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1. 发明公开

US20240092649A1 SYSTEMS AND METHODS FOR SOLID-PHASE REACTIONS 审中-公开
公开(公告)号：US20240092649A1
公开(公告)日：2024-03-21
申请号：US18463992
申请日：2023-09-08
申请人： Phoenix Tailings, Inc.
发明人： Thomas Anthony Villalon, Jr. , Henry Chase Hutcheson
IPC分类号： C01G1/06 , B01J8/18 , C01G3/05 , C01G9/04 , C01G49/10
CPC分类号： C01G1/06 , B01J8/18 , C01G3/05 , C01G9/04 , C01G49/10
摘要： The present disclosure is related to systems and methods for solid-phase reactions.

2. 发明申请

US20170361377A1 Neutralization of Reactive Metal Condensate in Additive Manufacturing 审中-公开
公开(公告)号：US20170361377A1
公开(公告)日：2017-12-21
申请号：US15532273
申请日：2015-12-02
申请人： Moog Inc.
发明人： Paul Guerrier , Ian L. Brooks
IPC分类号： B22F3/105 , B33Y40/00 , B33Y10/00 , B33Y30/00 , C01G23/02
CPC分类号： B22F3/1055 , B22F2003/1056 , B22F2003/1059 , B33Y10/00 , B33Y30/00 , B33Y40/00 , C01G1/06 , C01G23/02 , Y02P10/295
摘要： An additive manufacturing system with a build chamber has a halide vessel that generates a halide gas and a dissociation chamber with a filament. Metal condensate is contacted with the halide gas to form a gaseous metal halide compound. The gaseous metal halide compound is decomposed to deposit metal on the filament. In an example, titanium reacts with gaseous iodine to form gaseous titanium tetraiodide.

3. 发明申请

US20140050653A1 Process for Producing Fluorine-Containing Combined Salt 有权
标题翻译：生产含氟组合盐的方法
公开(公告)号：US20140050653A1
公开(公告)日：2014-02-20
申请号：US14113156
申请日：2012-04-11
申请人： Tetsuya Tamura
发明人： Tetsuya Tamura
IPC分类号： C01D15/04 , C01D3/02 , C01F11/22
CPC分类号： C01D15/04 , C01B9/08 , C01D3/02 , C01F11/00 , C01F11/22 , C01G1/06 , C01G23/002 , C01G49/009 , C01P2004/03 , C01P2004/52
摘要： Disclosed is a process for producing a fluorine-containing complex salt, characterized by that, on a reaction mother liquor containing a plurality of cation species and a fluoroanion in a state that they have been dissolved in a solvent, a trigger for accelerating decomposition of the fluoroanion is allowed to act, thereby precipitating a complex salt containing a plurality of cation species and fluorine, as a solid, from the reaction mother liquor. According to this process, it is possible to produce a monodispersed fluorine-containing complex salt with uniform particle size and shape.
摘要翻译：公开了一种制备含氟络盐的方法，其特征在于，在溶解有溶剂的状态下，在含有多种阳离子物质和氟代阴离子的反应母液中，加速分解的触发剂使氟代阴离子起作用，由此从反应母液中析出含有多个阳离子种类的络合盐和作为固体的氟。根据该方法，可以制造均匀的粒径和形状的单分散的含氟络合盐。

