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1. 发明授权

US06229146B1 Position sensitive radioactivity detection for gas and liquid chromatography 失效
标题翻译：气体和液相色谱的位置敏感放射性检测
公开(公告)号：US06229146B1
公开(公告)日：2001-05-08
申请号：US09164107
申请日：1998-09-30
申请人： Joseph L. Cochran , John F. McCarthy , Anthony V. Palumbo , Tommy J. Phelps
发明人： Joseph L. Cochran , John F. McCarthy , Anthony V. Palumbo , Tommy J. Phelps
IPC分类号： G01T120
CPC分类号： G01T1/178
摘要： A method and apparatus are provided for the position sensitive detection of radioactivity in a fluid stream, particularly in the effluent fluid stream from a gas or liquid chromatographic instrument. The invention represents a significant advance in efficiency and cost reduction compared with current efforts.
摘要翻译：提供了一种方法和装置，用于对液体流中的放射性进行位置敏感检测，特别是来自气体或液体色谱仪的流出液流。与目前的努力相比，本发明显着提高了效率和成本。

2. 发明授权

US07569737B2 Method for excluding salt and other soluble materials from produced water 失效
标题翻译：从生产水中排除盐和其他可溶性物质的方法
公开(公告)号：US07569737B2
公开(公告)日：2009-08-04
申请号：US11171561
申请日：2005-06-30
申请人： Tommy J. Phelps , Costas Tsouris , Anthony V. Palumbo , David E. Riestenberg , Scott D. McCallum
发明人： Tommy J. Phelps , Costas Tsouris , Anthony V. Palumbo , David E. Riestenberg , Scott D. McCallum
IPC分类号： C02F1/00
CPC分类号： C02F1/265 , C02F1/22 , C02F2101/32 , C02F2103/08 , C02F2301/066 , Y02A20/132
摘要： A method for reducing the salinity, as well as the hydrocarbon concentration of produced water to levels sufficient to meet surface water discharge standards. Pressure vessel and coflow injection technology developed at the Oak Ridge National Laboratory is used to mix produced water and a gas hydrate forming fluid to form a solid or semi-solid gas hydrate mixture. Salts and solids are excluded from the water that becomes a part of the hydrate cage. A three-step process of dissociation of the hydrate results in purified water suitable for irrigation.
摘要翻译：将盐度降低的方法以及产生的水的碳氢化合物浓度达到足以满足地表水排放标准的水平。在橡树岭国家实验室开发的压力容器和共流注入技术用于混合生产的水和形成气体水合物的气体水合物形成固体或半固体气体水合物混合物。将盐和固体排除在成为水合物笼的一部分的水中。水合物的三步解离过程产生适合灌溉的纯净水。

3. 发明授权

US5480549A Method for phosphate-accelerated bioremediation 失效
标题翻译：磷酸盐加速生物修复方法
公开(公告)号：US5480549A
公开(公告)日：1996-01-02
申请号：US186065
申请日：1994-01-25
申请人： Brian B. Looney , Kenneth H. Lombard , Terry C. Hazen , Susan M. Pfiffner , Tommy J. Phelps , James W. Borthen
发明人： Brian B. Looney , Kenneth H. Lombard , Terry C. Hazen , Susan M. Pfiffner , Tommy J. Phelps , James W. Borthen
IPC分类号： B09C1/10 , C02F3/34
CPC分类号： B09C1/10 , B09C2101/00 , Y02E50/343
摘要： An apparatus and method for supplying a vapor-phase nutrient to contaminated soil for in situ bioremediation. The apparatus includes a housing adapted for containing a quantity of the liquid nutrient, a conduit in fluid communication with the interior of the housing, means for causing a gas to flow through the conduit, and means for contacting the gas with the liquid so that a portion thereof evaporates and mixes with the gas. The mixture of gas and nutrient vapor is delivered to the contaminated site via a system of injection and extraction wells configured to the site. The mixture has a partial pressure of vaporized nutrient that is no greater than the vapor pressure of the liquid. If desired, the nutrient and/or the gas may be heated to increase the vapor pressure and the nutrient concentration of the mixture. Preferably, the nutrient is a volatile, substantially nontoxic and nonflammable organic phosphate that is a liquid at environmental temperatures, such as triethyl phosphate or tributyl phosphate.
摘要翻译：一种用于向污染土壤供应气相营养物质用于原位生物修复的装置和方法。该装置包括适于容纳一定数量的液体营养物质的壳体，与壳体内部流体连通的导管，用于使气体流过导管的装置，以及用于使气体与液体接触的装置，其部分蒸发并与气体混合。气体和营养蒸气的混合物通过配置到现场的注射和提取井的系统输送到污染部位。该混合物具有不大于液体的蒸气压的汽化营养物的分压。如果需要，可以加热营养物和/或气体以增加混合物的蒸气压和营养物浓度。优选地，营养物是在环境温度下为液体的挥发性，基本上无毒的和不可燃的有机磷酸盐，例如磷酸三乙酯或磷酸三丁酯。

