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1. 发明授权

US4517283B1 失效
公开(公告)号：US4517283B1
公开(公告)日：1992-04-28
申请号：US56219083
申请日：1983-12-15
申请人： CIBA GEIGY AG
发明人： DAVID G LEPPARD , JEAN RODY
IPC分类号： G03C7/26 , G03C7/392 , G03C1/34
CPC分类号： G03C7/39296 , G03C7/39216 , G03C7/39248 , G03C7/39256 , G03C7/3928 , Y10S430/132 , Y10S430/162

2. 发明授权

US3929826A Indazole derivatives as optical brighteners 失效
标题翻译：吲唑衍生物作为荧光增白剂
公开(公告)号：US3929826A
公开(公告)日：1975-12-30
申请号：US47151474
申请日：1974-05-20
申请人： CIBA GEIGY AG
发明人： STAGI MAURO
IPC分类号： C07D231/54
摘要： The present invention relates to new 1,3-diaryl-3a, 4, 5, 6, 7, 7a-hexahydroindazoles, which are useful as optical brighteners for high molecular organic materials.
摘要翻译：本发明涉及可用作高分子有机材料的荧光增白剂的新的1,3-二芳基-3a,4,5,6,7,7a-六氢吲唑。

3. 发明授权

US3928314A One step process of preparing azo dyes by simultaneous diazotization and coupling at low pH 失效
标题翻译：通过在低pH下同时重氮化和偶联制备偶氮染料的一步法
公开(公告)号：US3928314A
公开(公告)日：1975-12-23
申请号：US36184173
申请日：1973-05-18
申请人： CIBA GEIGY AG
发明人： ROCHAT ALAIN CLAUDE , STOCKER EMIL
IPC分类号： C09B41/00 , C09B29/00
CPC分类号： C09B41/009
摘要： Metal-free azo compounds are produced by the addition of an ester of nitrous acid to a mixture of a diazotisable amine, a coupling component, an organic acid and an organic solvent. The compounds produced are azo pigments or intermediates therefor.
摘要翻译：通过向可重氮胺，偶联组分，有机酸和有机溶剂的混合物中加入亚硝酸酯制备无金属偶氮化合物。所生产的化合物是偶氮颜料或其中间体。

4. 发明授权

US3925346A Mixed chromium-containing azo dyestuffs containing, per atom of chromium, one molecule of an o,o'-dihydroxy-sulphophenylene-azo-naphthalene and one molecule of an -o-hydroxyphenylene-azo-acetoacetamide 失效
标题翻译：含有铬的混合的含有AZO的白蛋白，每个原子含有一个O，O-二羟基 - 亚磺酰基 - 亚油酸和一个O-羟基苯甲酰氨基 - 乙酰胺的分子
公开(公告)号：US3925346A
公开(公告)日：1975-12-09
申请号：US19067971
申请日：1971-10-19
申请人： CIBA GEIGY AG
发明人： BUEHLER ARTHUR , SCHUETZ HANS-ULRICH
IPC分类号： C09B45/06 , C09B45/16 , C09B45/48 , D06P3/00 , D06P3/04
CPC分类号： C09B45/16 , C09B45/06 , C09B45/48 , Y10S8/917
摘要： IN WHICH D represents the residue of a diazo component of the benzene series bound to the azo bridge in vicinal position to the hydroxyl group and A represents the residue of an acetoacetamide which is bound to the azo bridge in vicinal position to the enolized keto group; the new dyestuffs are especially valuable for dyeing wool and leather and yield brown dyeings of good general fastness properties such as light, washing, perspiration, dry and wet rubbing, and great tinctorial strength.

IN WHICH ONE X represents a nitro group and the other X a sulphonic acid group, and the other corresponds to the formula

The invention relates to metal compounds which contain one molecule each of two different monoazo dyestuffs, one of which corresponds to the formula

5. 发明授权

US3923677A 2-Stilbenyl-4-styryl-v-triazoles, their use for the optical brightening of organic materials, and processes for their manufacture 失效
标题翻译： 2-苯乙烯基-4-苯乙烯基-V-三唑，它们用于有机材料的光学增亮及其制造方法
公开(公告)号：US3923677A
公开(公告)日：1975-12-02
申请号：US51769774
申请日：1974-10-24
申请人： CIBA GEIGY AG
发明人： KABAS GUGLIELMO , SCHLAEPFER HANS , FLETCHER IAN JOHN
IPC分类号： C07D249/06 , C11D3/42
CPC分类号： C07D249/06 , C11D3/42
摘要： The present invention relates to detergents containing 0.001 to 0.5% by weight of new v-triazoles of the formula

