中加入至少一种碳酸酯化合物包括对苯二甲酸二甲酯，萘二羧酸二甲酯及其混合物，其中所述反应产物不用Ti催化剂形成。

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