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1. 发明申请

US20080154060A1 Processes for Producing Hydroxyalkyl (Meth) Acrylate 有权
标题翻译：生产羟烷基（甲基）丙烯酸酯的方法
公开(公告)号：US20080154060A1
公开(公告)日：2008-06-26
申请号：US11659370
申请日：2005-08-05
申请人： Tokumasa Ishida , Hiroyuki Takaki , Masahiro Uemura
发明人： Tokumasa Ishida , Hiroyuki Takaki , Masahiro Uemura
IPC分类号： C07C59/42
CPC分类号： C07C67/26 , C07C69/54
摘要： Processes for producing a hydroxyalkyl(meth)acrylate which comprise reacting (meth)acrylic acid with an alkylene oxide in the presence of a catalyst. A first process is characterized in that the amount of the acid ingredient is kept, on calculation, at 0.010 or more in terms of molar ratio to the catalyst present in the liquid reaction mixture and that the liquid reaction mixture from which the hydroxyalkyl(meth)acrylate has been distilled off is used in the subsequent reaction. A second process is characterized in that a dialkylene glycol mono(meth)acylate is supplied to the reaction system to cause the dialkyleneglycol mono(meth)acylate to coexist in the liquid reaction mixture.
摘要翻译：制备（甲基）丙烯酸羟烷基酯的方法，其包括在催化剂存在下使（甲基）丙烯酸与烯化氧反应。第一种方法的特征在于，根据计算，按照与液体反应混合物中存在的催化剂的摩尔比计算酸成分的量为0.010以上，并且其中（甲基）丙烯酸羟烷基酯的液体反应混合物，蒸馏出的丙烯酸酯用于随后的反应。第二种方法的特征在于向反应体系中加入单（甲基）丙烯酸二亚烷基二醇酯，以使液体反应混合物中的二烷基二醇单（甲基）酰化物共存。

2. 发明授权

US07214817B2 Hydroxyalkyl (meth)acrylate and its production process 有权
标题翻译：（甲基）丙烯酸羟烷基酯及其制备方法
公开(公告)号：US07214817B2
公开(公告)日：2007-05-08
申请号：US10436662
申请日：2003-05-13
申请人： Tokumasa Ishida , Hiroyuki Takaki , Masahiro Uemura
发明人： Tokumasa Ishida , Hiroyuki Takaki , Masahiro Uemura
IPC分类号： C07C67/26 , C07C69/73
CPC分类号： C07C67/26 , C07C69/54
摘要： The present invention provides: a high-quality hydroxyalkyl (meth)acrylate of which the alkylene glycol di(meth)acrylate content and the acid component content are both low; and its novel production process. The hydroxyalkyl (meth)acrylate, which has a content, in terms of an alkylene glycol di(meth)acrylate as an impurity, of not more than 0.1 weight % and an acid component content of not more than 0.1 weight %, is obtained by a process comprising the step of carrying out a batch reaction between (meth)acrylic acid and an alkylene oxide in the presence of a catalyst in order to produce the hydroxyalkyl (meth)acrylate; with the process making an adjustment as to charging of both raw materials in such a manner that, for, of a time as needed for supplying both raw materials, a supplying time of not less than 40% of a total supplying time when the raw materials as supplied have a temperature of not lower than 40° C., the molar ratio of the integrated amount of the alkylene oxide to the integrated amount of the (meth)acrylic acid that have been added to a reactor by then can be more than 1.0.
摘要翻译：本发明提供：其中亚烷基二醇二（甲基）丙烯酸酯含量和酸成分含量均低的（甲基）丙烯酸羟烷基酯; 及其新颖的生产工艺。通过以0.1重量％以下的亚烷基二醇二（甲基）丙烯酸酯作为杂质含量，酸成分含量为0.1重量％以下的（甲基）丙烯酸羟烷基酯，可以通过一种方法，包括在催化剂存在下进行（甲基）丙烯酸和烯化氧之间的间歇反应以制备（甲基）丙烯酸羟烷基酯的步骤; 该方法对两种原材料的充电进行调整，使得在供应两种原料的时间内，当原料的供应时间不少于总供应时间的40％时，如所供应的温度不低于40℃，那么环氧烷的一体化量与当时加入到反应器中的（甲基）丙烯酸的一体化量的摩尔比可以大于1.0 。

3. 发明授权

US06984751B2 Production process for hydroxyalkyl (meth) acrylate 失效
标题翻译：（甲基）丙烯酸羟烷基酯的制备方法
公开(公告)号：US06984751B2
公开(公告)日：2006-01-10
申请号：US10633139
申请日：2003-08-01
申请人： Hiroyuki Takaki , Tokumasa Ishida , Masahiro Uemura
发明人： Hiroyuki Takaki , Tokumasa Ishida , Masahiro Uemura
IPC分类号： C07C67/26
CPC分类号： C07C67/26 , C07C67/48 , C07C69/54
摘要： There is disclosed a novel production process for a hydroxyalkyl (meth)acrylate in which: the diffusion of harmful substances due to disposal of catalysts can be reduced; and also the amount of the catalyst as used can be greatly saved in the entire production process. This production process comprises the step of carrying out a reaction between (meth)acrylic acid and an alkylene oxide in the presence of a catalyst in order to produce the hydroxyalkyl (meth)acrylate; with the production process being characterized by further comprising the step of recovering the catalyst as has been used for the reaction.
摘要翻译：公开了一种新型的（甲基）丙烯酸羟烷基酯的制备方法，其中可以减少由于处理催化剂而引起的有害物质的扩散; 并且在整个生产过程中可以极大地节省所使用的催化剂的量。该制造方法包括在催化剂的存在下进行（甲基）丙烯酸与烯化氧的反应以制备（甲基）丙烯酸羟烷基酯的步骤; 其制备方法的特征在于还包括如已经用于反应的回收催化剂的步骤。

