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1. 发明申请

US20050215736A1 Olefin polymerization catalyst and olefin polymerization method using the same 失效
公开(公告)号：US20050215736A1
公开(公告)日：2005-09-29
申请号：US10998837
申请日：2004-11-30
申请人： Toshifumi Takemori , Minoru Iijima , Yoshihisa Hayashida , Masashi Iida
发明人： Toshifumi Takemori , Minoru Iijima , Yoshihisa Hayashida , Masashi Iida
IPC分类号： C08F4/02 , C08F4/658 , C08F4/659 , C08F4/6592 , C08F110/02 , C08F210/02 , C08F210/16 , C08F4/44 , B01J31/00
CPC分类号： C08F210/02 , C08F4/65916 , C08F4/65925 , C08F4/65927 , C08F110/02 , C08F210/16 , C08F4/65922 , C08F4/65912 , C08F2500/18 , C08F2500/24 , C08F2500/03 , C08F210/14
摘要： An olefin polymerization solid catalyst which comprises having a reaction product of (C) a transition metal compound of the following formula (1) or (2) and (D) an organoaluminum compound carried on a support having (A) silica treated with (B) an organoaluminum-oxy compound; (R1aCp)m(R2bCp)nM-(-X-Ar-Yc)4-(m+n) (1) wherein M is titanium, zirconium or hafnium, Cp is a group having a cyclopentadienyl structure, R1 and R2 are a hydrogen atom, an alkyl group, an alkenyl group, an aryl group, an alkylaryl group, an arylalkyl group or an alkylsilyl group, X is an oxygen atom or a sulfur atom, Ar is an aromatic ring, Y may be the same or different and is a hydrogen atom or a substituent selected from the group consisting of a hydrocarbon group, an alkylsilyl group, a halogen atom, a halogenated hydrocarbon group, a nitrogen-containing organic group, an oxygen-containing organic group or a sulfur-containing organic group, a and b are an integer of from 0 to 5, m and n are an integer of from 0 to 3, m+n is an integer of from 1 to 3, and c is an integer of from 1 to 5, provided that Y is not hydrogen when Ar is a benzene ring, R3(R1dCp)(R2eCp)M-(-X-Ar-Yc)2 (2) wherein M is titanium, zirconium or hafnium, Cp is a group having a cyclopentadienyl structure, R1 and R2 are a hydrogen atom, an alkyl group, an alkenyl group, an aryl group, an alkylaryl group, an arylalkyl group or an alkylsilyl group, R3 is a divalent group selected from the group consisting of an alkylene group, an arylalkylene group, a dialkylsilylene group, a dialkylgermylene group, an alkylphosphinediyl group or an alkylimino group, which crosslinks (R1dCp) and (R2eCp), X is an oxygen atom or a sulfur atom, Ar is an aromatic ring, Y may be the same or different and is a hydrogen atom or a substituent selected from the group consisting of a hydrocarbon group, an alkylsilyl group, a halogen atom, a halogenated hydrocarbon group, a nitrogen-containing organic group, an oxygen-containing organic group and a sulfur-containing organic group, d and e are an integer of from 0 to 4, and c is an integer of from 1 to 5, provided that Y is not hydrogen when Ar is a benzene ring.

2. 发明授权

US06787616B2 Catalyst for olefin polymerization and process for polymerizing olefin by means thereof 失效
公开(公告)号：US06787616B2
公开(公告)日：2004-09-07
申请号：US10463698
申请日：2003-06-18
申请人： Toshifumi Takemori , Masashi Iida , Minoru Iijima , Yoshihisa Hayashida , Masao Kawahara
发明人： Toshifumi Takemori , Masashi Iida , Minoru Iijima , Yoshihisa Hayashida , Masao Kawahara
IPC分类号： C08F4608
CPC分类号： C08F10/02 , C08F4/65912 , C08F4/65922 , C08F110/02 , C08F210/16 , Y10S526/943 , C08F4/65916 , C08F2500/03 , C08F2500/18 , C08F2500/24 , C08F210/14
摘要： A solid catalyst for olefin polymerization, which comprises a silica carrier (A) having a specific surface area of from 600 to 850 m2/g, a pore volume of from 0.1 to 0.8 ml/g and an average particle size of from 2 to 12 &mgr;m, and an organoaluminum-oxy compound (B) and a Group IVB transition metal compound (C) containing a ligand having a cyclopentadienyl skeleton, supported on the carrier (A).