WHEREIN X1 denotes hydrogen, halogen, methyl or optionally substituted phenyl, R1 denotes hydrogen, halogen, alkyl with 1 to 4 carbon atoms, optionally substituted phenyl or alkoxy with 1 to 4 carbon atoms, or together with R2 in the o-position denotes a fused benzene ring, R2 denotes hydrogen, halogen, alkyl with 1 to 4 carbon atoms or alkoxy with 1 to 4 carbon atoms, or together with R1 in the o-position denotes a fused benzene ring, R3 denotes hydrogen, a nitrile group, an optionally functionally modified sulpho group or an optionally functionally modified carboxyl group, R4 denotes hydrogen, halogen, a nitrile group, alkyl with 1 to 4 carbon atoms, optionally substituted phenyl, alkoxy with 1 to 4 carbon atoms, optionally functionally modified carboxyl or an optionally functionally modified sulpho group and R5 denotes hydrogen, alkyl with 1 to 4 carbon atoms or alkoxy with 1 to 4 carbon atoms. The detergent compositions can be used for brightening textiles.
摘要翻译：本发明涉及含有0.001至0.5重量％的新的式v-三唑，式WHEREIN X1表示氢，卤素，甲基或任选取代的苯基，R 1表示氢，卤素，具有1至4个碳原子的烷基，任选取代的具有1至4个碳原子的苯基或烷氧基，或与o位置的R 2一起表示稠合苯环，R 2表示氢，卤素，具有1至4个碳原子的烷基或具有1至4个碳原子的烷氧基，或与 o位的R 1表示稠合的苯环，R 3表示氢，腈基，任选的功能修饰的磺基或任选的官能改性的羧基，R 4表示氢，卤素，腈基，具有1至4个碳原子的烷基原子，任选取代的苯基，具有1至4个碳原子的烷氧基，任选的官能改性的羧基或任选的功能修饰的磺基，R 5表示氢，具有1至4个碳原子的烷基或烷氧基wi 1至4个碳原子。

6. 发明授权

US3923452A Amine salt of a dyestuff in a ketone solution 失效
标题翻译：酮溶液中染料的胺盐
公开(公告)号：US3923452A
公开(公告)日：1975-12-02
申请号：US34838373
申请日：1973-04-05
申请人： CIBA GEIGY AG
发明人： WEGMANN JACQUES , BECKER CARL , ZWAHLEN GUENTHER , KUSTER WERNER
IPC分类号： C08J3/205 , C08J3/22 , C09B67/00 , D06P1/10
CPC分类号： C08J3/2053 , C08J3/226 , C08J2301/08 , C09B67/00
摘要： A process for the manufacture of coloured shaped articles from high polymer synthetic resins, wherein water-insoluble, hydrophobic, high polymer synthetic resins in solid form, especially in the form of granules or powders, in a mixture of hydrophilic and organophilic solvents that are recriprocally soluble in one another only to a limited extent and form a twophase system, are treated with dyestuffs or optical brighteners, the solubility of which in the organophilic portion of the twophase system is greater than in the hydrophilic portion, the solvent is removed, the synthetic resin dried and shaped, optionally with addition of untreated high polymer fully synthetic resin, from the melt or from a solvent.
摘要翻译：用于从高分子合成树脂制造着色成形制品的方法，其中固体形式的水不溶性，疏水性，高聚合物合成树脂，特别是颗粒或粉末形式，在亲水和亲有机溶剂的混合物中，其反复地在有限程度上相互溶解并形成两相体系，用染料或荧光增白剂处理，其在两相体系的亲有机部分的溶解度大于亲水部分的溶解度，溶剂是将合成树脂干燥并成形，任选地从熔体或溶剂中加入未处理的高分子全合成树脂。

7. 发明授权

US3920719A Water-insoluble styryl dyestuffs 失效
公开(公告)号：US3920719A
公开(公告)日：1975-11-18
申请号：US34166873
申请日：1973-03-15
申请人： CIBA GEIGY AG
发明人： DESAI NALIN BINDUPRASAD , JENNY WALTER
IPC分类号： C09B23/14 , C07C121/78
CPC分类号： C07C255/00 , C09B23/143 , Y10S8/922
摘要： Water-insoluble styryl dyestuffs of the formula

WHEREIN X is an alkylsulphonyl, carbamyl, carbalkoxy or cyano group and B is a monovalent organic radical, A is an alkylene group which may be interrupted by a hetero-atom, Y1 and Y2 each represents a hydrogen or halogen atom or an alkyl or alkoxy group, Y1 and Y2 being identical or different from one another, Z is a substituted or unsubstituted alkyl group or can represent a radical of the formula -A-CO-V-B, V is a sulphur atom or an -NHgroup or, when B is an aromatic radical an oxygen atom. The dyestuffs dye polyester fibres in fast yellow shades.

