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1. 发明申请

US20180312629A1 NOVEL BRANCHED SULFUR-CONTAINING POLYMERS 审中-公开
公开(公告)号：US20180312629A1
公开(公告)日：2018-11-01
申请号：US15770307
申请日：2016-10-28
申请人： PIVERT , UNIVERSITÉ DE BORDEAUX , IINSTITUT DES CORPS GRAS ETUDES ET RECHERCHES TECHNIQUES - ITERG , INSTITUT POLYTECHNIQUE DE BORDEAUX , CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE
发明人： Blandine TESTUD , Etienne GRAU , Daniel TATON , Henri CRAMAIL , Didier PINTORI
IPC分类号： C08G63/688 , C07C323/52
CPC分类号： C07C323/52 , C08G63/688 , C08G63/83 , C08G63/85 , C08G63/87
摘要： The present invention relates to a compound that may be obtained according to a method comprising at least one polymerization step of at least one monomer of formula (I) below: wherein the polymerization step is carried out in the presence of a catalyst selected from the group consisting of: Zn(OAc)2, Ti(OBu)4, Ti(OiPr)4, Sb2O3, stannous octanoate, dibutyltin oxide, 7-methyl-1,5,7-triazabicyclo[4.4.0]dec-5-ene, NaOMe, 1,5,7-triazabicyclo[4.4.0]dec-5-ene and Lipase B Candida Antartica.

2. 发明申请

US20180208714A1 A low chromatic aberration polyester different-shrinkage composite yarn and its preparation method 审中-公开
公开(公告)号：US20180208714A1
公开(公告)日：2018-07-26
申请号：US15744869
申请日：2016-10-25
申请人： JIANGSU HENGLI CHEMICAL FIBRE CO., LTD.
发明人： Guanfan JIN , Yiwei SHAO , Ye ZHANG , Lijun WANG , Huaizhi ZHUO , Zhujun DING
IPC分类号： C08G63/183 , C08G63/83 , C08G63/86 , D01F6/92 , D01F1/10
CPC分类号： C08G63/183 , C08G63/83 , C08G63/86 , C08G63/866 , C25B3/12 , D01D5/08 , D01F1/10 , D01F6/62 , D01F6/92 , D02G1/18 , D06P1/16
摘要： A low chromatic aberration polyester different-shrinkage composite yarn is made of polyester POY yarn and polyester FDY composite yarn. The polyester POY yarn and polyester FDY yarn is obtained by spinning the polyester solution, the rupture strength of the low color polyester different-shrinkage composite yarn is ≥1.9 cN/dtex, the elongation at break is 30.0±5.0%, the crimp shrinkage is 2.50±3.0%, the network degree is 20±5/m, the color difference ΔE is less than 0.200. In the invention, the magnesium ethylene glycol is relatively mild, the thermal degradation coefficient is small, the oligomers in the polymerization process is reduced, and the oligomers in the dissolution process are further reduced, so that the appearance of stains and streaks reduces during the dyeing and post-processing heat setting of the polyester fiber, which ensures the fiber's leveling and rubbing fastness.

3. 发明申请

US20180022867A1 METHOD FOR PRODUCING POLYESTER 审中-公开
公开(公告)号：US20180022867A1
公开(公告)日：2018-01-25
申请号：US15543932
申请日：2016-01-15
申请人： NIPPON SODA CO., LTD.
发明人： Eiji TAKAHASHI
IPC分类号： C08G63/82 , C08G63/87 , C08G63/08 , C08G63/84 , C08G63/83
CPC分类号： C08G63/823 , C08G63/08 , C08G63/83 , C08G63/84 , C08G63/87
摘要： A cyclic ester such as lactides and the like is mixed, in an organic solvent, with an alkyl aluminum compound such as trimethyl aluminum, triethyl aluminum and the like, and then, to the resulting mixture, at least one selected from the group consisting of an organic lithium ring-opening polymerization catalyst, an organic sodium ring-opening polymerization catalyst, an organic potassium ring-opening polymerization catalyst, an organic zinc ring-opening polymerization catalyst, an organic magnesium ring-opening polymerization catalyst, an organic tin ring-opening polymerization catalyst, an organic calcium ring-opening polymerization catalyst, an organic titanium ring-opening polymerization catalyst, and an amine ring-opening polymerization catalyst to allow ring-opening polymerization of the cyclic ester, thereby a polyester is obtained.