4. 发明申请

US20100258479A1 THERMAL DISSOLUTION CATALYSIS METHOD FOR PREPARING LIQUID FUEL FROM LIGNITE AND THE CATALYST AND THE SOLVENT SUITABLE FOR THE METHOD 审中-公开
标题翻译：用于从Lignite和催化剂制备液体燃料的热解决方案和适用于该方法的溶剂
公开(公告)号：US20100258479A1
公开(公告)日：2010-10-14
申请号：US12746583
申请日：2008-12-10
申请人： Ke Wu , Chong Chen , Wenyi Huang , Pai Peng , Chunlai Wu
发明人： Ke Wu , Chong Chen , Wenyi Huang , Pai Peng , Chunlai Wu
IPC分类号： C10G1/00 , C10G1/06 , B01J31/12 , B01F1/00
CPC分类号： C01G1/06 , B01J31/146 , B01J31/1805 , B01J31/2213 , B01J2531/37 , B01J2531/64 , B01J2531/842 , B01J2531/845 , C01G29/00 , C01G39/00 , C01G49/00 , C01G51/00
摘要： The present invention relates to coal chemical processing, and particularly to a thermal dissolution catalysis method for preparing liquid fuel from lignite. The method comprises steps of: 1) crushing and drying lignite into coal powder; 2) stirring and mixing coal powder, a solvent and a catalyst sufficiently to form coal slurry, wherein there are 30-40% mass of coal powder, 60-70% mass of solvent, and 0.5-1% mass of catalyst relative to coal powder mass; 3) subjecting the coal slurry to thermal dissolution catalysis reaction to obtain thermal dissolution liquefied product, wherein the reaction is carried out for 30-60 minutes at a temperature 390-450° C. under a pressure 5.0-9.0 MPa; 4) separating the thermal dissolution liquefied product into gas, liquid and solid phases; and 5) upgrading the liquid product into liquid fuel. The present invention further discloses a catalyst and a solvent for use in the above method. The method according to the present invention requires moderate operation conditions and can enable organic matter in the lignite to convert at a relatively high level, the liquid fuel product, after being processed, can be used to prepare engine fuel meeting a national standard; the method requires a simple preparation apparatus, a small investment and a low cost and is a coal liquefying method meeting China's status quo.
摘要翻译：本发明涉及煤化学处理，特别涉及从褐煤制备液体燃料的热溶解催化方法。该方法包括以下步骤：1）将褐煤粉碎和干燥成粉煤灰; 2）充分搅拌和搅拌煤粉，溶剂和催化剂，形成煤浆，其中煤粉含量为30-40％，溶剂质量为60-70％，催化剂质量相对于煤为0.5-1％粉末质量 3）对煤浆进行热溶解催化反应，得到热溶液化产物，其中在温度390-450℃，压力5.0-9.0MPa下反应30-60分钟; 4）将热溶解液化产物分离成气相，液相和固相; 和5）将液体产品升级成液体燃料。本发明还公开了用于上述方法的催化剂和溶剂。根据本发明的方法需要适度的操作条件，并且能够使褐煤中的有机物质以较高的水平转化，液态燃料产品经处理后可用于制备符合国家标准的发动机燃料; 该方法需要一个简单的准备装置，投资少，成本低，是符合中国现状的煤液化方法。

5. 发明授权

US07708968B2 Nano-scale metal oxide, oxyhalide and oxysulfide scintillation materials and methods for making same 失效
标题翻译：纳米级金属氧化物，卤氧化物和氧硫化物闪烁材料及其制备方法
公开(公告)号：US07708968B2
公开(公告)日：2010-05-04
申请号：US11728445
申请日：2007-03-26
申请人： Brent Allen Clothier , Sergio Paulo Martins Loureiro , Alok Srivastava , Stanley John Stoklosa , Steven Jude Duclos , Venkat Subramaniam Venkataramani
发明人： Brent Allen Clothier , Sergio Paulo Martins Loureiro , Alok Srivastava , Stanley John Stoklosa , Steven Jude Duclos , Venkat Subramaniam Venkataramani
IPC分类号： C01F17/00 , C01B13/00 , C01G41/02 , C01G9/02 , C01G29/00 , C01G30/00
CPC分类号： C01G1/06 , B82Y30/00 , C01B13/328 , C01F17/0043 , C01F17/0056 , C01F17/0093 , C01G1/12 , C01P2002/54 , C01P2004/64
摘要： Crystalline scintillator materials comprising nano-scale particles of metal oxides, metal oxyhalides and metal oxysulfides are provided. The nano-scale particles are less than 100 nm in size. Methods are provided for preparing the particles. In one method, used to form oxyhalides and oxysulfides, metal salts are dissolved in water, and then precipitated out as fine particles using an aqueous base. After the particles are separated from the solution, they are annealed under a flow of a water saturated hydrogen anion gas, such as HCl or H2S, to form the crystalline scintillator particles. The other methods take advantage of the characteristics of microemulsion solutions to control droplet size, and, thus, the particle size of the final nano-particles. For example, in one method, a first micro-emulsion containing metal salts if formed. The first micro-emulsion is mixed with an aqueous base in a second micro-emulsion to form the final nano-scale particles.
摘要翻译：提供了包含金属氧化物，金属卤氧化物和金属氧硫化物的纳米级颗粒的结晶闪烁体材料。纳米级颗粒的尺寸小于100nm。提供了制备颗粒的方法。在一种用于形成卤氧化物和氧硫化物的方法中，将金属盐溶解在水中，然后使用碱水溶液作为细颗粒沉淀出来。在将颗粒从溶液中分离出来之后，在水饱和氢阴离子气体如HCl或H 2 S的流动下进行退火以形成晶体闪烁体颗粒。其他方法利用微乳液溶液的特性来控制液滴尺寸，从而控制最终纳米颗粒的粒度。例如，在一种方法中，如果形成含有金属盐的第一微乳液。将第一微乳液与第二微乳液中的水性碱混合以形成最终的纳米尺度颗粒。

