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1. 发明申请

US20100041860A1 POLYIMIDE, DIAMINE COMPOUND AND METHOD FOR PRODUCING THE SAME 审中-公开
标题翻译：聚酰亚胺，DIAMINE化合物及其生产方法
公开(公告)号：US20100041860A1
公开(公告)日：2010-02-18
申请号：US12514437
申请日：2007-11-12
申请人： Hiroaki Yamaguchi , Shuichi Maeda , Nobuharu Hisano , Shinsuke Yabunaka , Kiyotaka Yoshii , Masayoshi Ohue , Akio Matsushita , Yasuhiro Kawachi
发明人： Hiroaki Yamaguchi , Shuichi Maeda , Nobuharu Hisano , Shinsuke Yabunaka , Kiyotaka Yoshii , Masayoshi Ohue , Akio Matsushita , Yasuhiro Kawachi
IPC分类号： C08G69/26 , C07C229/52
CPC分类号： C08G73/16 , C07C219/34 , C07D277/16 , C08G73/1042 , C08G73/1046 , C08G73/1053 , C08G73/1067 , C08G73/1071 , C08L79/08 , H05K1/0346 , H05K1/0393
摘要： A polyimide obtained by reacting a tetracarboxylic acid component with a diamine component containing a diamine compound represented by the following general formula (1): wherein, A represents a biphenylene group which may be substituted with an alkyl group having up to 4 carbon atoms.
摘要翻译：通过使四羧酸成分与含有下述通式（1）表示的二胺化合物的二胺成分反应得到的聚酰亚胺：其中，A表示可被至多具有4个碳原子的烷基取代的亚联苯基。

2. 发明申请

US20090137822A1 Process for preparing 3-substituted thiophene 审中-公开
标题翻译：制备3-取代噻吩的方法
公开(公告)号：US20090137822A1
公开(公告)日：2009-05-28
申请号：US11920568
申请日：2006-05-16
申请人： Akio Matsushita , Kiyotaka Yoshii , Mizuho Oda , Masayoshi Oue , Shuji Yamada
发明人： Akio Matsushita , Kiyotaka Yoshii , Mizuho Oda , Masayoshi Oue , Shuji Yamada
IPC分类号： C07D333/38 , C07D333/22 , C07D333/16
CPC分类号： C07D333/38 , C07D333/22
摘要： The present invention relates to a process for preparing a 3-substituted thiophene represented by the formula (2): wherein R represents a cyano group, a formyl group, a carboxyl group, a hydrocarbyloxycarbonyl group which may have a substituent(s) or an acyl group which may have a substituent(s), which comprises reacting a vinyl compound represented by the formula (1): RCH═CHY (1) wherein R has the same meaning as defined above, and Y represents a leaving group, and an α-mercaptoacetaldehyde or a multimer thereof.
摘要翻译：本发明涉及一种由式（2）表示的3-取代噻吩的制备方法：其中R表示氰基，甲酰基，羧基，可具有取代基的烃氧基羰基或可以具有取代基的酰基，其包括使由式（1）表示的乙烯基化合物：<？in-line-formula description =“In-line formula”end =“lead”→RCH-CHY （1）<？in-line-formula description =“In-line Formulas”end =“tail”？>其中R具有与上述相同的含义，Y表示离去基团，而α-巯基乙醛或多聚体其中。

3. 发明授权

US07141693B2 Process for producing β-oxonitrile compound or alkali metal salt thereof 有权
标题翻译：制备β-氧腈化合物或其碱金属盐的方法
公开(公告)号：US07141693B2
公开(公告)日：2006-11-28
申请号：US10485495
申请日：2002-08-02
申请人： Akio Matsushita , Kiyotaka Yoshii , Masayoshi Oue , Taku Nakamura , Shuji Yamada
发明人： Akio Matsushita , Kiyotaka Yoshii , Masayoshi Oue , Taku Nakamura , Shuji Yamada
IPC分类号： C07C255/03
CPC分类号： C07C253/30 , C07C255/17
摘要： The present invention relates to a process for preparing a β-oxonitrile compound or an alkali metal salt thereof which comprises reacting a carboxylic ester represented by the formula (1): R1CO2R2 (1) wherein R1 and R2 each represent a group which does not participate in a reaction, provided that R2 excludes a hydrogen atom, with a nitrile compound represented by the formula (2): R3CH2CN (2) wherein R3 represents an alkyl group, and a base at 145 to 300° C. in a sealed vessel to obtain an alkali metal salt of a β-oxonitrile compound represented by the formula (3): wherein R1 and R3 have the same meanings as defined above, and neutralizing the same with an acid, if necessary.
摘要翻译：本发明涉及一种制备β-氧腈化合物或其碱金属盐的方法，包括使由式（1）表示的羧酸酯：<？in-line-formula description =“In-line Formula”end =“lead”？> R <1> 2 2（1）<？in-line-formula description =“在线公式 “末端”“尾”→其中R 1和R 2各自表示不参与反应的基团，条件是R 2 O >不包括氢原子与式（2）表示的腈化合物：<？in-line-formula description =“In-line formula”end =“lead”？> R 3 CN（2）<βin-line-formula description =“In-line Formulas”end =“tail”？>其中R 3表示烷基，和在密封容器中在145-300℃的碱，得到由式（3）表示的β-氧腈化合物的碱金属盐：其中R 1和R 3， / SUP>与定义的含义相同如果需要，用酸中和酸。