4. 发明授权

US08203018B2 Processes for producing hydroxyalkyl (meth) acrylate 有权
标题翻译：（甲基）丙烯酸羟烷基酯的制备方法
公开(公告)号：US08203018B2
公开(公告)日：2012-06-19
申请号：US11659370
申请日：2005-08-05
申请人： Tokumasa Ishida , Hiroyuki Takaki , Masahiro Uemura
发明人： Tokumasa Ishida , Hiroyuki Takaki , Masahiro Uemura
IPC分类号： C07C67/26 , C07C59/00
CPC分类号： C07C67/26 , C07C69/54
摘要： Processes for producing a hydroxyalkyl(meth)acrylate which comprise reacting (meth)acrylic acid with an alkylene oxide in the presence of a catalyst. A first process is characterized in that the amount of the acid ingredient is kept, on calculation, at 0.010 or more in terms of molar ratio to the catalyst present in the liquid reaction mixture and that the liquid reaction mixture from which the hydroxyalkyl(meth)acrylate has been distilled off is used in the subsequent reaction. A second process is characterized in that a dialkylene glycol mono(meth)acylate is supplied to the reaction system to cause the dialkyleneglycol mono(meth)acylate to coexist in the liquid reaction mixture.
摘要翻译：制备（甲基）丙烯酸羟烷基酯的方法，其包括在催化剂存在下使（甲基）丙烯酸与烯化氧反应。第一种方法的特征在于，根据计算，按照与液体反应混合物中存在的催化剂的摩尔比计算酸成分的量为0.010以上，并且其中（甲基）丙烯酸羟烷基酯的液体反应混合物，蒸馏出的丙烯酸酯用于随后的反应。第二种方法的特征在于向反应体系中加入单（甲基）丙烯酸二亚烷基二醇酯，以使液体反应混合物中的二烷基二醇单（甲基）酰化物共存。

5. 发明申请

US20140011959A1 N-PHENYLMALEIMIDE COMPOUND AND COPOLYMER COMPOSITION OBTAINED USING SAME 有权
标题翻译：使用其的N-苯基咪唑化合物和共聚物组合物
公开(公告)号：US20140011959A1
公开(公告)日：2014-01-09
申请号：US14006751
申请日：2012-03-19
申请人： Hiroyuki Takaki
发明人： Hiroyuki Takaki
IPC分类号： C08C19/28
CPC分类号： C08C19/28 , C07D207/448 , C08F222/40 , C08F236/12 , C08F279/02 , C08L55/02 , C08F212/08 , C08F220/44
摘要： The present invention provides an N-phenylmaleimide compound that can improve the quality of the obtained copolymer by using N-phenylmaleimide containing impurities in specific amounts or less as at least one component of the copolymerization monomers. The N-phenylmaleimide compound of the present invention contains 0.1% by weight or less of N-(2,5-dioxo-1-phenyl-3-pyrrolidinyl)-N-phenylmaleamic acid (PPMA) and/or 0.3% by weight or less of N-phenylfumaramic acid (PFA).
摘要翻译：本发明提供一种N-苯基马来酰亚胺化合物，其可以通过使用含有特定量以上的杂质的N-苯基马来酰亚胺作为共聚单体的至少一种成分来提高所得共聚物的质量。本发明的N-苯基马来酰亚胺化合物含有0.1重量％以下的N-（2,5-二氧代-1-苯基-3-吡咯烷基）-N-苯基马来酸（PPMA）和/或0.3重量％较少的N-苯基呋喃甲酸（PFA）。

6. 发明授权

US09631033B2 N-phenylmaleimide compound and copolymer composition obtained using same 有权
公开(公告)号：US09631033B2
公开(公告)日：2017-04-25
申请号：US14006751
申请日：2012-03-19
申请人： Hiroyuki Takaki
发明人： Hiroyuki Takaki
IPC分类号： C08L55/02 , C08C19/28 , C07D207/448 , C08F236/12 , C08F222/40 , C08F279/02
CPC分类号： C08C19/28 , C07D207/448 , C08F222/40 , C08F236/12 , C08F279/02 , C08L55/02 , C08F212/08 , C08F220/44
摘要： The present invention provides an N-phenylmaleimide compound that can improve the quality of the obtained copolymer by using N-phenylmaleimide containing impurities in specific amounts or less as at least one component of the copolymerization monomers. The N-phenylmaleimide compound of the present invention contains 0.1% by weight or less of N-(2,5-dioxo-1-phenyl-3-pyrrolidinyl)-N-phenylmaleamic acid (PPMA) and/or 0.3% by weight or less of N-phenylfumaramic acid (PFA).

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