6. 发明申请

US20100035155A1 CATHODE ACTIVE MATERIAL FOR NON-AQUEOUS ELECTROLYTE SECONDARY BATTERY AND MANUFACTURING METHOD OF THE SAME 有权
标题翻译：非水电解二次电池用阴极活性材料及其制造方法
公开(公告)号：US20100035155A1
公开(公告)日：2010-02-11
申请号：US12515212
申请日：2007-11-16
申请人： Shigeto Okada , Manabu Nishijima , Takayuki Doi , Jun-ichi Yamaki , Irina D. Gocheva , Toshiyasu Kiyabu
发明人： Shigeto Okada , Manabu Nishijima , Takayuki Doi , Jun-ichi Yamaki , Irina D. Gocheva , Toshiyasu Kiyabu
IPC分类号： H01M4/58 , H01B1/02
CPC分类号： H01M10/0562 , C01G1/06 , C01P2006/40 , H01M4/13 , H01M4/582 , H01M4/626 , H01M10/0525 , Y02T10/7011
摘要： In a non-aqueous electrolyte secondary battery, in order to adjust a cathode active material in which guest cation such as Na and Li is included, alkaline metal fluoride which is expressed by a general formula AF and transition metal fluoride which is expressed by a formula M′ F2 are subjected to a mechanical milling process to produce metal fluoride compound AM′ F3. The mechanical milling process desirably uses a planetary ball mill.
摘要翻译：在非水电解质二次电池中，为了调整包含Na和Li等客体阳离子的正极活性物质，由通式AF表示的碱金属氟化物和由式对M'F2进行机械研磨处理以产生金属氟化物化合物AM'F3。机械铣削加工优选使用行星式球磨机。

7. 发明申请

US20080105536A1 Method For Producing Elemental Halides 审中-公开
标题翻译：生产元素卤化物的方法
公开(公告)号：US20080105536A1
公开(公告)日：2008-05-08
申请号：US11719043
申请日：2005-11-10
申请人： Norbert Auner
发明人： Norbert Auner
IPC分类号： C01B7/00 , C01B33/00
CPC分类号： C01B33/107 , B01J19/126 , B01J2219/0875 , B01J2219/0877 , B01J2219/0879 , B01J2219/0892 , C01B9/00 , C01B9/02 , C01B9/04 , C01B9/06 , C01B9/08 , C01F7/48 , C01F7/60 , C01G1/06 , C01G9/04 , C01G11/00 , C01G19/04 , C01G23/02 , C01G23/022 , C01G27/04 , C01G28/007 , C01G49/10
摘要： Element halides are prepared in high yield by contacting an element or compound thereof and carbon or a carbon source with a gas stream containing a halogen or halogen compound in the gaseous state, and heating by means of an alternating magnetic field.
摘要翻译：通过使元素或其化合物和碳或碳源与气态的含有卤素或卤素化合物的气流接触，并通过交变磁场进行加热，以高产率制备元素卤化物。

8. 发明申请

US20040234446A1 Process for the production of metal fluoride materials 审中-公开
标题翻译：金属氟化物材料生产工艺
公开(公告)号：US20040234446A1
公开(公告)日：2004-11-25
申请号：US10662992
申请日：2003-09-15
申请人： Platinum Research Organization Ltd.
发明人： F. Conrad Greer , Ronald L. Elsenbaumer , David P. Owen
IPC分类号： C01B009/08
CPC分类号： B01J35/0013 , B01J27/12 , C01B7/035 , C01B9/08 , C01G1/06 , C01G49/10
摘要： A process for the production of metal fluorides comprising introducing a predetermined weight of anhydrous hydrofluoric acid into a reaction vessel and initiate a mixing action, preheating a predetermined weight of anhydrous metal to a predetermined reaction temperature, introducing aliquots of the anhydrous metal into the reaction vessel at intervals until the entire predetermined weight of the anhydrous metal has been added, removing excess anhydrous hydrofluoric acid from the reaction vessel, and remove a metal fluoride resultant product from the reaction vessel.
摘要翻译：一种生产金属氟化物的方法，包括将预定重量的无水氢氟酸引入反应容器中并引发混合作用，将预定重量的无水金属预热至预定的反应温度，将无水金属的等分试样引入反应容器间隔直至加入了无水金属的整个预定重量，从反应容器中除去过量的无水氢氟酸，并从反应容器中除去金属氟化物。