4. 发明申请

US20180009939A1 CATALYTIC COMPOSITION FOR PREPARING PET RESIN 审中-公开
公开(公告)号：US20180009939A1
公开(公告)日：2018-01-11
申请号：US15437747
申请日：2017-02-21
申请人： ALMIGHTY GREEN MATERIAL INC. , CHUNG HOW PAINT FACTORY CO., LTD.
发明人： WEN-TING WANG , SUNG-JENG JONG , PAO-TANG CHUNG
IPC分类号： C08G63/85 , C08K3/22
CPC分类号： C08G63/85 , B01J31/0212 , C08G63/127 , C08G63/183 , C08G63/82 , C08G63/83 , C08G2390/00 , C08K3/105 , C08K3/22 , C08K2003/2258 , C08K2201/00 , C08L67/02 , C08L2203/10 , C08L2666/54
摘要： A catalytic composition for preparing a polyethylene terephthalate (PET) resin is provided. The catalytic composition comprises a polycondensation catalyst and cesium tungsten oxide (CsxWO3-yCly), and 0

5. 发明授权

US09676904B2 Metal alkoxide complex, catalyst composition, and production method of polycaprolactone or polylactide 有权
公开(公告)号：US09676904B2
公开(公告)日：2017-06-13
申请号：US14363281
申请日：2012-09-11
申请人： Dongmei Cui , Xinli Liu , Bo Liu , Shihui Li , Dongtao Liu , Chunji Wu
发明人： Dongmei Cui , Xinli Liu , Bo Liu , Shihui Li , Dongtao Liu , Chunji Wu
IPC分类号： C08G63/82 , C08G63/84 , C07C31/28 , C07C29/70 , C07C33/22 , C07C33/24 , C08G63/83 , C08G63/85 , C07C31/30 , B01J31/02 , C07F3/04 , C07F5/06
CPC分类号： C08G63/823 , B01J31/0212 , B01J2231/14 , B01J2531/22 , C07C29/70 , C07C31/28 , C07C31/30 , C07C33/22 , C07C33/24 , C07F3/04 , C07F5/069 , C08G63/826 , C08G63/83 , C08G63/84 , C08G63/85
摘要： The invention provides a metal alkoxide complex of Formula (I), wherein X, M, R1, R2, R3, m, n, y and z are as defined in the Description. The invention also provides a catalyst composition comprising the metal alkoxide complex and a hydroxy-containing compound, wherein the molar ratio of the metal alkoxide complex to the hydroxy-containing compound is 1:0.1-1000. The invention also provides a production method of poly-ε-caprolactone or polyactide, wherein an ε-caprolactone monomer or a lactide monomer is reacted in the presence of the metal alkoxide complex or catalyst composition to obtain poly-ε-caprolactone or polylactide. The metal alkoxide complex and the catalyst composition thereof can be used to catalyze the synthesis of poly-ε-caprolactone or polylactide with a high efficiency. The molecular weight of polycaprolactone or polylactide can be controlled by the molar ratio of the metal alkoxide complex and the hydroxy-containing compound, and is adjustable in the range of 1000-600,000, and wherein the molecular weight distribution is from 1.03 to 1.50. [Xn-mM(OCR1R2R3)m]y.(organic solvent)z (I)

6. 发明授权

US09334361B2 Process for preparing hyperbranched polyesters 有权
标题翻译：制备超支化聚酯的方法
公开(公告)号：US09334361B2
公开(公告)日：2016-05-10
申请号：US14001322
申请日：2012-02-23
申请人： Darbha Srinivas , Joby Sebastian
发明人： Darbha Srinivas , Joby Sebastian
IPC分类号： C08G63/00 , C08G63/83 , C08G63/12 , C08G63/87 , B01J27/26 , B01J35/10
CPC分类号： C08G63/83 , B01J27/26 , B01J35/1061 , C08G63/12 , C08G63/87 , Y02P20/52
摘要： Process for preparing hyperbranched polyesters at atmospheric pressure by reacting polyols with polycarboxylic acid in the presence of a heterogeneous, reusable, acid, crystalline, micro-mesoporous double-metal cyanide catalyst Zn3M2(CN)n(ROH).xZnCl2.yH2O at moderate temperatures for a short period of reaction time. Examples of a polyol include glycerol, sorbitol, mannitol, glucose and sucrose. Examples of a polycarboxylic acid include succinic acid and adipic acid. The hyper-branched polyester produced has a high degree of branching (56-90%), a low viscosity (inherent viscosity 0.02-0.1 dL/g), and a controlled gelation.
摘要翻译：在大气压下通过使多元醇与多元羧酸在不均匀，可重复使用的酸，结晶，微孔介孔双金属氰化物催化剂Zn3M2（CN）n（ROH）xZnCl2.yH2O存在下，在中等温度下反应制备超支化聚酯的方法反应时间短。多元醇的实例包括甘油，山梨糖醇，甘露糖醇，葡萄糖和蔗糖。多元羧酸的实例包括琥珀酸和己二酸。所生产的超支化聚酯具有高度支化度（56-90％），低粘度（特性粘度0.02-0.1dL / g）和受控凝胶化。

