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1. 发明授权

US07148301B2 High purity fluoropolymers 失效
公开(公告)号：US07148301B2
公开(公告)日：2006-12-12
申请号：US10743208
申请日：2003-12-22
申请人： Thomas J. Blong , Denis Duchesne , Gernot Loehr , Albert Killich , Tilman Zipplies , Ralph Kaulbach , Herbert Strasser
发明人： Thomas J. Blong , Denis Duchesne , Gernot Loehr , Albert Killich , Tilman Zipplies , Ralph Kaulbach , Herbert Strasser
IPC分类号： C08F116/12
CPC分类号： C08F6/06 , C08F6/22 , C08L27/12
摘要： The invention relates to high purity fluoropolymers and processes for making such materials. These polymers are particularly suited for applications in the semiconductor industry. The process comprises removal of unstable polymer end groups by fluorination and removal of heavy metal impurities by extraction with an aqueous acid medium.

2. 发明授权

US07148300B2 Fluoroelastomers with improved permeation resistance and method for making the same 失效
标题翻译：具有改善渗透阻力的氟弹性体及其制备方法
公开(公告)号：US07148300B2
公开(公告)日：2006-12-12
申请号：US10659877
申请日：2003-09-11
申请人： Tatsuo Fukushi , Allan T. Worm , Erik D. Hare , Greggory S. Bennett , William D. Coggio
发明人： Tatsuo Fukushi , Allan T. Worm , Erik D. Hare , Greggory S. Bennett , William D. Coggio
IPC分类号： C08F116/12
CPC分类号： C08F214/18 , C08F214/16 , C08K5/0025 , C08L27/12
摘要： A compound is prepared, suitable for forming fluoroelastomers, having the unique features of a low glass transition temperature and desirable permeation resistance. The compound generally comprises two primary components. The first component is an amorphous copolymer including interpolymerized units derived from one or more perfluorinated ethers. The second component is a curable component including at least one filler having at least 10 parts per 100 parts of the first component. Upon vulcanization the resulting elastomeric compound has desirable physical characteristics as indicated by the durometer, the retraction at lower temperatures (TR-10) and permeation resistance.
摘要翻译：制备适合于形成含氟弹性体的化合物，其具有低玻璃化转变温度和所需渗透阻力的独特特征。化合物通常包含两个主要组分。第一组分是包含衍生自一种或多种全氟化醚的共聚单元的无定形共聚物。第二组分是可固化组分，其包含至少一种每100份第一组分至少10份的填料。硫化后，得到的弹性体化合物具有所需的物理特性，如硬度计所示，在较低温度下回缩（TR-10）和耐渗透性。

3. 发明授权

US07071273B2 Tetrafluoroethylene copolymer, its production method and paste extruded product 失效
标题翻译：四氟乙烯共聚物，其生产方法和糊状挤出产品
公开(公告)号：US07071273B2
公开(公告)日：2006-07-04
申请号：US10992718
申请日：2004-11-22
申请人： Shigeki Kobayashi , Shinya Higuchi , Masataka Arai , Hiroki Nagai
发明人： Shigeki Kobayashi , Shinya Higuchi , Masataka Arai , Hiroki Nagai
IPC分类号： C08F16/24 , C08F116/12 , C08F26/00
CPC分类号： C08F214/262 , Y10S526/919 , Y10T428/2998
摘要： Provided are a tetrafluoroethylene copolymer excellent in paste extrudability, which comprises a unit based on tetrafluoroethylene and a unit based on a monomer represented by a formula of CF2═CF—O—(CF2)nCF═CF2 (wherein n is an integer of from 1 to 6), wherein a content of the unit based on the monomer represented by the formula is from 0.1 to 0.5% by mass, wherein a particle size of a primary particle is from 0.1 to 0.5 μm, wherein a standard specific gravity is from 2.14 to 2.25, wherein a paste extrusion pressure is from 24.5 to 73.5 MPa and wherein the copolymer remains not undergoing melt molding; a fine powder of a tetrafluoroethylene copolymer; and a production method and a paste extruded product thereof. The TFE copolymer is excellent in paste extrudability and the molded product thereof is excellent in heat resistance and transparency.
摘要翻译：提供了一种糊状挤出性优异的四氟乙烯共聚物，其包含基于四氟乙烯的单元和基于由CF 2 -SF-O-（CF 2 O）2表示的单体的单元， /其中n为1至6的整数），其中基于由式（I）表示的单体的单元的含量为0.1〜0.5质量％，其中一次粒子的粒径为0.1〜0.5μm，标准比重为2.14〜2.25，糊料挤出压力为24.5〜73.5MPa，共聚物仍未经熔融成型; 四氟乙烯共聚物的细粉末; 及其制造方法及其糊状挤压制品。 TFE共聚物的糊状挤出性优异，其成型体的耐热性和透明性优异。