9. 发明授权

US5649894A Compositions and methods for waste treatment 失效
标题翻译：废物处理的组成和方法
公开(公告)号：US5649894A
公开(公告)日：1997-07-22
申请号：US403924
申请日：1995-05-01
申请人： Timothy John White , James Hamilton Kyle , Gregory Francis Eaton
发明人： Timothy John White , James Hamilton Kyle , Gregory Francis Eaton
IPC分类号： A62D3/00 , A62D3/33 , A62D3/38 , A62D101/04 , A62D101/40 , A62D101/43 , A62D101/45 , A62D101/47 , B09B3/00 , C01B25/37 , C01B25/455 , C01F11/46 , C01G1/02 , C01G1/06 , C01G11/00 , C01G13/00 , C01G21/00 , C01G28/02 , C02F1/62 , C02F11/00 , C04B18/04 , G21F9/00
CPC分类号： C04B18/0463 , A62D3/33 , A62D3/38 , B09B3/0041 , C01B25/37 , C01B25/455 , C01G1/02 , C01G1/06 , C01G28/023 , A62D2101/04 , A62D2101/40 , A62D2101/43 , A62D2101/45 , A62D2101/47 , A62D2203/02 , C01P2006/60 , C04B2111/00784 , Y02W30/91
摘要： Methods for waste treatment and compositions of stabilized waste elements are provided, typically for the disposal of arsenical wastes. Arsenic trioxide waste produced as a by-product of metal extraction is slurried in water for from 6 to 24 hours with finely divided quicklime to produce nonvolatile calcium arsenate (III). An excess of CaO stoichiometry with As is used to consume secondary waste species such as sulphate, silicate and iron oxides. The precipitated arsenate is oven dried at 120.degree. C. and then calcined in air between 15 minutes to several hours at 1000.degree. C. to 500.degree. C. respectively to oxidize arsenate (III) to arsenate (V) as Ca.sub.5 (AsO.sub.4).sub.3 (OH) (an apatite) as the major arsenic immobilization phase, with minor arsenic incorporated in Ca.sub.3 (AsO.sub.4).sub.2. Calcium sulphate anhydrate (sulphate immobilization) and calcium iron oxide (iron immobilization) are also produced. Tertiary immobilization is achieved milling or fracturing and incorporating the apatite an encapsulant consisting of ordinary portland cement and flyash. After curing for one month in steel drums in a water saturated atmosphere, the waste form is ready to be transported either to a repository or to used as landfill. Further security may be achieved at the back end of the process by lining the repository with ferric clays that will strongly absorb and adsorb heavy metal species which may escape.
摘要翻译： PCT No.PCT / AU93 / 00489 Sec。 371日期：1995年5月1日 102（e）日期1995年5月1日PCT提交1993年9月21日PCT公布。出版物WO94 / 06575 日期1995年3月31日提供废物处理方法和稳定化废物的组成，通常用于处理砷废物。作为金属萃取副产物产生的三氧化二砷废水在水中制成6至24小时，细碎的生石灰生成不挥发性砷酸钙（III）。过量的CaO化学计量与As一起用于消耗二次废物物质，如硫酸盐，硅酸盐和氧化铁。将沉淀的砷酸盐在120℃下烘箱干燥，然后在空气中在1000℃〜500℃下在15分钟〜数小时之间煅烧，分别将Ca（AsO 4）3的砷酸盐（III）氧化为砷酸盐（V）（OH）（磷灰石）作为主要的砷固定相，在Ca3（AsO4）2中掺入少量砷。也产生硫酸钙无水物（硫酸盐固定化）和氧化铁（铁固定化）。三次固定实现了铣削或压裂，并将磷灰石作为由普通波特兰水泥和飞灰组成的密封剂。在水饱和气氛中，在钢桶中固化一个月后，废物形式准备运往储存库或用作填埋场。通过用强力吸收和吸附可能逸出的重金属物质的铁粘土衬里储存库，可以在该方法的后端实现进一步的安全性。

