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1. 发明授权

US07659359B1 Stabilization of isosorbide-based polycarbonate 有权
标题翻译：异山梨醇基聚碳酸酯的稳定化
公开(公告)号：US07659359B1
公开(公告)日：2010-02-09
申请号：US12273132
申请日：2008-11-18
申请人： Roland Assink , Hans de Brouwer , Bernd Jansen , Jan Henk Kamps , Wilhelmus Johannes Daniel Steendam , Jan-Willem Goedmakers
发明人： Roland Assink , Hans de Brouwer , Bernd Jansen , Jan Henk Kamps , Wilhelmus Johannes Daniel Steendam , Jan-Willem Goedmakers
IPC分类号： C08G64/00 , C08G63/00
CPC分类号： C08J3/02 , C08G64/0208 , C08J2369/00
摘要： An isosorbide-containing polycarbonate composition is provided. The composition contains a polycarbonate having repeat units derived from isosorbide, a polycarbonate-property-modifying additive, and a pH stabilizer. When a solution containing 10 wt. % of the composition dissolved in dichloromethane is prepared the solution has a non-aqueous pH in a range of equal to or between 0.8 below and 0.5 above the pH of the dichloromethane.
摘要翻译：提供含有异山梨醇的聚碳酸酯组合物。组合物含有具有衍生自异山梨醇，聚碳酸酯性质改性添加剂和pH稳定剂的重复单元的聚碳酸酯。当含有10wt。制备溶解在二氯甲烷中的组合物的％，该溶液具有在二氯甲烷的pH以下等于或低于0.8或低于0.5的范围内的非水性pH。

2. 发明申请

US20080004418A1 Method of Preparing Polycarbonate 有权
标题翻译：聚碳酸酯的制备方法
公开(公告)号：US20080004418A1
公开(公告)日：2008-01-03
申请号：US11427885
申请日：2006-06-30
申请人： Bernd Jansen , Jan Henk Kamps , Edward Kung , Patrick Joseph McCloskey , Paul Michael Smigelski
发明人： Bernd Jansen , Jan Henk Kamps , Edward Kung , Patrick Joseph McCloskey , Paul Michael Smigelski
IPC分类号： C08G64/00
CPC分类号： C08G64/14 , C08G64/307
摘要： Polycarbonates incorporating terminal carbonate groups derived from ester-substituted activated carbonates in a transesterification process have unfavorable properties with respect to color, hydrolytic stability and thermal stability, particularly when the polycarbonate containing such end groups is molded. The number of activated carbonate end groups formed during the melt transesterification formation of polycarbonate can be reduced by reacting a dihydroxy compound with an activated diaryl carbonate in the presence of an esterification catalyst to produce a polycarbonate, in the presence of a monohydroxy chainstopper such as para-cumyl phenol in an amount that results in 35 to 65 mol % of the end groups being derived from the monohydroxy chainstopper. Suitably, the reactants are provided such that the molar ratio of activated diaryl carbonate to the total of dihydroxy compound plus ½ the chainstopping reagent that is less than 1.
摘要翻译：在酯交换方法中，衍生自酯取代的活性碳酸酯的末端碳酸酯基团的聚碳酸酯在颜色，水解稳定性和热稳定性方面具有不利的性质，特别是当含有这样的端基的聚碳酸酯被成型时。在聚碳酸酯的熔融酯交换形成期间形成的活化碳酸酯端基的数量可以通过在酯化催化剂的存在下使二羟基化合物与活化的碳酸二芳基酯反应来制备聚碳酸酯，在单羟基链断裂剂例如对 - 辛基苯酚，其量导致35-65mol％端基衍生自单羟基链断裂剂。适当地，提供反应物使得活化的碳酸二芳基酯与二羟基化合物的总和加上1/2的阻滞剂的摩尔比小于1。