3. 发明授权

US07345119B2 Olefin polymerization catalyst and olefin polymerization method using the same 失效
标题翻译：烯烃聚合催化剂和烯烃聚合方法使用相同
公开(公告)号：US07345119B2
公开(公告)日：2008-03-18
申请号：US10998837
申请日：2004-11-30
申请人： Toshifumi Takemori , Minoru Iijima , Yoshihisa Hayashida , Masashi Iida
发明人： Toshifumi Takemori , Minoru Iijima , Yoshihisa Hayashida , Masashi Iida
IPC分类号： C08F4/02 , C08F4/6392 , C08F110/02 , C08F4/64
CPC分类号： C08F210/02 , C08F4/65916 , C08F4/65925 , C08F4/65927 , C08F110/02 , C08F210/16 , C08F4/65922 , C08F4/65912 , C08F2500/18 , C08F2500/24 , C08F2500/03 , C08F210/14
摘要： An olefin polymerization solid catalyst including a reaction product of a transition metal compound and an organoaluminum compound carried on a support having silica treated with an organoaluminum-oxy compound.
摘要翻译：一种烯烃聚合固体催化剂，其包括过渡金属化合物和有机铝化合物的反应产物，该反应产物承载在具有用有机铝 - 氧化合物处理的二氧化硅的载体上。

4. 发明授权

US06455647B1 Solid catalyst for olefin polymerization and process for producing olefin polymer with the same 失效
标题翻译：用于烯烃聚合的固体催化剂和用于制备烯烃聚合物的方法
公开(公告)号：US06455647B1
公开(公告)日：2002-09-24
申请号：US09581042
申请日：2000-06-08
申请人： Sakae Kamiyama , Toshifumi Takemori , Minoru Iijima , Yukiko Hane , Shigeharu Yamamoto
发明人： Sakae Kamiyama , Toshifumi Takemori , Minoru Iijima , Yukiko Hane , Shigeharu Yamamoto
IPC分类号： C08F442
CPC分类号： C08F10/00 , C08F4/65912 , C08F4/65925 , Y10S526/943 , C08F4/65916 , C08F210/16 , C08F210/14 , C08F2500/03
摘要： The present invention relates to a solid catalyst (D) for olefin polymerization comprising a magnesium-containing solid component (A) carrying thereon an organoaluminum-oxy compound (B) and a metallocene compound (C), the magnesium-containing compound (A) being obtained by heat treating a magnesium compound represented by the general formula: MgX2.nH2O where X represents a halogen atom and n is an integer of 1 to 12, and to a method of producing an olefinic polymer using the catalyst. In the case where the above solid catalyst for olefin polymerization is used, catalyst activity, particularly activity per solid catalyst, is high. Therefore, a deashing treatment step such as catalyst removal can be omitted. Further, the olefinic polymer produced has a narrow molecular weight distribution, and in the case of a copolymer, its monomer composition is uniform.
摘要翻译：本发明涉及一种用于烯烃聚合的固体催化剂（D），其包含含有有机铝 - 氧化合物（B）和茂金属化合物（C）的含镁固体组分（A），含镁化合物（A）通过热处理由通式MgX 2·nH 2 O表示的镁化合物得到，其中X表示卤素原子，n表示1〜12的整数，以及使用该催化剂制造烯烃类聚合物的方法。在使用上述用于烯烃聚合的固体催化剂的情况下，催化剂活性，特别是每固体催化剂的活性高。因此，可以省略诸如催化剂去除的脱气处理步骤。此外，所生产的烯烃聚合物具有窄的分子量分布，在共聚物的情况下，其单体组成是均匀的。