10. 发明授权

US5320674A Ultraviolet ray screening agent 失效
标题翻译：紫外线屏蔽剂
公开(公告)号：US5320674A
公开(公告)日：1994-06-14
申请号：US939948
申请日：1992-09-02
申请人： Yuji Takao , Akitsugu Ando , Tetsusi Kosugi , Fukuji Suzuki , Kazuhisa Ohno , Katsuki Ogawa
发明人： Yuji Takao , Akitsugu Ando , Tetsusi Kosugi , Fukuji Suzuki , Kazuhisa Ohno , Katsuki Ogawa
IPC分类号： C01B33/26 , A61K8/11 , A61K8/26 , A61Q17/04 , C01B33/40 , C01B33/42 , C01G1/06 , C01G49/00 , C04B14/20 , C09C1/00 , C09C1/28 , C09C1/40 , C09C3/06 , C09K3/00 , C01B33/00
CPC分类号： A61Q17/04 , A61K8/0241 , A61K8/11 , A61K8/26 , C01B33/26 , C01B33/42 , C01B33/425 , C01G1/06 , C01G49/009 , C09C1/00 , C09C1/0081 , C09C1/28 , C09C1/405 , A61K2800/412 , A61K2800/61 , C01P2002/72 , C01P2002/84 , C01P2004/03 , C01P2004/61 , C01P2004/62 , C01P2006/60 , C01P2006/62 , C01P2006/63 , C01P2006/64
摘要： A composite synthetic mica powder having an excellent ultraviolet ray screening effect, the composite synthetic mica powder comprising a fine particle layer (B) containing one or more types of elements selected from the group of Te, Bi, Pb, Ce, Fe, Mo, Nb, W, Sb, Sn, V, Mn, Ni, Co, Zn and Ti is formed on the surface of scale-like mica particles (A). The covering ratio of particles (A) by particles (B) is in the range of 0.5 to 1; the ratio of particle size of the particles (B) to plane direction diameter of the particles (A) is 0.1 or less; and particle size of the particles (A) is 1 to 100 .mu.m. Also, a red synthetic mica which develops light-resistant red color closer to the color of human skin and ultraviolet rays, a method for manufacturing the same, and an ultraviolet ray screening agent which contains the synthetic mica. The synthetic mica is expressed by the following formula (I):X.sub.1/3.about.1 Y.sub.2.about.3 (Z.sub.4 O.sub.10)F.sub.2.times.0.75.about.2.times.0.99 (I)where X represents one or more ions selected from the group of Na, K, Li, Ca, Rb and Sr; Y represents one or more ions selected from the group of Mg, Fe, Ni, Mn, Al, Li, Co, Ti and Zn; Z represents one or more ions selected from the group of Al, Si, Ge, Fe, B, Co and Ti; and at least one of Y and Z represents an iron ion; and the molar number of iron contained in the synthetic mica is 0.01 to 3 mols.
摘要翻译：具有优异的紫外线屏蔽效果的复合合成云母粉末，所述复合合成云母粉末包含含有选自Te，Bi，Pb，Ce，Fe，Mo等的一种或多种元素的微粒子层（B）在鳞片状云母粒子（A）的表面形成有Nb，W，Sb，Sn，V，Mn，Ni，Co，Zn，Ti。颗粒（B）颗粒（A）的覆盖率在0.5至1的范围内; 颗粒（B）的颗粒尺寸与颗粒（A）的平面方向直径的比率为0.1以下; 粒子（A）的粒径为1〜100μm。而且，红色合成云母，其显影更接近人体皮肤和紫外线的颜色的耐光性红色，其制造方法和含有合成云母的紫外线屏蔽剂。合成云母由下式（I）表示：X1 / 3差异1Y2差3（Z4O10）F2x0.75差异2x0.99（I）其中X表示选自Na，K，Li中的一种或多种离子，Ca，Rb和Sr; Y表示选自Mg，Fe，Ni，Mn，Al，Li，Co，Ti和Zn中的一种或多种离子; Z表示选自Al，Si，Ge，Fe，B，Co和Ti中的一种或多种离子; 并且Y和Z中的至少一个代表铁离子; 并且合成云母中含有的铁的摩尔数为0.01〜3摩尔。

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