4. 发明授权

US07067593B2 Poly(arylene ethers) with pendant crosslinkable groups, and devices incorporating same 失效
标题翻译：具有侧链可交联基团的聚（亚芳基醚）和与其结合的装置
公开(公告)号：US07067593B2
公开(公告)日：2006-06-27
申请号：US10713469
申请日：2003-11-14
申请人： Timothy M. Londergan
发明人： Timothy M. Londergan
IPC分类号： C08F116/12 , C08F16/12 , C08F14/00
CPC分类号： C08G65/40 , C08G18/4879 , C08G65/48 , G03F7/0388
摘要： A polymer comprising units having the formula (I) wherein: Q1 comprises at least one aryl or heteroaryl group; Q2 comprises at least one aryl or heteroaryl group; X1 is O bonded directly to an aryl carbon of Q1; X2 is O bonded directly to an aryl carbon of Q2; Z is a linker comprising at least one —(C(R2)2)— group; Y is a single bond or linker group (e.g., comprising up to about 50 carbons); R1 is independently at each occurrence H, a halogen, an alkyl group, a heteroalkyl group, an aryl group, or a heteroaryl group; R2 is independently at each occurrence H, an alkyl group, or a heteroalkyl group; and R3 is H or a crosslinkable group.
摘要翻译：包含具有式（I）的单元的聚合物其中：Q 1至少包含一个芳基或杂芳基; Q ^{2包含至少一个芳基或杂芳基; O 1直接与Q 1的芳基碳键合; X 2直接与Q 2的芳基碳键合; Z是包含至少一个 - （C（R 2）N 2） - 基团的连接体; Y是单键或连接基团（例如包含至多约50个碳原子）; R 1在每次出现时独立地为H，卤素，烷基，杂烷基，芳基或杂芳基; R 2在每次出现时独立地为H，烷基或杂烷基; R 3是H或可交联基团。}

5. 发明授权

US07009018B2 Tetrafluoroethylene copolymer 失效
标题翻译：四氟乙烯共聚物
公开(公告)号：US07009018B2
公开(公告)日：2006-03-07
申请号：US11080636
申请日：2005-03-16
申请人： Kazuya Oharu , Hidekazu Okamoto , Shin Tatematsu , Shigeki Kobayashi , Shinya Higuchi , Masataka Arai , Hiroki Nagai
发明人： Kazuya Oharu , Hidekazu Okamoto , Shin Tatematsu , Shigeki Kobayashi , Shinya Higuchi , Masataka Arai , Hiroki Nagai
IPC分类号： C08F116/12 , C08F16/24 , C08F216/12 , C08F114/18 , C08F14/18
CPC分类号： C08F214/26
摘要： Provided is a tetrafluoroethylene copolymer consisting of a unit based on tetrafluoroethylene and a unit based on a monomer represented by CF2═CFORf1Rf2 (where Rf1 is a polyfluoroalkylene group which may contain an etheric oxygen atom and Rf2 is a polyfluorocycloalkyl group which may contain an etheric oxygen atom), wherein a content of the latter is from 0.005 to 0.5% by mass. The tetrafluoroethylene copolymer is excellent both in paste extrudability and in heat resistance, has characteristics such as excellent transparency of a molded product, and is suitably applicable to paste extrusion and compression molding.
摘要翻译：提供一种四氟乙烯共聚物，其由基于四氟乙烯的单元和基于由CF 2 - （CH 2）2表示的单体组成的单元组成其中R f1是可以含有醚性氧原子的多氟亚烷基，R f2是可以含有醚性氧原子的多氟环烷基），其中后者的含量为0.005〜0.5质量％。四氟乙烯共聚物在糊状挤出性和耐热性方面优异，具有成型品的透明性优异的特性，适用于糊料挤出和压塑。