3. 发明申请

US20080004407A1 Method for Making Molded Polycarbonate Articles with Improved Color 有权
标题翻译：制造具有改进颜色的模制聚碳酸酯制品的方法
公开(公告)号：US20080004407A1
公开(公告)日：2008-01-03
申请号：US11688533
申请日：2007-03-20
申请人： Sjef Berndsen , Hans-Peter Brack , Bernd Jansen , Jan Henk Kamps , Edward Kung , Daniel Lowery , Patrick Joseph McCloskey , Paul Michael Smigelski , Dennis Willemse
发明人： Sjef Berndsen , Hans-Peter Brack , Bernd Jansen , Jan Henk Kamps , Edward Kung , Daniel Lowery , Patrick Joseph McCloskey , Paul Michael Smigelski , Dennis Willemse
IPC分类号： C08G64/14 , C08G65/48
CPC分类号： C08G64/307 , C08G64/14
摘要： A method for preparing a molded article includes the steps of (a) obtaining a polycarbonate resin and (b) molding the polycarbonate resin. The polycarbonate resin is made by a transesterification reaction using an activated diaryl carbonate such that the polycarbonate is susceptible to the formation of internal ester linkages (IEL). The method occurs with the proviso that the polycarbonate resin, the molding conditions or both are selected to control the amount of IEL formed during the molding process to a level of less than 0.4 mol %.
摘要翻译：制备模塑制品的方法包括以下步骤：（a）获得聚碳酸酯树脂和（b）模塑聚碳酸酯树脂。聚碳酸酯树脂通过使用活化的碳酸二芳基酯的酯交换反应制备，使得聚碳酸酯容易形成内部酯键（IEL）。该方法发生，条件是选择聚碳酸酯树脂，成型条件或两者以控制在模制过程中形成的IEL的量至小于0.4mol％的水平。

4. 发明授权

US07541420B2 Method for making molded polycarbonate articles with improved color 有权
标题翻译：制造具有改进颜色的聚碳酸酯制品的方法
公开(公告)号：US07541420B2
公开(公告)日：2009-06-02
申请号：US11688533
申请日：2007-03-20
申请人： Sjef Berndsen , Hans Peter Brack , Bernd Jansen , Jan Henk Kamps , Edward Kung , Daniel Lowery , Patrick Joseph McCloskey , Paul Michael Smigelski, Jr. , Dennis Willemse
发明人： Sjef Berndsen , Hans Peter Brack , Bernd Jansen , Jan Henk Kamps , Edward Kung , Daniel Lowery , Patrick Joseph McCloskey , Paul Michael Smigelski, Jr. , Dennis Willemse
IPC分类号： C08G64/00 , C08G63/02
CPC分类号： C08G64/307 , C08G64/14
摘要： A method for preparing a molded article includes the steps of (a) obtaining a polycarbonate resin and (b) molding the polycarbonate resin. The polycarbonate resin is made by a transesterification reaction using an activated diaryl carbonate such that the polycarbonate is susceptible to the formation of internal ester linkages (IEL). The method occurs with the proviso that the polycarbonate resin, the molding conditions or both are selected to control the amount of IEL formed during the molding process to a level of less than 0.4 mol %.
摘要翻译：制备模塑制品的方法包括以下步骤：（a）获得聚碳酸酯树脂和（b）模塑聚碳酸酯树脂。聚碳酸酯树脂通过使用活化的碳酸二芳基酯的酯交换反应制备，使得聚碳酸酯容易形成内部酯键（IEL）。该方法发生，条件是选择聚碳酸酯树脂，成型条件或两者以控制在模制过程中形成的IEL的量至小于0.4mol％的水平。

5. 发明授权

US07498400B2 Method of preparing polycarbonate 有权
标题翻译：聚碳酸酯的制备方法
公开(公告)号：US07498400B2
公开(公告)日：2009-03-03
申请号：US11427885
申请日：2006-06-30
申请人： Bernd Jansen , Jan Henk Kamps , Edward Kung , Patrick Joseph McCloskey , Paul Michael Smigelski, Jr.
发明人： Bernd Jansen , Jan Henk Kamps , Edward Kung , Patrick Joseph McCloskey , Paul Michael Smigelski, Jr.
IPC分类号： C08G64/00 , C08G63/02
CPC分类号： C08G64/14 , C08G64/307
摘要： Polycarbonates incorporating terminal carbonate groups derived from ester-substituted activated carbonates in a transesterification process have unfavorable properties with respect to color, hydrolytic stability and thermal stability, particularly when the polycarbonate containing such end groups is molded. The number of activated carbonate end groups formed during the melt transesterification formation of polycarbonate can be reduced by reacting a dihydroxy compound with an activated diaryl carbonate in the presence of an esterification catalyst to produce a polycarbonate, in the presence of a monohydroxy chainstopper such as para-cumyl phenol in an amount that results in 35 to 65 mol % of the end groups being derived from the monohydroxy chainstopper. Suitably, the reactants are provided such that the molar ratio of activated diaryl carbonate to the total of dihydroxy compound plus ½ the chainstopping reagent that is less than 1.
摘要翻译：在酯交换方法中，衍生自酯取代的活性碳酸酯的末端碳酸酯基团的聚碳酸酯在颜色，水解稳定性和热稳定性方面具有不利的性质，特别是当含有这样的端基的聚碳酸酯被成型时。在聚碳酸酯的熔融酯交换形成期间形成的活化碳酸酯端基的数量可以通过在酯化催化剂的存在下使二羟基化合物与活化的碳酸二芳基酯反应来制备聚碳酸酯，在单羟基链断裂剂例如对 - 辛基苯酚，其量导致35-65mol％端基衍生自单羟基链断裂剂。适当地，提供反应物使得活化的碳酸二芳基酯与二羟基化合物的总和加上1/2的阻滞剂的摩尔比小于1。