8. 发明授权

US3920689A N-heterocyclic perfluoroalkylmonocarboxylic acid esters, processes for their manufacture and their use 失效
标题翻译： N-杂环戊二烯甲氧基酸酯，其制造方法及其使用
公开(公告)号：US3920689A
公开(公告)日：1975-11-18
申请号：US33016073
申请日：1973-02-06
申请人： CIBA GEIGY AG
发明人： JAEGER HORST
IPC分类号： C03C17/32 , C07D233/32 , C07D233/72 , C14C11/00 , D06M13/236 , D06M13/35 , D06M13/385 , D06M15/423 , D06M15/433 , C07D233/34
CPC分类号： D06M15/433 , C03C17/324 , C07D233/32 , C07D233/72 , C14C11/00 , D06M13/236 , D06M13/35 , D06M13/385 , D06M15/423
摘要： Perfluoroalkylmonocarboxylic acid esters from ethylene urea epoxides are provided. These esters contain a perfluoro alkyl radical, which is bonded directly or via an alkylene group with 1 to 10 carbon atoms to a carboxyl group. This carboxyl group is bonded in an ester-like manner to an acylic, aliphatic radical substituted in the 2-position to the ester bridge by a free, etherified or esterified hydroxyl group. This latter radical being bonded to a ring nitrogen atom of an ethylene urea radical, which in turn at least by its second ring nitrogen atom is bonded to an acylic aliphatic radical which contains an epoxide group in the terminal position or is linked to an acylic aliphatic radical which is in turn bonded in an esterlike manner to a perfluoroalkyl radical. These fluoro compounds are manufactured from the corresponding perfluoroalkylcarboxylic acids and epoxides and are used for finishing of porous and non-porous substrates, especially for producing oleophobic finishes on textiles.

9. 发明授权

US3919183A Perfluoroalkyl groups containing polymerisation products 失效
标题翻译：含有聚合产物的全氟烷基
公开(公告)号：US3919183A
公开(公告)日：1975-11-11
申请号：US39752273
申请日：1973-09-17
申请人： CIBA GEIGY AG
发明人： JAGER HORST , SCHAFER PAUL
IPC分类号： C09K3/00 , C08F20/00 , C08F20/22 , C08F20/24 , C08F120/68 , C08F220/68 , C09K3/18 , D06M15/277 , C08F3/64 , C08F3/66 , C08F15/16
CPC分类号： D06M15/277 , C08F20/24
摘要： wherein Rf represents an unbranched or branched perfluoroalkyl radical with 3 to 12 carbon atoms, R represents hydrogen or fluorine, and R1 and R2 represent hydrogen or methyl and m is 1 or 2, n is a whole number from 2 to 12, and p is a whole number from 1 to 3, and optionally of other copolymerisable, ethylenically unsaturated monomeric compounds are provided. The polymerisation products can be homopolymers or copolymers. The polymerisation products are useful for producing oleophobic, hydrophobic or dirt repellent finishes on various substrates.

Polymerisation products of at least one perfluoroalkylalkyl ester of the formula
摘要翻译：至少一种式RO的全氟烷基烷基酯的聚合产物| PARALLEL Rf CH2-CF pCnH2nOC-CH2 m-1-C = CH || R1R2其中Rf表示具有3至12个碳原子的无支链或支链全氟烷基，R表示氢或氟，并且R 1和R 2表示氢或甲基，m为1或2，n为2至12的整数，p为1至3的整数，并且任选地其它可共聚的烯属不饱和单体化合物为提供。聚合产物可以是均聚物或共聚物。

10. 发明授权

US3919158A Polyvinyl chloride plasticized with mixed phosphate esters 失效
标题翻译：聚氯乙烯用混合磷酸酯增塑
公开(公告)号：US3919158A
公开(公告)日：1975-11-11
申请号：US37045573
申请日：1973-06-15
申请人： CIBA GEIGY AG
发明人： RANDELL DONALD RICHARD , PICKLES WILFRED
IPC分类号： C07F9/12 , C08K5/523 , C10L1/26 , C08K5/52
CPC分类号： C10M1/08 , C07F9/12 , C08K5/52 , C08K5/523 , C10L1/2641 , C10M2223/041 , C10N2240/08 , C10N2250/121 , C08L27/06
摘要： Phosphorylated alkylated phenol/phenol ester mixtures in which the weight ratio of the alkyl moiety to the phenol moiety ranges from 0.05 to about 0.65, and the number of carbon atoms per alkyl moiety ranges from 3 to 16, preferably from 3 to 12, which mixtures have satisfactory viscosity range and impart to polymeric materials and especially to polyvinylchloride plasticized therewith good light and heat stability: a process for producing such phosphorylated alkylated phenol/phenol ester mixtures; and polymeric materials plasticized therewith.
摘要翻译：其中烷基部分与苯酚部分的重量比为0.05至约0.65的磷酸化烷基化苯酚/酚酯混合物，每个烷基部分的碳原子数范围为3至16，优选3至12，该混合物具有令人满意的粘度范围并赋予聚合物材料，特别是对具有良好的光和热稳定性的聚氯乙烯进行增塑：一种生产这种磷酸化烷基化酚/苯酚酯混合物的方法; 并且用其增塑的聚合物材料。

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