6. 发明申请

US20050282955A1 Fluoroelastomer gels 有权
标题翻译：氟弹性体凝胶
公开(公告)号：US20050282955A1
公开(公告)日：2005-12-22
申请号：US11158334
申请日：2005-06-22
申请人： Marco Apostolo , Stefano Arrigoni , Margherita Albano
发明人： Marco Apostolo , Stefano Arrigoni , Margherita Albano
IPC分类号： C08F14/22 , C08F214/18 , C08F214/22 , C08L27/16 , C08F116/12
CPC分类号： C08L27/20 , C08F214/18 , C08F214/22 , C08K3/20 , C08L27/16 , C08L27/18 , C08L2205/02 , C08L2666/04
摘要： Fluoroelastomeric gel having the following properties: appearance: transparent gelatinous solid; water content between 10% and 90% by weight; a density between 1.1 and 2.1 g/cm3; said gel satisfies the following test: dried in a stove at 90° C. until a constant weight gives curable fluoroelastomers.
摘要翻译：具有以下性质的氟弹性体凝胶：外观：透明凝胶状固体; 水含量在10％至90％之间; 1.1至2.1g / cm 3之间的密度; 所述凝胶满足以下试验：在90℃的炉子中干燥直到恒重为固化性的含氟弹性体。

7. 发明申请

US20040225095A1 Process for the manufacture of thermally stable PVDF 有权
标题翻译：用于制造热稳定PVDF的工艺
公开(公告)号：US20040225095A1
公开(公告)日：2004-11-11
申请号：US10791226
申请日：2004-03-02
发明人： Patrick Kappler , Veronique Gauthe
IPC分类号： C08F116/12
CPC分类号： C08K5/098 , C08F14/22 , C08K5/42 , C08F2/16 , C08L27/16
摘要： The present invention relates to a process for the manufacture of PVDF homopolymer or copolymer by radical polymerization of vinylidene fluoride (VDF), and optionally of a comonomer, in aqueous dispersion and in the presence of a transfer agent, of a persulphate as radical initiator, optionally of a surface-active additive and optionally of a paraffin wax, in which: a) sodium acetate is added, either at the start of or during or after the polymerization, b) a potassium alkylsulphonate is optionally added after the polymerization, c) an aqueous PVDF dispersion is obtained, d) the PVDF is collected by atomizing the dispersion obtained in c) with air at a temperature of between 120 and 220null C., the aqueous dispersion obtained in c) not being washed with water before atomizing.
摘要翻译：本发明涉及通过偏二氟乙烯（VDF）和任选的共聚单体在水分散体中和在转移剂的存在下通过过氧化氢作为自由基引发剂的自由基聚合制备PVDF均聚物或共聚物的方法，任选的表面活性添加剂和任选的石蜡，其中：a）在聚合开始或聚合期间或之后加入乙酸钠，b）在聚合后任选地加入烷基磺酸钾，c）得到水性PVDF分散体，d）通过在空气中在120-220℃的温度下雾化c）中得到的分散体来收集PVDF，c）中得到的水分散体在雾化之前不被水洗涤。