4. 发明授权

US06570015B2 Process for producing 2-substituted thiopyrimidine-4-carboxylate 失效
标题翻译：制备2-取代硫代嘧啶-4-羧酸酯的方法
公开(公告)号：US06570015B2
公开(公告)日：2003-05-27
申请号：US10245571
申请日：2002-09-17
申请人： Akio Matsushita , Kiyotaka Yoshii , Masayoshi Oue , Taku Nakamura , Shuji Yamada
发明人： Akio Matsushita , Kiyotaka Yoshii , Masayoshi Oue , Taku Nakamura , Shuji Yamada
IPC分类号： C07D23938
CPC分类号： C07D239/38
摘要： There is disclosed a process for producing a 2-substituted thiopyrimidine-4-carboxylate represented by the formula (3): wherein R2 represents a substituted or unsubstituted hydrocarbon group and R3 represents a hydrocarbon group, which comprises reacting-an &agr;-keto ester compound represented by the formula (1): R1OCH═CHCOCO2R2 (1) wherein R1 represents a substituted or unsubstituted hydrocarbon group, and R has the same meaning as defined above, with an isothiourea compound represented by the formula (2): wherein R3 has the same meaning as defined above.
摘要翻译：公开了由式（3）表示的2-取代硫代嘧啶-4-羧酸盐的制备方法：其中R2表示取代或未取代的烃基，R3表示烃基，其包括使α-酮酯化合物由式（1）表示：其中R 1表示取代或未取代的烃基，R具有与上述相同的含义，与式（2）表示的异硫脲化合物：其中R3具有与上述相同的含义。

5. 发明授权

US07816528B2 Preparation of aminopyrimidine compounds 有权
标题翻译：氨基嘧啶化合物的制备
公开(公告)号：US07816528B2
公开(公告)日：2010-10-19
申请号：US11933626
申请日：2007-11-01
申请人： Akio Matsushita , Mizuho Oda , Yasuhiro Kawachi , Jun-ichi Chika
发明人： Akio Matsushita , Mizuho Oda , Yasuhiro Kawachi , Jun-ichi Chika
IPC分类号： C07D239/34 , C07D239/22 , C07D239/42 , A61K31/505 , A61P3/06
CPC分类号： C07D239/22 , C07D239/30 , C07D239/34 , C07D239/36 , C07D239/42
摘要： A 2-(N-methyl-N-methanesulfonylamino)pyrimidine compound of the formula (3): [R is a hydrocarbyl group], is prepared by the steps of: (I) reacting an isobutyrylacetate ester with 4-fluorobenzaldehyde and urea in the presence of a protonic compound and a metal salt; (II) oxidizing the reaction product of the step (I); (III) reacting the oxidation product of the step (II) with an organic sulfonyl halide or an organic sulfonyl anhydride; and (IV) reacting the reaction product of the step (III) with N-methyl-N-methanesulfonamide.
摘要翻译：通过以下步骤制备式（3）的2-（N-甲基-N-甲磺酰基氨基）嘧啶化合物：[R是烃基]：（I）使异丁酰乙酸酯与4-氟苯甲醛和尿素反应质子化合物和金属盐的存在; （II）氧化步骤（I）的反应产物; （III）使步骤（II）的氧化产物与有机磺酰卤或有机磺酰酐反应; 和（IV）使步骤（III）的反应产物与N-甲基-N-甲磺酰胺反应。

