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1. 发明申请

US20180339959A1 Process For Preparing Amino Compounds From Nitrile Compounds 审中-公开
公开(公告)号：US20180339959A1
公开(公告)日：2018-11-29
申请号：US15982590
申请日：2018-05-17
申请人： Evonik Degussa GmbH
发明人： Anne Rittsteiger , Stephan Kohlstruk , Dirk Hoppe , Alexander Martin Rüfer , Sabrina Sowka , Sven Schneider , Norbert Schlüter , Axel Hengstermann , Markus Galle , Stefan Röder , Monika Berweiler
IPC分类号： C07C209/52 , C07C209/48 , C07C209/26 , C07C211/36
CPC分类号： C07C209/52 , C07C209/26 , C07C209/48 , C07C211/36 , C07C253/30 , C07C2521/02 , C07C2523/86 , C07C2601/14 , C07C255/46
摘要： The present invention relates to a process for hydrogenating nitrile compounds to amino compounds, in which the cross-sectional loading of the reactor during the hydrogenation is less than or equal to 4.0 kg/m2*s, based on the liquid phase.

2. 发明授权

US09822062B2 Method and apparatus for producing dicyanobenzene 有权
公开(公告)号：US09822062B2
公开(公告)日：2017-11-21
申请号：US15025812
申请日：2015-03-09
申请人： MITSUBISHI GAS CHEMICAL COMPANY, INC.
发明人： Yukiya Ibi , Tatsuyuki Kumano , Natsumi Wakita
IPC分类号： C07C209/48 , C07C211/00 , C07C253/34 , C07C253/28 , B01D53/14 , B01D11/04 , B01D17/02 , B01D19/00 , B01D1/00 , B01D3/14
CPC分类号： C07C209/48 , B01D1/0082 , B01D3/14 , B01D11/0492 , B01D17/0214 , B01D19/00 , B01D53/1418 , B01D53/1493 , B01D2252/2053 , C07C253/24 , C07C253/28 , C07C253/34 , C07C255/51 , C07C211/27
摘要： The object is to prevent deterioration and loss of dicyanobenzene in producing dicyanobenzene by ammoxidation of xylene to thereby achieve industrial and economical advantage in producing of dicyanobenzene. The method for producing dicyanobenzene of the present invention includes: contacting a xylene-ammoxidation reaction gas containing dicyanobenzene in ammoxidation of xylene with an organic solvent so as to obtain a dicyanobenzene-absorbing solution; contacting the dicyanobenzene-absorbing solution with a basic aqueous solution containing a salt such as ammonium carbonate so as to extract a water-soluble salt formed by neutralization reaction between carboxylic acid in the dicyanobenzene-absorbing solution and a base in the basic aqueous solution into an aqueous phase; separating the mixture of the dicyanobenzene-absorbing solution and the basic aqueous solution into an organic phase and an aqueous phase; decomposing the salt such as ammonium carbonate contained in the organic phase for separation of the salt from the organic phase; and distilling the organic phase to separate low boiling point compounds contained in the organic phase from the organic phase so as to obtain dicyanobenzene.

3. 发明授权

US09670148B2 Method for producing meta-xylylenediisocyanates 有权
公开(公告)号：US09670148B2
公开(公告)日：2017-06-06
申请号：US14903268
申请日：2014-08-11
申请人： MITSUI CHEMICALS, INC.
发明人： Kouya Kojima , Hidetaka Tsukada , Mamoru Takashina , Chitoshi Shimakawa , Naoyuki Kakinuma
IPC分类号： C07C263/06 , C07C263/04 , C07C269/00 , C07C273/18 , C07C271/20 , C07C209/48 , C07C253/28
CPC分类号： C07C263/06 , C07C209/48 , C07C253/28 , C07C263/04 , C07C269/00 , C07C269/06 , C07C271/20 , C07C273/1809 , C07C273/1854 , C07C265/14 , C07C271/14 , C07C275/24
摘要： A method for producing meta-xylylenediisocyanates includes a reaction step in which monohalogenated benzenes, formaldehydes, and an amide compound represented by general formula (1) below are allowed to react in the presence of an acidic liquid to produce a bisamide compound; a dehalogenation step in which in the bisamide compound, the halogen atom derived from the monohalogenated benzenes is replaced with a hydrogen atom; and a thermal decomposition step in which the bisamide compound from which the halogen atom is eliminated is subjected to thermal decomposition. In the reaction step, the acidic liquid contains inorganic acid, the equivalent ratio of the hydrogen atom of the inorganic acid relative to the monohalogenated benzenes is more than 14, the acidic liquid has an inorganic acid concentration of more than 90 mass %, and the reaction temperature is more than 10° C.General formula (1): wherein R1 represents an alkoxy group or an amino group.