8. 发明申请

US20030216531A1 High vinyl ether modified sinterable polytetrafluoroethylene 有权
标题翻译：高乙烯基醚改性可烧结聚四氟乙烯
公开(公告)号：US20030216531A1
公开(公告)日：2003-11-20
申请号：US10420144
申请日：2003-04-22
发明人： Ralph M. Aten , Sharon Ann Libert
IPC分类号： C08F116/12
CPC分类号： C08F214/262 , Y10T428/2982
摘要： Modified polytetrafluoroethylene powder of a sinterable copolymer of tetrafluoroethylene containing about 0.5 to about 10 weight % of fluorinated vinyl ether, the copolymer having a melt creep viscosity of greater than about 1null106 PanullS. In preferred embodiments, the sinterable copolymer has a melt creep viscosity of greater than about 1null107 PanullS and fluorinated vinyl ether content of from about 1 to about 7 weight %. The polymer has a combination of a high level of fluorinated vinyl ether and a melt creep viscosity which is high enough to enable the fabrication of articles by sintering.
摘要翻译：包含约0.5至约10重量％氟化乙烯基醚的四氟乙烯的可烧结共聚物的改性聚四氟乙烯粉末，该共聚物的熔体蠕变粘度大于约1×10 6 Paa.S。在优选的实施方案中，可烧结共聚物的熔体蠕变粘度大于约1×10 7 Pa，氟化乙烯基醚含量为约1至约7重量％。该聚合物具有高水平的氟化乙烯基醚和熔体蠕变粘度的组合，其足够高以能够通过烧结制造制品。

9. 发明申请

US20030153700A1 Low equivalent weight ionomer 有权
标题翻译：低当量离聚物
公开(公告)号：US20030153700A1
公开(公告)日：2003-08-14
申请号：US10011242
申请日：2001-12-06
发明人： Huey Shen Wu , Charles W. Martin , Xin Kang Chen
IPC分类号： C08F016/24 , C08F116/12 , C08F216/12
CPC分类号： H01M8/1004 , B01D69/10 , B01D71/32 , B01D71/38 , B01D71/76 , C08F214/184 , C08F214/262 , C08J5/2281 , C08J2327/18 , H01M4/8605 , H01M8/1023 , H01M8/1039 , H01M8/106 , Y10T442/2918
摘要： An ionomer and a process for forming the ionomer such that the ionomer has (1) low equivalent weight; below 950, preferably between 625 and 850, and most preferably between about 700 and about 800; and (2) high conductivity, (greater than 0.15 S/cm). In an alternative embodiment, the ionomer has (1) low equivalent weight; below 950, preferably between 625 and 850, and most preferably between about 700 and about 800; and (2) acceptably low hydration, (less than about 75 weight percent). These ionomers are adapted to be processed into thin films that have acceptable physical stability. They are thus extremely well-suited for low humidity or high temperature fuel cell applications.
摘要翻译：离聚物和用于形成离聚物的方法使得离聚物具有（1）低当量重量; 低于950，优选625至850，最优选约700至约800; 和（2）高导电率（大于0.15S / cm）。在替代实施方案中，离聚物具有（1）低当量重量; 低于950，优选625至850，最优选约700至约800; 和（2）可接受的低水合（小于约75重量％）。这些离聚物适于被加工成具有可接受的物理稳定性的薄膜。因此，它们非常适用于低湿度或高温燃料电池应用。

10. 发明授权

US6153663A UV curable high index vinyl esters 失效
标题翻译：紫外光固化高指数乙烯基酯
公开(公告)号：US6153663A
公开(公告)日：2000-11-28
申请号：US194503
申请日：1999-03-31
申请人： Fang Chen , Huan Kiak Toh
发明人： Fang Chen , Huan Kiak Toh
IPC分类号： C08F16/32 , C08F18/14 , C08F290/06 , C08F2/46 , C08F116/12 , C08F216/12 , C08G63/52
CPC分类号： C08F16/32 , C08F18/14 , C08F290/062
摘要： A cross-linkage polymeric casting composition including an effective amount of a divinyl ester monomer of a bicyclic or polycyclic compound, and optionally, a minor amount of a di- or polythio compound. The specification and claims include allylic ethers withing the definition of divinyl ester, for example bisphenol fluorene diglycidyl allylic ether and bisphenol S diallyl ether.
摘要翻译： PCT No.PCT / AU97 / 00310 Sec。 371日期1999年3月31日 102（e）1999年3月31日PCT PCT 1997年5月22日PCT公布。公开号WO97 / 44372 日期1997年11月27日一种交联聚合物浇铸组合物，其包含有效量的双环或多环化合物的二乙烯基酯单体和任选的少量二 - 或多硫代化合物。说明书和权利要求书包括具有二乙烯基酯定义的烯丙基醚，例如双酚芴二缩水甘油基烯丙基醚和双酚S二烯丙基醚。

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