6. 发明授权

US5677455A Preparation of 3-oxy-5-oxo-6-heptenoic acid derivatives 失效
标题翻译： 3-氧基-5-氧代-6-庚烯酸衍生物的制备
公开(公告)号：US5677455A
公开(公告)日：1997-10-14
申请号：US524045
申请日：1995-09-06
申请人： Katsumasa Harada , Akio Matsushita , Yasuhiro Kawachi , Hiroshi Sasaki
发明人： Katsumasa Harada , Akio Matsushita , Yasuhiro Kawachi , Hiroshi Sasaki
IPC分类号： C07F7/18 , C07F7/02 , C07D213/30
CPC分类号： C07F7/1852 , C07F7/1856 , C07F7/1892
摘要： Methyl (3R,6E)-3-�(tert-butyldimethylsilyl)oxy!-7-�2',6'-diisopropyl-4'-(4"-fluorophenyl)-5'-(methoxymethyl)pyridin-3'-yl!-5-oxy-6-heptenoate or other 3-oxy-5-oxo-6-heptenoic acid derivative is prepared by the reaction of an aromatic aldehyde and an oxyglutaric acid derivative in an aliphatic alcohol containing a small amount of water in the presence of an alkali metal carbonate or hydrogen carbonate.
摘要翻译：将（3R，6E）-3 - [（叔丁基二甲基甲硅烷基）氧基] -7- [2'，6'-二异丙基-4' - （4“ - 氟苯基）-5' - （甲氧基甲基） - 基] -5-氧基-6-庚烯酸乙酯或其它3-氧基-5-氧代-6-庚烯酸衍生物通过芳族醛和羟基戊二酸衍生物在含少量水的脂族醇中的反应来制备在碱金属碳酸盐或碳酸氢盐存在下进行。

7. 发明授权

US08614320B2 Preparation of aminopyrimidine compounds 有权
标题翻译：氨基嘧啶化合物的制备
公开(公告)号：US08614320B2
公开(公告)日：2013-12-24
申请号：US13523534
申请日：2012-06-14
申请人： Akio Matsushita , Mizuho Oda , Yasuhiro Kawachi , Jun-ichi Chika
发明人： Akio Matsushita , Mizuho Oda , Yasuhiro Kawachi , Jun-ichi Chika
IPC分类号： C07D239/36 , C07D239/42 , C07D239/22 , A61K31/505 , A61P3/06
CPC分类号： C07D239/22 , C07D239/30 , C07D239/34 , C07D239/36 , C07D239/42
摘要： A 2-(N-methyl-N-methanesulfonylamino)pyrimidine compound of the formula (3): [R is a hydrocarbyl group], is prepared by the steps of: (I) reacting an isobutyrylacetate ester with 4-fluorobenzaldehyde and urea in the presence of a protonic compound and a metal salt; (II) oxidizing the reaction product of the step (I); (III) reacting the oxidation product of the step (II) with an organic sulfonyl halide or an organic sulfonyl anhydride; and (IV) reacting the reaction product of the step (III) with N-methyl-N-methanesulfonamide.
摘要翻译：通过以下步骤制备式（3）的2-（N-甲基-N-甲磺酰基氨基）嘧啶化合物：[R是烃基]：（I）使异丁酰乙酸酯与4-氟苯甲醛和尿素反应质子化合物和金属盐的存在; （II）氧化步骤（I）的反应产物; （III）使步骤（II）的氧化产物与有机磺酰卤或有机磺酰酐反应; 和（IV）使步骤（III）的反应产物与N-甲基-N-甲烷磺酰胺反应。