7. 发明授权

US08791187B2 Aluminum/alkyline or alkali/titanium containing polyesters having improved reheat, color and clarity 有权
标题翻译：铝/烷基或含碱/钛的聚酯具有改善的再热，颜色和透明度
公开(公告)号：US08791187B2
公开(公告)日：2014-07-29
申请号：US13149248
申请日：2011-05-31
申请人： Donna Rice Quillen , Rodney Scott Armentrout , Mary Therese Jernigan , Steven Lee Stafford , Zhiyong Xia
发明人： Donna Rice Quillen , Rodney Scott Armentrout , Mary Therese Jernigan , Steven Lee Stafford , Zhiyong Xia
IPC分类号： B32B27/18
CPC分类号： C08G63/83 , B29C47/0004 , B29C47/0016 , B29C47/0021 , C08G63/183 , C08G63/84 , Y10T428/1352 , Y10T428/1355 , Y10T428/139 , Y10T428/1397
摘要： A polyester composition containing: a) aluminum atoms; and b) alkaline earth atoms or alkali metal atoms or alkali compound residues such as lithium atoms; and c) particles comprising titanium, zirconium, vanadium, niobium, hafnium, tantalum, chromium, tungsten, molybdenum, iron, or nickel atoms or combinations thereof, where the particles improve the reheat rate of the polyester composition. The polyester polymer compositions may also contain phosphorus catalyst deactivators/stabilizers. The polyester compositions and the articles made from the compositions such as bottle preforms and stretch blow molded bottles have improved reheat rate while maintaining low haze, high L*, a b* below 3, and have low levels of acetaldehyde. In the process for making the polyester polymer, the polymer melt is polycondensed in the presence of a) and b), with the particles c) added in a melt phase process or added to the polymer in an injection molding machine or extruder. The polyester polymer composition can be made to high IV from the melt phase while avoiding solid state polymerization.
摘要翻译：一种聚酯组合物，其含有：a）铝原子; 和b）碱土金属原子或碱金属原子或碱金属化合物残基如锂原子; 和c）包含钛，锆，钒，铌，铪，钽，铬，钨，钼，铁或镍原子或其组合的颗粒，其中颗粒改善了聚酯组合物的再热速率。聚酯聚合物组合物还可以含有磷催化剂失活剂/稳定剂。聚酯组合物和由诸如瓶子预成型件和拉伸吹塑成型瓶的组合物制成的制品具有改善的再加热速率，同时保持低雾度，高L *，低于3的b *，并且具有低水平的乙醛。在制备聚酯聚合物的过程中，聚合物熔体在a）和b）存在下缩聚，颗粒c）以熔融相方式加入，或者在注射成型机或挤出机中加入到聚合物中。聚酯聚合物组合物可以从熔融相制成高IV，同时避免固态聚合。

8. 发明申请

US20140148558A1 ONE-STEP, ONE-POT PROCESS FOR PREPARING MULTIBLOCK AND GRADIENT COPOLYMER 有权
标题翻译：一步法，一步法制备多层和梯度共聚物
公开(公告)号：US20140148558A1
公开(公告)日：2014-05-29
申请号：US13825513
申请日：2011-09-02
申请人： Marion Helou , Sophie Guillaume , Jean-François Carpentier , Martine Slawinski , William Guerin
发明人： Marion Helou , Sophie Guillaume , Jean-François Carpentier , Martine Slawinski , William Guerin
IPC分类号： C08G63/87 , C08G63/84 , C08G63/83
CPC分类号： C08G63/87 , C08G63/08 , C08G63/64 , C08G63/83 , C08G63/84 , C08G64/0208 , C08G64/18 , C08G64/30
摘要： The present invention relates to the field of tailored di-, tri- and multi-block as well as gradient polyesters/polycarbonates copolymers prepared by introducing monomers simultaneously in the reaction medium in the presence of an organometallic, metal salt or organic catalyst.
摘要翻译：本发明涉及通过在有机金属，金属盐或有机催化剂的存在下在反应介质中同时引入单体而制备的定制的二，三和多嵌段以及梯度聚酯/聚碳酸酯共聚物的领域。