4. 发明申请

US20160376227A1 METHOD FOR PURIFYING ADIPODINITRILE (ADN) 有权
标题翻译：净化ADIPODINITRILE（ADN）的方法
公开(公告)号：US20160376227A1
公开(公告)日：2016-12-29
申请号：US15116541
申请日：2015-02-03
申请人： BASF SE
发明人： Hermann Luyken , Peter PFAB , Tim JUNGKAMP
IPC分类号： C07C253/34
CPC分类号： C07C253/34 , C07C209/48 , C07C253/10 , C07C255/04 , C07C211/12
摘要： The present invention relates to a process for purifying adiponitrile (ADN), wherein crude ADN is introduced into a rectification apparatus (R1). The rectification apparatus (R1) comprises a first side draw and preferably also a second side draw, the first side draw being disposed below the crude ADN introduction point and the optional second side draw being disposed above the crude ADN introduction point. The first side draw is used to draw off a gaseous stream comprising ADN while the optional second side draw is used to draw off undesired by-products such as 1-amino-2-cyanocyclopentene (ACCP) which are often generated in ADN production and consequently may be present in the crude ADN. The gaseous stream from the first side draw of (R1) is introduced into a second rectification apparatus (R2). (R2) is used to separate off ADN from remaining high boilers and any other by-products present, pure ADN being drawn off from (D2) as overhead product. It is preferable when the process according to the invention employs crude ADN from a reaction of butadiene with hydrocyanic acid (HCN).
摘要翻译：本发明涉及一种纯化己二腈（ADN）的方法，其中将粗ADN引入精馏装置（R1）。整流装置（R1）包括第一侧拉伸，优选地还包括第二侧拉伸，第一侧拉伸设置在粗ADN引入点的下方，并且可选的第二侧拉伸设置在粗ADN引入点的上方。第一侧拉伸用于抽出包含ADN的气流，而任选的第二侧拉伸用于除去常常在ADN生产中产生的不希望的副产物，例如1-氨基-2-氰基环戊烯（ACCP），因此可能存在于粗ADN中。将来自（R1）的第一侧拉制的气流引入第二整流装置（R2）。（R2）用于将ADN与剩余的高锅炉和任何其他副产物分离出来，纯的ADN作为塔顶产物从（D2）中排出。当根据本发明的方法从丁二烯与氢氰酸（HCN）的反应中使用粗ADN时，是优选的。

5. 发明授权

US09505870B2 Amine suitable as PU-catalyst 有权
标题翻译：胺适合作为PU催化剂
公开(公告)号：US09505870B2
公开(公告)日：2016-11-29
申请号：US14401953
申请日：2013-04-23
申请人： HUNTSMAN PETROCHEMICAL LLC
发明人： Eugene P Wiltz, Jr. , Robert Allison Grigsby, Jr. , Jennifer Price , Jingjun Zhou
IPC分类号： C08G18/18 , C08G18/76 , C08G18/48 , C07C217/04 , C07C213/02 , C07C217/08 , C07C209/48 , C07C253/30
CPC分类号： C08G18/1833 , C07C209/48 , C07C213/02 , C07C217/04 , C07C217/08 , C07C253/30 , C08G18/48 , C08G18/7621
摘要： An amine according to the invention has a formula (CH3)2NCH2CH2OCH2CH2CH2N(R1)(R2) wherein R1 is selected from (CH3)2NCH2CH2OCH2CH2CH2— and R2 is selected from the group consisting of H—, CH3(CnH2n)—, HO(CmH2m)— and (CH3)2NCH2CH2OCH2CH2CH2—, n being an integer in the range of 0 to 5, m being an integer in the range of 2 to 4.