8. 发明授权

US08222412B2 Preparation of aminopyrimidine compounds 有权
标题翻译：氨基嘧啶化合物的制备
公开(公告)号：US08222412B2
公开(公告)日：2012-07-17
申请号：US12889186
申请日：2010-09-23
申请人： Akio Matsushita , Mizuho Oda , Yasuhiro Kawachi , Jun-ichi Chika
发明人： Akio Matsushita , Mizuho Oda , Yasuhiro Kawachi , Jun-ichi Chika
IPC分类号： C07D239/34 , C07D239/22 , C07D239/42
CPC分类号： C07D239/22 , C07D239/30 , C07D239/34 , C07D239/36 , C07D239/42
摘要： A 2-(N-methyl-N-methanesulfonylamino)pyrimidine compound of the formula (3): [R is a hydrocarbyl group], is prepared by the steps of: (I) reacting an isobutyrylacetate ester with 4-fluorobenzaldehyde and urea in the presence of a protonic compound and a metal salt; (II) oxidizing the reaction product of the step (I); (III) reacting the oxidation product of the step (II) with an organic sulfonyl halide or an organic sulfonyl anhydride; and (IV) reacting the reaction product of the step (III) with N-methyl-N-methanesulfonamide.
摘要翻译：通过以下步骤制备式（3）的2-（N-甲基-N-甲磺酰基氨基）嘧啶化合物：[R是烃基]：（I）使异丁酰乙酸酯与4-氟苯甲醛和尿素反应质子化合物和金属盐的存在; （II）氧化步骤（I）的反应产物; （III）使步骤（II）的氧化产物与有机磺酰卤或有机磺酰酐反应; 和（IV）使步骤（III）的反应产物与N-甲基-N-甲磺酰胺反应。

9. 发明申请

US20110160455A1 Preparation of Aminopyrimidine Compounds 有权
标题翻译：氨基嘧啶化合物的制备
公开(公告)号：US20110160455A1
公开(公告)日：2011-06-30
申请号：US12889186
申请日：2010-09-23
申请人： Akio Matsushita , Mizuho Oda , Yasuhiro Kawachi , Jun-ichi Chika
发明人： Akio Matsushita , Mizuho Oda , Yasuhiro Kawachi , Jun-ichi Chika
IPC分类号： C07D239/22 , C07D239/42 , C07D239/30
CPC分类号： C07D239/22 , C07D239/30 , C07D239/34 , C07D239/36 , C07D239/42
摘要： A 2-(N-methyl-N-methanesulfonylamino)pyrimidine compound of the formula (3): [R is a hydrocarbyl group], is prepared by the steps of: (I) reacting an isobutyrylacetate ester with 4-fluorobenzaldehyde and urea in the presence of a protonic compound and a metal salt; (II) oxidizing the reaction product of the step (I); (III) reacting the oxidation product of the step (II) with an organic sulfonyl halide or an organic sulfonyl anhydride; and (IV) reacting the reaction product of the step (III) with N-methyl-N-methanesulfonamide.
摘要翻译：通过以下步骤制备式（3）的2-（N-甲基-N-甲磺酰基氨基）嘧啶化合物：[R是烃基]：（I）使异丁酰乙酸酯与4-氟苯甲醛和尿素反应质子化合物和金属盐的存在; （II）氧化步骤（I）的反应产物; （III）使步骤（II）的氧化产物与有机磺酰卤或有机磺酰酐反应; 和（IV）使步骤（III）的反应产物与N-甲基-N-甲磺酰胺反应。

10. 发明申请

US20080058520A1 Preparation of Aminopyrimidine Compounds 有权
标题翻译：氨基嘧啶化合物的制备
公开(公告)号：US20080058520A1
公开(公告)日：2008-03-06
申请号：US11933626
申请日：2007-11-01
申请人： Akio Matsushita , Mizuho ODA , Yasuhiro KAWACHI , Jun-ichi CHIKA
发明人： Akio Matsushita , Mizuho ODA , Yasuhiro KAWACHI , Jun-ichi CHIKA
IPC分类号： C07D239/36
CPC分类号： C07D239/22 , C07D239/30 , C07D239/34 , C07D239/36 , C07D239/42
摘要： A 2-(N-methyl-N-methanesulfonylamino)pyrimidine compound of the formula (3): [R is a hydrocarbyl group], is prepared by the steps of: (I) reacting an isobutyrylacetate ester with 4-fluorobenzaldehyde and urea in the presence of a protonic compound and a metal salt; (II) oxidizing the reaction product of the step (I); (III) reacting the oxidation product of the step (II) with an organic sulfonyl halide or an organic sulfonyl anhydride; and (IV) reacting the reaction product of the step (III) with N-methyl-N-methanesulfonamide.
摘要翻译：通过以下步骤制备式（3）的2-（N-甲基-N-甲磺酰基氨基）嘧啶化合物：[R是烃基]：（I）使异丁酰乙酸酯与4-氟苯甲醛和尿素反应质子化合物和金属盐的存在; （II）氧化步骤（I）的反应产物; （III）使步骤（II）的氧化产物与有机磺酰卤或有机磺酰酐反应; 和（IV）使步骤（III）的反应产物与N-甲基-N-甲磺酰胺反应。

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