5. 发明授权

US06368995B1 Solid catalysts for the polymerization of olefins and process for the production of olefin polymers therewith 失效
标题翻译：用于烯烃聚合的固体催化剂和用于生产烯烃聚合物的方法
公开(公告)号：US06368995B1
公开(公告)日：2002-04-09
申请号：US09530264
申请日：2000-06-08
申请人： Sakae Kamiyama , Toshifumi Takemori , Minoru Iijima , Yukiko Hane , Shigeharu Yamamoto
发明人： Sakae Kamiyama , Toshifumi Takemori , Minoru Iijima , Yukiko Hane , Shigeharu Yamamoto
IPC分类号： B01J3122
CPC分类号： C08F10/00 , C08F4/65912 , C08F4/65922 , C08F10/02 , C08F110/02 , C08F210/16 , C08F4/02 , C08F4/65916 , C08F4/61912 , C08F4/61916 , C08F2500/18 , C08F2500/24 , C08F2500/03 , C08F210/14
摘要： A solid catalyst for olefin polymerization, obtained by reacting a least one of a hydropolysiloxane compound, having the formula R1aHbSiO(4−a−b)/2, a silane compound of formula R2cSi(OH)4−c, and condensates of the silane, with a compound of formula (MgR32)p.(R3MgX)q to form a reaction product. The reaction product is reacted with an alcohol, having 1 to 4 carbon atoms, to obtain an intermediate product. The intermediate product, is then reacted with water to obtain reaction product. An organoaluminum oxy compound and a metallocene compound are carried on the solid reaction product. The solid catalyst may be used for olefin polymerization. The catalyst requires no deashing treatment and produces a polymer having high bulk density and narrow particle size distribution. Thus the solid catalystenables control of particle size of the polymer in a simple easy manner, and shows no adhesion of polymer onto the inner wall of autoclave.
摘要翻译：一种用于烯烃聚合的固体催化剂，其通过使具有式R1aHbSiO（4-ab）/ 2的氢化聚硅氧烷化合物，式R 2 c Si（OH）4-c的硅烷化合物和硅烷的缩合物中的至少一种与硅烷的缩合物与式（MgR32）p。（R3MgX）q的化合物以形成反应产物。使反应产物与具有1至4个碳原子的醇反应以获得中间产物。然后将中间产物与水反应以获得反应产物。有机铝氧化合物和茂金属化合物载于固体反应产物上。固体催化剂可用于烯烃聚合。该催化剂不需要脱屑处理，并且产生具有高堆积密度和窄粒度分布的聚合物。因此，固体催化剂以简单的方式控制聚合物的粒度，并且不显示聚合物对高压釜的内壁的粘附。

6. 发明授权

US08709698B2 Copolymer for positive type lithography, polymerization initiator used in production of said copolymer, and composition for semiconductor lithography 有权
标题翻译：用于正型光刻的共聚物，用于制备所述共聚物的聚合引发剂和用于半导体光刻的组合物
公开(公告)号：US08709698B2
公开(公告)日：2014-04-29
申请号：US13199907
申请日：2011-09-12
申请人： Minoru Iijima , Takanori Yamagishi
发明人： Minoru Iijima , Takanori Yamagishi
IPC分类号： G03F7/00 , C09B31/16
CPC分类号： G03F7/0397 , C08F220/28
摘要： A radical polymerization initiator represented by the following formula (G) in the formula (G), R71 and R72 are each a hydrocarbon group of 3 to 6 carbon atoms which may contain nitrogen atom; R73 and R74 are each a hydrogen atom or an acid-dissociating, dissolution-suppressing group; and at least one of R73 and R74 is an acid-dissociating, dissolution-suppressing group represented by the following formula (R78); and wherein R77 is a hydrocarbon group of 1 to 26 carbon atoms which may contain hetero atoms.
摘要翻译：由式（G）中的下式（G）表示的自由基聚合引发剂R71和R72各自为可含有氮原子的3〜6个碳原子的烃基; R73和R74各自为氢原子或酸解离溶解抑制基团; R73和R74中的至少一个为下式（R78）表示的酸解离溶解抑制基团。并且其中R 77是可含有杂原子的1至26个碳原子的烃基。