6. 发明授权

US09403753B2 Dual site catalyst for mild, selective nitrile reduction 有权
标题翻译：用于轻度，选择性腈还原的双位点催化剂
公开(公告)号：US09403753B2
公开(公告)日：2016-08-02
申请号：US14948898
申请日：2015-11-23
申请人： University of Southern California
发明人： Travis J. Williams , Zhiyao Lu
IPC分类号： C07F15/00 , C07D213/00 , C07C209/00 , C07C209/48 , B01J31/18 , C07C213/02 , C07D213/38 , C07D307/68 , C07D333/38
CPC分类号： C07C209/48 , B01J31/181 , B01J31/1815 , B01J2231/64 , B01J2231/643 , B01J2531/0244 , B01J2531/821 , C07C29/143 , C07C29/147 , C07C209/16 , C07C213/02 , C07D213/38 , C07D307/68 , C07D333/38 , C07F15/0046 , C07C211/29 , C07C217/58 , C07C215/30 , C07C211/49 , C07C211/27 , C07C33/22 , C07C33/26
摘要： A ruthenium bis(pyrazolyl)borate scaffold that enables cooperative reduction reactivity in which boron and ruthenium centers work in concert to effect selective nitrile reduction is provided. The pre-catalyst compound [κ3-(1-pz)2HB(N═CHCH3)]Ru(cymene)+ TfO− (pz=pyrazolyl) was synthesized using readily-available materials through a straightforward route, thus making it an appealing catalyst for a number of reactions.
摘要翻译：提供了一种能够协同还原反应性的钌双（吡唑基）硼酸盐支架，其中硼和钌中心协同工作以实现选择性腈还原。使用容易获得的材料通过简单的途径合成催化剂前催化剂化合物[κ3-（1-pz）2HB（N = CHCH3）] Ru（异丙基苯）+ TfO-（pz =吡唑基），从而使其成为吸引人的催化剂对于一些反应。

7. 发明申请

US20160145193A1 DUAL SITE CATALYST FOR MILD, SELECTIVE NITRILE REDUCTION 有权
标题翻译：双位催化剂，选择性降解
公开(公告)号：US20160145193A1
公开(公告)日：2016-05-26
申请号：US14948898
申请日：2015-11-23
申请人： University of Southern California
发明人： Travis J. WILLIAMS , Zhiyao LU
IPC分类号： C07C209/48 , C07F15/00 , C07D333/38 , C07D213/38 , C07D307/68 , B01J31/18 , C07C213/02
CPC分类号： C07C209/48 , B01J31/181 , B01J31/1815 , B01J2231/64 , B01J2231/643 , B01J2531/0244 , B01J2531/821 , C07C29/143 , C07C29/147 , C07C209/16 , C07C213/02 , C07D213/38 , C07D307/68 , C07D333/38 , C07F15/0046 , C07C211/29 , C07C217/58 , C07C215/30 , C07C211/49 , C07C211/27 , C07C33/22 , C07C33/26
摘要： A ruthenium bis(pyrazolyl)borate scaffold that enables cooperative reduction reactivity in which boron and ruthenium centers work in concert to effect selective nitrile reduction is provided. The pre-catalyst compound [κ3-(1-pz)2HB(N═CHCH3)]Ru(cymene)− TfO− (pz=pyrazolyl) was synthesized using readily-available materials through a straightforward route, thus making it an appealing catalyst for a number of reactions.
摘要翻译：提供了一种能够协同还原反应性的钌双（吡唑基）硼酸盐支架，其中硼和钌中心协同工作以实现选择性腈还原。使用容易获得的材料通过简单的途径合成预催化剂化合物[＆kgr; 3-（1-pz）2HB（N = CHCH 3）]钌（异佛
苯母酰基）-TfO-（pz =吡唑基），从而使其成为吸引了许多反应的催化剂。