9. 发明授权

US08476183B2 Catalyst for polyester polycondensation and method for producing polyester resin using the same 有权
标题翻译：聚酯缩聚用催化剂及使用其的聚酯树脂的制造方法
公开(公告)号：US08476183B2
公开(公告)日：2013-07-02
申请号：US13210755
申请日：2011-08-16
申请人： Michio Higashijima , Yutaka Yatsugi , Naoki Yukita , Motohiro Munakata
发明人： Michio Higashijima , Yutaka Yatsugi , Naoki Yukita , Motohiro Munakata
IPC分类号： B01J23/00
CPC分类号： C08G63/83 , C08G63/85
摘要： The invention provides: a polycondensation catalyst for polyester production, which contains titanium atoms, alkaline earth metal atoms and phosphorus atoms, has high reactivity and excellent long-term storage stability, can be easily produced industrially, and has an advantage in cost; a polyester resin obtained with the catalyst; and a molded article. These are: a polymerization catalyst for polyester production containing titanium atoms, alkaline earth metal atoms and phosphorus atoms and having a specific constitution; a polyester resin obtained with the catalyst; and a molded article.
摘要翻译：本发明提供：含有钛原子，碱土金属原子和磷原子的聚酯制造用缩聚催化剂具有高反应性和优异的长期保存稳定性，可以容易地在工业上生产，并具有成本优势; 用催化剂得到的聚酯树脂; 和模制品。它们是：含有钛原子，碱土金属原子和磷原子并具有特定构成的聚酯制造用聚合催化剂; 用催化剂得到的聚酯树脂; 和模制品。

10. 发明申请

US20120071625A1 PROCESS FOR MAKING POLYETHYLENE TEREPHTHALATE 有权
标题翻译：制备聚乙烯三烯酸的方法
公开(公告)号：US20120071625A1
公开(公告)日：2012-03-22
申请号：US13256437
申请日：2010-03-10
申请人： Mummaneni Venkateswara Rao , Munif Al-Munif , Zahir Bashir
发明人： Mummaneni Venkateswara Rao , Munif Al-Munif , Zahir Bashir
IPC分类号： C08G63/183
CPC分类号： C08G63/82 , C08G63/83 , C08G63/866
摘要： The invention relates to a process for making polyethylene terephthalate (PET) from ethylene glycol (EG), purified terephthalic acid (PTA) and optionally up to 30 mol % comonomer, using a catalyst system essentially consisting of antimony—(Sb), zinc—(Zn) and phosphorous—(P) compounds, comprising the steps of a) esterifying EG and PTA to form diethyleneglycol terephthalate and oligomers (DGT), and b) melt-phase polycondensing DGT to form polyester and EG1 wherein the Sb- and P-compounds are added in step a) and the Zn-compound is added after step a). With this process PET can be obtained that shows favourable colour and optical clarity, also if recycling of EG is applied in the process, and a relatively low rate of acetaldehyde re-generation during melt-processing.
摘要翻译：本发明涉及一种由乙二醇（EG），纯对苯二甲酸（PTA）和任选的至多30mol％共聚单体制备聚对苯二甲酸乙二醇酯（PET）的方法，该催化剂体系主要由锑 - （Sb），锌 - （Zn）和磷 - （P）化合物，包括以下步骤：a）酯化EG和PTA以形成对二醇二乙二醇酯和低聚物（DGT），和b）熔融相缩聚DGT以形成聚酯和EG1，其中Sb-和P - 化合物在步骤a）中加入，并且在步骤a）之后加入Zn化合物。通过该方法，可以获得显示有利的颜色和光学透明度的PET，以及在该方法中应用EG的再循环以及在熔融加工期间相对较低的乙醛再生速率。

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