7. 发明申请

US20070269741A1 Copolymer for positive type lithography, polymerization initiator used in production of said copolymer, and composition for semiconductor lithography 有权
标题翻译：用于正型光刻的共聚物，用于制备所述共聚物的聚合引发剂和用于半导体光刻的组合物
公开(公告)号：US20070269741A1
公开(公告)日：2007-11-22
申请号：US11800295
申请日：2007-05-04
申请人： Minoru Iijima , Takanori Yamagishi
发明人： Minoru Iijima , Takanori Yamagishi
IPC分类号： G03C1/00
CPC分类号： G03F7/0397 , C08F220/28
摘要： A copolymer for positive type lithography, having at least a recurring unit (A) having a structure wherein an alkali-soluble group is protected by an acid-dissociating, dissolution-suppressing group, represented by the following formula (A) [in the formula (A), R10 is a hydrogen atom or a hydrocarbon group which may be substituted by fluorine atom; R11 is a crosslinked, alicyclic hydrocarbon group; n is an integer of 0 or 1; and R12 is an acid-dissociating, dissolution-suppressing group], and a terminal structure (B) having a structure wherein an alkali-soluble group is protected by an acid-dissociating, dissolution-suppressing group, represented by the following formula (B) [in the formula (B), R21 is a hydrocarbon group which may contain nitrogen atom; R22 is an acid-dissociating, dissolution-suppressing group; and p is a site of bonding with copolymer main chain].The copolymer is used in chemically amplified positive type lithography and is superior in lithography properties (e.g. dissolution contrast).
摘要翻译：一种正型平版印刷用共聚物，其至少具有具有下式（A）表示的酸溶解抑制基团的碱溶性基团保护的结构的重复单元（A）[式（A）中，R 10是氢原子或可被氟原子取代的烃基; R 11是交联的脂环族烃基; n为0或1的整数; 并且R 12是酸解离的溶解抑制基团]和具有其中碱溶性基团被酸解离的溶解抑制基团保护的结构的末端结构（B）由下式（B）表示[式（B）中，R 21是可以含有氮原子的烃基， R 22是酸解离的溶解抑制基团; 和p是与共聚物主链键合的位点]。该共聚物用于化学放大正型光刻中，并且在光刻性能（例如溶出对比度）方面是优异的。

8. 发明授权

US5557189A Method and apparatus including a current detector and a power source control circuit for charging a number of batteries 失效
标题翻译：包括用于对多个电池充电的电流检测器和电源控制电路的方法和装置
公开(公告)号：US5557189A
公开(公告)日：1996-09-17
申请号：US352618
申请日：1994-12-09
申请人： Mamoru Suzuki , Minoru Iijima , Yasuyuki Ishihama , Nobuhiro Fujiwara
发明人： Mamoru Suzuki , Minoru Iijima , Yasuyuki Ishihama , Nobuhiro Fujiwara
IPC分类号： H02J7/10 , H01M10/42 , H01M10/44 , H01M10/48 , H02J7/00 , H01M10/46
CPC分类号： H01M10/44 , H02J7/0016 , Y10S320/22
摘要： A battery charging apparatus for charging the electricity from a current source to a cell includes a variable resistor in parallel with the cell, a cell voltage detection unit for detecting the current voltage value of the cell and a comparator for comparing the current voltage value to a pre-set voltage value. The resistance value of the variable resistor is controlled responsive to the results of comparison so that the current from the current source is caused to flow through both the cell and the variable resistor with progress in the charging of the cell. The current is prevented from flowing through the cell when the cell is fully charged, so that overcharging is eliminated. If plural cells are charged in series, the control operation of not causing the current to flow through the fully charged cell can be carried out for each of the cells, so that integrated charging may be continued until all of the cells are fully charged thus shortening the cell charging time.
摘要翻译：用于从电流源向电池充电的电池充电装置包括与电池并联的可变电阻器，用于检测电池的当前电压值的电池电压检测单元和用于将电流电压值与预设电压值。响应于比较结果控制可变电阻器的电阻值，使得来自电流源的电流通过电池充电的进行而流过电池和可变电阻器。当电池完全充电时，防止电流流过电池，从而消除过充电。如果多个电池串联充电，则可以对每个电池进行不使电流流过充满电的电池的控制操作，使得可以继续进行集成充电直到所有电池充满电从而缩短电池充电时间。