4. 发明申请

US20100184179A1 MICROBIAL-MEDIATED METHOD FOR METAL OXIDE NANOPARTICLE FORMATION 有权
标题翻译：用于金属氧化物纳米颗粒形成的微观介质方法
公开(公告)号：US20100184179A1
公开(公告)日：2010-07-22
申请号：US12357523
申请日：2009-01-22
申请人： Adam J. Rondinone , Ji Won Moon , Lonnie J. Love , Lucas W. Yeary , Tommy J. Phelps
发明人： Adam J. Rondinone , Ji Won Moon , Lonnie J. Love , Lucas W. Yeary , Tommy J. Phelps
IPC分类号： C12P3/00
CPC分类号： C12P3/00 , B82Y5/00 , B82Y40/00
摘要： The invention is directed to a method for producing metal oxide nanoparticles, the method comprising: (i) subjecting a combination of reaction components to conditions conducive to microbial-mediated formation of metal oxide nanoparticles, wherein said combination of reaction components comprise: metal-reducing microbes, a culture medium suitable for sustaining said metal-reducing microbes, an effective concentration of one or more surfactants, a reducible metal oxide component containing one or more reducible metal species, and one or more electron donors that provide donatable electrons to said metal-reducing microbes during consumption of the electron donor by said metal-reducing microbes; and (ii) isolating said metal oxide nanoparticles, which contain a reduced form of said reducible metal oxide component. The invention is also directed to metal oxide nanoparticle compositions produced by the inventive method.
摘要翻译：本发明涉及一种生产金属氧化物纳米颗粒的方法，所述方法包括：（i）使反应组分的组合经受有助于微生物介导的金属氧化物纳米颗粒形成的条件，其中所述反应组分的组合包括：金属还原微生物，适于维持所述金属还原微生物的培养基，有效浓度的一种或多种表面活性剂，含有一种或多种可还原金属物质的可还原金属氧化物组分和一种或多种向所述金属 - 通过所述金属还原微生物在电子给体消耗期间还原微生物; 和（ii）分离含有还原形式的所述可还原金属氧化物组分的所述金属氧化物纳米颗粒。本发明还涉及通过本发明方法制备的金属氧化物纳米颗粒组合物。

5. 发明申请

US20100193752A1 MICROBIALLY-MEDIATED METHOD FOR SYNTHESIS OF NON-OXIDE SEMICONDUCTOR NANOPARTICLES 有权
标题翻译：用于合成非氧化物半导体纳米粒子的微观介质方法
公开(公告)号：US20100193752A1
公开(公告)日：2010-08-05
申请号：US12364638
申请日：2009-02-03
申请人： Tommy J. Phelps , Robert J. Lauf , Ji Won Moon , Adam J. Rondinone , Lonnie J. Love , Chad Edward Duty , Andrew Stephen Madden , Yiliang Li , Ilia N. Ivanov , Claudia Jeanette Rawn
发明人： Tommy J. Phelps , Robert J. Lauf , Ji Won Moon , Adam J. Rondinone , Lonnie J. Love , Chad Edward Duty , Andrew Stephen Madden , Yiliang Li , Ilia N. Ivanov , Claudia Jeanette Rawn
IPC分类号： H01B1/10 , C12P3/00
CPC分类号： C12P3/00
摘要： The invention is directed to a method for producing non-oxide semiconductor nanoparticles, the method comprising: (a) subjecting a combination of reaction components to conditions conducive to microbially-mediated formation of non-oxide semiconductor nanoparticles, wherein said combination of reaction components comprises i) anaerobic microbes, ii) a culture medium suitable for sustaining said anaerobic microbes, iii) a metal component comprising at least one type of metal ion, iv) a non-metal component containing at least one non-metal selected from the group consisting of S, Se, Te, and As, and v) one or more electron donors that provide donatable electrons to said anaerobic microbes during consumption of the electron donor by said anaerobic microbes; and (b) isolating said non-oxide semiconductor nanoparticles, which contain at least one of said metal ions and at least one of said non-metals. The invention is also directed to non-oxide semiconductor nanoparticle compositions produced as above and having distinctive properties.
摘要翻译：本发明涉及一种生产非氧化物半导体纳米颗粒的方法，所述方法包括：（a）使反应组分的组合经受有利于微生物介导的非氧化物半导体纳米颗粒的形成的条件，其中所述反应组分的组合包括 i）厌氧微生物，ii）适于维持所述厌氧微生物的培养基，iii）包含至少一种类型的金属离子的金属组分，iv）含有至少一种选自以下的非金属的非金属组分：的S，Se，Te和As，以及v）一个或多个电子给体，其在所述厌氧微生物消耗电子给体期间向所述厌氧微生物提供可供给的电子; 和（b）分离含有至少一种所述金属离子和至少一种所述非金属的所述非氧化物半导体纳米颗粒。本发明还涉及如上制备的且具有独特性质的非氧化物半导体纳米颗粒组合物。