6. 发明授权

US07759456B2 Branched polycarbonate resins and processes to prepare the same 失效
标题翻译：分支聚碳酸酯树脂及其制备方法
公开(公告)号：US07759456B2
公开(公告)日：2010-07-20
申请号：US11623847
申请日：2007-01-17
申请人： Hans-Peter Brack , Bernd Jansen , Jan Henk Kamps , Edward Kung , Jan Pleun Lens , Hans Looij , Han Vermeulen
发明人： Hans-Peter Brack , Bernd Jansen , Jan Henk Kamps , Edward Kung , Jan Pleun Lens , Hans Looij , Han Vermeulen
IPC分类号： C09J3/00 , C08G64/40 , C08G64/06 , C08G64/14
CPC分类号： C08G64/06 , C08G64/307
摘要： A method of increasing the branching and polydispersity of a polycarbonate includes the steps of: (a) including in the polycarbonate at least one species of an alkyl substituted monomer, and (b) treating the polycarbonate at an elevated temperature and for a sufficient time to increase the branching and polydispersity relative to an otherwise equivalent polycarbonate without alkyl substituents.
摘要翻译：增加聚碳酸酯的支化和多分散性的方法包括以下步骤：（a）在聚碳酸酯中包含至少一种烷基取代的单体，和（b）在高温下处理聚碳酸酯足够的时间，相对于没有烷基取代基的其他等效聚碳酸酯，增加支化和多分散性。

7. 发明授权

US07482423B2 Polycarbonates and method of preparing same 有权
标题翻译：聚碳酸酯及其制备方法
公开(公告)号：US07482423B2
公开(公告)日：2009-01-27
申请号：US11427861
申请日：2006-06-30
申请人： Bernd Jansen , Jan Henk Kamps , Edward Kung , Patrick Joseph McCloskey , Paul Michael Smigelski, Jr.
发明人： Bernd Jansen , Jan Henk Kamps , Edward Kung , Patrick Joseph McCloskey , Paul Michael Smigelski, Jr.
IPC分类号： C08G64/00 , C08G63/02
CPC分类号： C08G64/307 , C08G64/04
摘要： Polycarbonates incorporating terminal carbonate groups derived from ester-substituted activated carbonates, for example terminal methyl salicyl carbonate (TMSC) derived from the use of BMSC as the activated carbonate in a transesterification process, have unfavorable properties with respect to color, hydrolytic stability and thermal stability, particularly when the polycarbonate containing such end groups is molded. The number of activated carbonate end groups formed during the melt transesterification formation of polycarbonate can be reduced, however, without sacrificing the benefits of using an activated diaryl carbonate, and without requiring a separate reaction or additional additives by reacting a dihydroxy compound with an activated diaryl carbonate in the presence of an esterification catalyst to produce a polycarbonate, wherein the molar ratio of activated diaryl carbonate to dihydroxy compound is less than 1 when expressed to at least three decimal places, for example 0.996 or less.
摘要翻译：由酯取代的活性碳酸酯衍生的末端碳酸酯基团的聚碳酸酯，例如在酯交换法中使用BMSC作为活性碳酸酯的末端甲基水杨酸碳酸酯（TMSC）在颜色，水解稳定性和热稳定性方面具有不利的性质特别是当含有这种端基的聚碳酸酯被模制时。然而，在聚碳酸酯的熔融酯交换形成期间形成的活化碳酸酯端基的数量可以降低，但不会牺牲使用活性碳酸二芳基酯的优点，并且不需要单独的反应或另外的添加剂，通过使二羟基化合物与活化的二芳基在酯化催化剂存在下制备碳酸酯以制备聚碳酸酯，其中活化的碳酸二芳酯与二羟基化合物的摩尔比当表示至少三位小数，例如0.996或更小时小于1。