9. 发明授权

US08067516B2 Copolymer for positive type lithography, polymerization initiator used in production of said copolymer, and composition for semiconductor lithography 有权
标题翻译：用于正型光刻的共聚物，用于制备所述共聚物的聚合引发剂和用于半导体光刻的组合物
公开(公告)号：US08067516B2
公开(公告)日：2011-11-29
申请号：US11800295
申请日：2007-05-04
申请人： Minoru Iijima , Takanori Yamagishi
发明人： Minoru Iijima , Takanori Yamagishi
IPC分类号： C08F18/02
CPC分类号： G03F7/0397 , C08F220/28
摘要： A copolymer for positive type lithography, having at least a recurring unit (A) having a structure wherein an alkali-soluble group is protected by an acid-dissociating, dissolution-suppressing group, represented by the following formula (A) [in the formula (A), R10 is a hydrogen atom or a hydrocarbon group which may be substituted by fluorine atom; R11 is a crosslinked, alicyclic hydrocarbon group; n is an integer of 0 or 1; and R12 is an acid-dissociating, dissolution-suppressing group], and a terminal structure (B) having a structure wherein an alkali-soluble group is protected by an acid-dissociating, dissolution-suppressing group, represented by the following formula (B) [in the formula (B), R21 is a hydrocarbon group which may contain nitrogen atom; R22 is an acid-dissociating, dissolution-suppressing group; and p is a site of bonding with copolymer main chain]. The copolymer is used in chemically amplified positive type lithography and is superior in lithography properties (e.g. dissolution contrast).
摘要翻译：一种正型平版印刷用共聚物，其至少具有具有下式（A）表示的酸溶解抑制基团的碱溶性基团保护的结构的重复单元（A）[式（A）中，R 10为氢原子或可被氟原子取代的烃基; R11是交联的脂环烃基; n为0或1的整数; 和R 12是酸解离的溶解抑制基团]和具有下式（B）表示的具有酸解离溶解抑制基团的碱溶性基团保护的结构的末端结构（B））[式（B）中，R 21表示可以含有氮原子的烃基， R22是酸解离，溶解抑制基团; 和p是与共聚物主链键合的位点]。该共聚物用于化学放大正型光刻中，并且在光刻性能（例如溶出对比度）方面是优异的。

10. 发明申请

US20120071638A1 Copolymer for positive type lithography, polymerization initiator used in production of said copolymer, and composition for semiconductor lithography 有权
标题翻译：用于正型光刻的共聚物，用于制备所述共聚物的聚合引发剂和用于半导体光刻的组合物
公开(公告)号：US20120071638A1
公开(公告)日：2012-03-22
申请号：US13199907
申请日：2011-09-12
申请人： Minoru Iijima , Takanori Yamagishi
发明人： Minoru Iijima , Takanori Yamagishi
IPC分类号： C07C245/04
CPC分类号： G03F7/0397 , C08F220/28
摘要： A copolymer for positive type lithography, having at least a recurring unit (A) having a structure wherein an alkali-soluble group is protected by an acid-dissociating, dissolution-suppressing group, represented by the following formula (A) [in the formula (A), R10 is a hydrogen atom or a hydrocarbon group which may be substituted by fluorine atom; R11 is a crosslinked, alicyclic hydrocarbon group; n is an integer of 0 or 1; and R12 is an acid-dissociating, dissolution-suppressing group], and a terminal structure (B) having a structure wherein an alkali-soluble group is protected by an acid-dissociating, dissolution-suppressing group, represented by the following formula (B) [in the formula (B), R21 is a hydrocarbon group which may contain nitrogen atom; R22 is an acid-dissociating, dissolution-suppressing group; and p is a site of bonding with copolymer main chain].
摘要翻译：一种正型平版印刷用共聚物，其至少具有具有下式（A）表示的酸溶解抑制基团的碱溶性基团保护的结构的重复单元（A）[式（A）中，R 10为氢原子或可被氟原子取代的烃基; R11是交联的脂环烃基; n为0或1的整数; 和R 12是酸解离的溶解抑制基团]和具有下式（B）表示的具有酸解离溶解抑制基团的碱溶性基团保护的结构的末端结构（B））[式（B）中，R 21表示可以含有氮原子的烃基， R22是酸解离，溶解抑制基团; 和p是与共聚物主链键合的位点]。

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