6. 发明授权

US09127295B2 Microbial-mediated method for metal oxide nanoparticle formation 有权
标题翻译：微生物介导的金属氧化物纳米颗粒形成方法
公开(公告)号：US09127295B2
公开(公告)日：2015-09-08
申请号：US12357523
申请日：2009-01-22
申请人： Adam J. Rondinone , Ji Won Moon , Lonnie J. Love , Lucas W. Yeary , Tommy J. Phelps
发明人： Adam J. Rondinone , Ji Won Moon , Lonnie J. Love , Lucas W. Yeary , Tommy J. Phelps
IPC分类号： C12P3/00 , B82Y5/00 , B82Y40/00
CPC分类号： C12P3/00 , B82Y5/00 , B82Y40/00
摘要： The invention is directed to a method for producing metal oxide nanoparticles, the method comprising: (i) subjecting a combination of reaction components to conditions conducive to microbial-mediated formation of metal oxide nanoparticles, wherein said combination of reaction components comprise: metal-reducing microbes, a culture medium suitable for sustaining said metal-reducing microbes, an effective concentration of one or more surfactants, a reducible metal oxide component containing one or more reducible metal species, and one or more electron donors that provide donatable electrons to said metal-reducing microbes during consumption of the electron donor by said metal-reducing microbes; and (ii) isolating said metal oxide nanoparticles, which contain a reduced form of said reducible metal oxide component. The invention is also directed to metal oxide nanoparticle compositions produced by the inventive method.
摘要翻译：本发明涉及一种生产金属氧化物纳米颗粒的方法，所述方法包括：（i）使反应组分的组合经受有助于微生物介导的金属氧化物纳米颗粒形成的条件，其中所述反应组分的组合包括：金属还原微生物，适于维持所述金属还原微生物的培养基，有效浓度的一种或多种表面活性剂，含有一种或多种可还原金属物质的可还原金属氧化物组分和一种或多种向所述金属 - 通过所述金属还原微生物在电子给体消耗期间还原微生物; 和（ii）分离含有还原形式的所述可还原金属氧化物组分的所述金属氧化物纳米颗粒。本发明还涉及通过本发明方法制备的金属氧化物纳米颗粒组合物。