8. 发明授权

US09296681B2 Cycloalkylmethylamines 有权
标题翻译：环烷基甲胺
公开(公告)号：US09296681B2
公开(公告)日：2016-03-29
申请号：US14073800
申请日：2013-11-06
申请人： Reviva Pharmaceuticals, Inc.
发明人： Laxminarayan Bhat , Seema Bhat
IPC分类号： C07C69/34 , C07C209/48 , C07C209/88 , C07C211/26 , C07C213/06 , C07C213/10 , C07C217/74 , C07C219/06 , C07C231/02 , C07C237/06 , C07C271/20 , C07C229/34 , C07C69/96 , C07C237/22
CPC分类号： C07C69/34 , C07C69/96 , C07C209/48 , C07C209/88 , C07C211/26 , C07C213/06 , C07C213/10 , C07C217/74 , C07C219/06 , C07C229/34 , C07C231/02 , C07C237/06 , C07C237/22 , C07C271/20 , C07C2601/04
摘要： The present invention provides novel cycloalkylmethylamine derivatives, and methods of preparing cycloalkylmethylamine derivatives. The present invention also provides methods of using cycloalkylmethylamine derivatives and compositions of cycloalkylmethylamine derivatives. The pharmaceutical compositions of the compounds of the present invention can be advantageously used for treating and/or preventing obesity and obesity related co-morbid indications and depression and depression related co-morbid indications.
摘要翻译：本发明提供新的环烷基甲基胺衍生物，以及制备环烷基甲基胺衍生物的方法。本发明还提供了使用环烷基甲基胺衍生物和环烷基甲基胺衍生物的组合物的方法。本发明化合物的药物组合物可以有利地用于治疗和/或预防肥胖和肥胖相关并发症适应症和抑郁症和抑郁症相关并发症的适应症。

9. 发明申请

US20160031790A1 METHOD OF MANUFACTURE OF OCTANEDIOIC ACID, PRECURSORS, AND DERIVATIVES 审中-公开
标题翻译：十八烷酸，前驱体和衍生物的制备方法
公开(公告)号：US20160031790A1
公开(公告)日：2016-02-04
申请号：US14777069
申请日：2014-03-11
申请人： SEGETIS, INC.
发明人： ERICH J. MOLITOR , BRIAN D. MULLEN
IPC分类号： C07C51/353 , C07C67/03 , C07D307/33 , C07C51/09 , C07C51/36 , C07C29/149 , C07C253/06 , C07C209/48 , C07C209/16 , C07C263/10 , C07C227/08 , C07C67/313 , C07D211/02 , C07D223/10 , C07C67/465
CPC分类号： C07C51/353 , C07C29/149 , C07C51/09 , C07C51/36 , C07C67/03 , C07C67/313 , C07C67/465 , C07C209/16 , C07C209/48 , C07C227/08 , C07C253/06 , C07C263/10 , C07D211/02 , C07D211/40 , C07D223/10 , C07D301/12 , C07D305/08 , C07D307/32 , C07D307/33 , C07D307/58 , C07D317/30 , C07D493/04 , C07C57/03 , C07C57/13
摘要： A method for the manufacture of 1,8-octanedioic acid comprises: reacting gamma-valerolactone with an alcohol in the presence of an acid or a base catalyst to provide an alkyl pentenoate, converting the alkyl pentenoate in the presence of a metathesis initiator to provide the dialkyl octenedioate, reacting the dialkyl octenedioate with hydrogen in the presence of a hydrogenation catalyst to provide a dialkyl 1,8-octanedioate and hydrolyzing the dialkyl 1,8-octanedioate to provide the 1,8-octanedioic acid.
摘要翻译：制备1,8-辛二酸的方法包括：在酸或碱催化剂存在下使γ-戊内酯与醇反应，得到戊烯酸烷基酯，在复分解引发剂存在下转化戊烯酸烷基酯以提供八氢萘二酸二烷基酯，在氢化催化剂存在下使辛烯二酸二烷基酯与氢气反应，得到1,8-辛二酸二烷基酯，并水解1,8-辛二酸二烷基酯，得到1,8-辛二酸。

10. 发明申请

US20150057466A1 Synthesis of Triethylenetetramines 审中-公开
标题翻译：三亚乙基四胺的合成
公开(公告)号：US20150057466A1
公开(公告)日：2015-02-26
申请号：US14529671
申请日：2014-10-31
申请人： PhilEra New Zealand Limited
发明人： Marco Jonas , Irene Vaulont , Antonio Soi , Gunther Schmidt
IPC分类号： C07C209/76
CPC分类号： C07D233/02 , C07B2200/13 , C07C55/10 , C07C57/145 , C07C57/15 , C07C209/48 , C07C209/62 , C07C209/76 , C07C211/10 , C07C211/13 , C07C211/14 , C07C255/30 , C07D233/26
摘要： Methods and intermediates for synthesizing triethylenetetramine and salts thereof, as well as novel triethylenetetramine salts and their crystal structure, and triethylenetetramine salts of high purity.
摘要翻译：用于合成三亚乙基四胺及其盐的方法和中间体，以及新型三亚乙基四胺盐及其晶体结构，以及高纯度的三亚乙基四胺盐。

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