8. 发明申请

US20080004426A1 Branched Polycarbonate Resins and Processes to Prepare the Same 失效
标题翻译：支化聚碳酸酯树脂及其制备方法
公开(公告)号：US20080004426A1
公开(公告)日：2008-01-03
申请号：US11623847
申请日：2007-01-17
申请人： Hans-Peter Brack , Bernd Jansen , Jan Henk Kamps , Edward Kung , Jan Pleun Lens , Hans Looij , Han Vermeulen
发明人： Hans-Peter Brack , Bernd Jansen , Jan Henk Kamps , Edward Kung , Jan Pleun Lens , Hans Looij , Han Vermeulen
IPC分类号： C08J3/00 , C08F6/00 , C08G64/00 , C08L69/00
CPC分类号： C08G64/06 , C08G64/307
摘要： A method of increasing the branching and polydispersity of a polycarbonate includes the steps of: (a) including in the polycarbonate at least one species of an alkyl substituted monomer, and (b) treating the polycarbonate at an elevated temperature and for a sufficient time to increase the branching and polydispersity relative to an otherwise equivalent polycarbonate without alkyl substituents.
摘要翻译：增加聚碳酸酯的支化和多分散性的方法包括以下步骤：（a）在聚碳酸酯中包含至少一种烷基取代的单体，和（b）在高温下处理聚碳酸酯足够的时间，相对于没有烷基取代基的其他等效聚碳酸酯，增加支化和多分散性。

9. 发明申请

US20080004417A1 Polycarbonates and method of preparing same 有权
标题翻译：聚碳酸酯及其制备方法
公开(公告)号：US20080004417A1
公开(公告)日：2008-01-03
申请号：US11427861
申请日：2006-06-30
申请人： Bernd Jansen , Jan Henk Kamps , Edward Kung , Patrick Joseph McCloskey , Paul Michael Smigelski
发明人： Bernd Jansen , Jan Henk Kamps , Edward Kung , Patrick Joseph McCloskey , Paul Michael Smigelski
IPC分类号： C08G64/00
CPC分类号： C08G64/307 , C08G64/04
摘要： Polycarbonates incorporating terminal carbonate groups derived from ester-substituted activated carbonates, for example terminal methyl salicyl carbonate (TMSC) derived from the use of BMSC as the activated carbonate in a transesterification process, have unfavorable properties with respect to color, hydrolytic stability and thermal stability, particularly when the polycarbonate containing such end groups is molded. The number of activated carbonate end groups formed during the melt transesterification formation of polycarbonate can be reduced, however, without sacrificing the benefits of using an activated diaryl carbonate, and without requiring a separate reaction or additional additives by reacting a dihydroxy compound with an activated diaryl carbonate in the presence of an esterification catalyst to produce a polycarbonate, wherein the molar ratio of activated diaryl carbonate to dihydroxy compound is less than 1 when expressed to at least three decimal places, for example 0.996 or less.
摘要翻译：由酯取代的活性碳酸酯衍生的末端碳酸酯基团的聚碳酸酯，例如在酯交换法中使用BMSC作为活性碳酸酯的末端甲基水杨酸碳酸酯（TMSC）在颜色，水解稳定性和热稳定性方面具有不利的性质特别是当含有这种端基的聚碳酸酯被模制时。然而，在聚碳酸酯的熔融酯交换形成期间形成的活化碳酸酯端基的数量可以降低，但不会牺牲使用活性碳酸二芳基酯的优点，并且不需要单独的反应或另外的添加剂，通过使二羟基化合物与活化的二芳基在酯化催化剂存在下制备碳酸酯以制备聚碳酸酯，其中活化的碳酸二芳酯与二羟基化合物的摩尔比当表示至少三位小数，例如0.996或更小时小于1。

10. 发明授权

US5750221A Abrasion-resistant fluoropolymer mixtures 失效
公开(公告)号：US5750221A
公开(公告)日：1998-05-12
申请号：US824340
申请日：1997-03-26
申请人： Helmut Scheckenbach , Andreas Schleicher , Jurgen Kulpe , Wolfgang Neumann , Bernd Jansen
发明人： Helmut Scheckenbach , Andreas Schleicher , Jurgen Kulpe , Wolfgang Neumann , Bernd Jansen
IPC分类号： B29C47/00 , B29D23/00 , C08L27/12 , C08L81/06 , C08L87/00 , F16C1/26 , F16C33/20 , B29D22/00
CPC分类号： F16C33/201 , B29C47/0004 , C08L27/12 , F16C1/26 , B29C47/0023 , B29K2027/18 , C08L81/06 , Y10T428/13 , Y10T428/1352 , Y10T428/2929
摘要： An abrasion-resistant fluoropolymer mixture comprising (A) from 75 to 99% by weight of a fluorocarbon polymer (B) from 1 to 25% by weight of an oxidized polyarylene sulfide and, based on the sum (A)+(B), (C) from 0 to 15% by weight of a filler, is used for the production of feed pipes for Bowden cables which are pressure-resistant and abrasion-resistant.

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