7. 发明申请

US20140220724A1 METHODS FOR PRODUCING COMPLEX FILMS, AND FILMS PRODUCED THEREBY 有权
标题翻译：生产复合膜的方法及其生产的薄膜
公开(公告)号：US20140220724A1
公开(公告)日：2014-08-07
申请号：US14110222
申请日：2012-03-22
申请人： Chad E. Duty , Charlee JC Bennett , Ji-Won Moom , Tommy J. Phelps , Craig A. Blue , Quanqin Dai , Michael Z. Hu , Ilia N. Ivanov , Gerald E. Jellison, JR. , Lonnie J. Love , Ronald D. Ott , Chad M. Parish , Steven Walker
发明人： Chad E. Duty , Charlee JC Bennett , Ji-Won Moom , Tommy J. Phelps , Craig A. Blue , Quanqin Dai , Michael Z. Hu , Ilia N. Ivanov , Gerald E. Jellison, JR. , Lonnie J. Love , Ronald D. Ott , Chad M. Parish , Steven Walker
IPC分类号： H01L31/0232
CPC分类号： H01L31/0232 , C12P3/00 , H01L21/02521 , H01L21/02568 , H01L21/02587 , H01L21/02601 , H01L21/02628 , H01L21/02656 , Y02P20/59
摘要： A method for producing a film, the method comprising melting a layer of precursor particles on a substrate until at least a portion of the melted particles are planarized and merged to produce the film. The invention is also directed to a method for producing a photovoltaic film, the method comprising depositing particles having a photovoltaic or other property onto a substrate, and affixing the particles to the substrate, wherein the particles may or may not be subsequently melted. Also described herein are films produced by these methods, methods for producing a patterned film on a substrate, and methods for producing a multilayer structure.
摘要翻译：一种薄膜的制造方法，其特征在于，在基材上熔融前体粒子层，直至将熔融粒子的至少一部分平坦化并合并，制成薄膜。本发明还涉及一种用于生产光伏膜的方法，该方法包括将具有光伏或其它性质的颗粒沉积在基材上，并将颗粒固定在基材上，其中颗粒可以随后熔化或不再熔化。本文还描述了通过这些方法制造的膜，在基板上制造图案化膜的方法，以及制造多层结构的方法。

8. 发明授权

US5753109A Apparatus and method for phosphate-accelerated bioremediation 失效
标题翻译：磷酸盐加速生物修复的装置和方法
公开(公告)号：US5753109A
公开(公告)日：1998-05-19
申请号：US579910
申请日：1995-12-28
申请人： Brian B. Looney , Susan M. Pfiffner , Tommy J. Phelps , Kenneth H. Lombard , Terry C. Hazen , James W. Borthen
发明人： Brian B. Looney , Susan M. Pfiffner , Tommy J. Phelps , Kenneth H. Lombard , Terry C. Hazen , James W. Borthen
IPC分类号： B09C1/10 , C02F3/34 , E21B43/22
CPC分类号： B09C1/10 , B09C2101/00
摘要： An apparatus and method for supplying a vapor-phase nutrient to contaminated soil for in situ bioremediation. The apparatus includes a housing adapted for containing a quantity of the liquid nutrient, a conduit in communication with the interior of the housing, means for causing a gas to flow through the conduit, and means for contacting the gas with the liquid so that a portion thereof evaporates and mixes with the gas. The mixture of gas and nutrient vapor is delivered to the contaminated site via a system of injection and extraction wells configured to the site and provides for the use of a passive delivery system. The mixture has a partial pressure of vaporized nutrient that is no greater than the vapor pressure of the liquid. If desired, the nutrient and/or the gas may be heated to increase the vapor pressure and the nutrient concentration of the mixture. Preferably, the nutrient is a volatile, substantially nontoxic and nonflammable organic phosphate that is a liquid at environmental temperatures, such as triethyl phosphate or tributyl phosphate.
摘要翻译：一种用于向污染土壤供应气相营养物质用于原位生物修复的装置和方法。该装置包括适于容纳一定数量的液体营养物的壳体，与壳体内部连通的导管，用于使气体流过导管的装置，以及用于使气体与液体接触的装置，其蒸发并与气体混合。气体和营养蒸汽的混合物通过配置到现场的注入和提取井系统输送到污染场地，并提供使用被动输送系统。该混合物具有不大于液体的蒸气压的汽化营养物的分压。如果需要，可以加热营养物和/或气体以增加混合物的蒸汽压力和营养物浓度。优选地，营养物是在环境温度下是液体的挥发性，基本上无毒的和不可燃的有机磷酸盐，例如磷酸三乙酯或磷酸三丁酯。

9. 发明授权

US09196760B2 Methods for producing complex films, and films produced thereby 有权
标题翻译：复合膜的制造方法以及由此制造的膜
公开(公告)号：US09196760B2
公开(公告)日：2015-11-24
申请号：US14110222
申请日：2012-03-22
申请人： Chad E. Duty , Charlee J C Bennett , Ji-Won Moon , Tommy J. Phelps , Craig A. Blue , Quanqin Dai , Michael Z. Hu , Ilia N. Ivanov , Gerald E. Jellison, Jr. , Lonnie J. Love , Ronald D. Ott , Chad M. Parish , Steven Walker
发明人： Chad E. Duty , Charlee J C Bennett , Ji-Won Moon , Tommy J. Phelps , Craig A. Blue , Quanqin Dai , Michael Z. Hu , Ilia N. Ivanov , Gerald E. Jellison, Jr. , Lonnie J. Love , Ronald D. Ott , Chad M. Parish , Steven Walker
IPC分类号： H01L21/00 , H01L31/0232 , H01L21/02 , C12P3/00
CPC分类号： H01L31/0232 , C12P3/00 , H01L21/02521 , H01L21/02568 , H01L21/02587 , H01L21/02601 , H01L21/02628 , H01L21/02656 , Y02P20/59
摘要： A method for producing a film, the method comprising melting a layer of precursor particles on a substrate until at least a portion of the melted particles are planarized and merged to produce the film. The invention is also directed to a method for producing a photovoltaic film, the method comprising depositing particles having a photovoltaic or other property onto a substrate, and affixing the particles to the substrate, wherein the particles may or may not be subsequently melted. Also described herein are films produced by these methods, methods for producing a patterned film on a substrate, and methods for producing a multilayer structure.
摘要翻译：一种薄膜的制造方法，其特征在于，在基材上熔融前体粒子层，直至将熔融粒子的至少一部分平坦化并合并，制成薄膜。本发明还涉及一种用于生产光伏膜的方法，该方法包括将具有光伏或其它性质的颗粒沉积在基材上，并将颗粒固定在基材上，其中颗粒可以随后熔化或不再熔化。本文还描述了通过这些方法制造的膜，在基板上制造图案化膜的方法，以及制造多层结构的方法。

10. 发明授权

US08759053B2 Microbially-mediated method for synthesis of non-oxide semiconductor nanoparticles 有权
标题翻译：用于合成非氧化物半导体纳米颗粒的微生物介导方法
公开(公告)号：US08759053B2
公开(公告)日：2014-06-24
申请号：US12364638
申请日：2009-02-03
申请人： Tommy J. Phelps , Robert J. Lauf , Ji Won Moon , Adam J. Rondinone , Lonnie J. Love , Chad Edward Duty , Andrew Stephen Madden , Yiliang Li , Ilia N. Ivanov , Claudia Jeanette Rawn
发明人： Tommy J. Phelps , Robert J. Lauf , Ji Won Moon , Adam J. Rondinone , Lonnie J. Love , Chad Edward Duty , Andrew Stephen Madden , Yiliang Li , Ilia N. Ivanov , Claudia Jeanette Rawn
IPC分类号： C12P3/00 , C01B17/00 , C01B19/00 , C01G9/00 , C01B11/00 , H01B1/00
CPC分类号： C12P3/00
摘要： The invention is directed to a method for producing non-oxide semiconductor nanoparticles, the method comprising: (a) subjecting a combination of reaction components to conditions conducive to microbially-mediated formation of non-oxide semiconductor nanoparticles, wherein said combination of reaction components comprises i) anaerobic microbes, ii) a culture medium suitable for sustaining said anaerobic microbes, iii) a metal component comprising at least one type of metal ion, iv) a non-metal component containing at least one non-metal selected from the group consisting of S, Se, Te, and As, and v) one or more electron donors that provide donatable electrons to said anaerobic microbes during consumption of the electron donor by said anaerobic microbes; and (b) isolating said non-oxide semiconductor nanoparticles, which contain at least one of said metal ions and at least one of said non-metals. The invention is also directed to non-oxide semiconductor nanoparticle compositions produced as above and having distinctive properties.
摘要翻译：本发明涉及一种生产非氧化物半导体纳米颗粒的方法，所述方法包括：（a）使反应组分的组合经受有利于微生物介导的非氧化物半导体纳米颗粒的形成的条件，其中所述反应组分的组合包括 i）厌氧微生物，ii）适于维持所述厌氧微生物的培养基，iii）包含至少一种类型的金属离子的金属组分，iv）含有至少一种选自以下的非金属的非金属组分：的S，Se，Te和As，以及v）一个或多个电子给体，其在所述厌氧微生物消耗电子给体期间向所述厌氧微生物提供可供给的电子; 和（b）分离含有至少一种所述金属离子和至少一种所述非金属的所述非氧化物半导体纳米颗粒。本发明还涉及如上制备的且具有独特性质的非氧化物半导体纳米颗粒组合物。

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