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1. 发明授权

US3923677A 2-Stilbenyl-4-styryl-v-triazoles, their use for the optical brightening of organic materials, and processes for their manufacture 失效
标题翻译： 2-苯乙烯基-4-苯乙烯基-V-三唑，它们用于有机材料的光学增亮及其制造方法
公开(公告)号：US3923677A
公开(公告)日：1975-12-02
申请号：US51769774
申请日：1974-10-24
申请人： CIBA GEIGY AG
发明人： KABAS GUGLIELMO , SCHLAEPFER HANS , FLETCHER IAN JOHN
IPC分类号： C07D249/06 , C11D3/42
CPC分类号： C07D249/06 , C11D3/42
摘要： The present invention relates to detergents containing 0.001 to 0.5% by weight of new v-triazoles of the formula

WHEREIN X1 denotes hydrogen, halogen, methyl or optionally substituted phenyl, R1 denotes hydrogen, halogen, alkyl with 1 to 4 carbon atoms, optionally substituted phenyl or alkoxy with 1 to 4 carbon atoms, or together with R2 in the o-position denotes a fused benzene ring, R2 denotes hydrogen, halogen, alkyl with 1 to 4 carbon atoms or alkoxy with 1 to 4 carbon atoms, or together with R1 in the o-position denotes a fused benzene ring, R3 denotes hydrogen, a nitrile group, an optionally functionally modified sulpho group or an optionally functionally modified carboxyl group, R4 denotes hydrogen, halogen, a nitrile group, alkyl with 1 to 4 carbon atoms, optionally substituted phenyl, alkoxy with 1 to 4 carbon atoms, optionally functionally modified carboxyl or an optionally functionally modified sulpho group and R5 denotes hydrogen, alkyl with 1 to 4 carbon atoms or alkoxy with 1 to 4 carbon atoms. The detergent compositions can be used for brightening textiles.
摘要翻译：本发明涉及含有0.001至0.5重量％的新的式v-三唑，式WHEREIN X1表示氢，卤素，甲基或任选取代的苯基，R 1表示氢，卤素，具有1至4个碳原子的烷基，任选取代的具有1至4个碳原子的苯基或烷氧基，或与o位置的R 2一起表示稠合苯环，R 2表示氢，卤素，具有1至4个碳原子的烷基或具有1至4个碳原子的烷氧基，或与 o位的R 1表示稠合的苯环，R 3表示氢，腈基，任选的功能修饰的磺基或任选的官能改性的羧基，R 4表示氢，卤素，腈基，具有1至4个碳原子的烷基原子，任选取代的苯基，具有1至4个碳原子的烷氧基，任选的官能改性的羧基或任选的功能修饰的磺基，R 5表示氢，具有1至4个碳原子的烷基或烷氧基wi 1至4个碳原子。

2. 发明授权

US3658833A Benzofurans 失效
标题翻译： BENZOFURANS
公开(公告)号：US3658833A
公开(公告)日：1972-04-25
申请号：US3658833D
申请日：1970-06-15
申请人： CIBA GEIGY AG
发明人： KABAS GUGLIELMO , SCHLAPFER HANS
IPC分类号： C07C205/35 , C07D307/81 , C07D405/10 , C09B43/06 , C11D1/00 , D06L3/12 , D06M13/10 , D06M13/358 , C07D99/04 , C09K1/02
CPC分类号： C09B43/06 , C07C205/44 , C07D307/81
摘要： 1-(BENZOFUR-2-YL)-4-(4'',5''-DISUBSTITUTED-VTRIAZOLE-2''-YL)-PHENYLENES ARE PREPARED BY DIAZOTISING P(BENZOFUR-2-YL)-ANILINES AND (A) COUPLING THE OBTAINED DIAZONIUM COMPOUND WITH A KETONE, REACTING THE OBTAINED HYDROXYLAMINE TO AN OXIMEHYDRAZONE, CLOSING THE V-TRAZOLE RING BY OXIDISING AND REDUCING THE OBTAINED V-TRIAZOLE-1-OXIDE OR (B) COUPLING WITH AN ANILINE OR NAPHTHYLAMINE AND HEATING THE OBTAINED AZO COMPOUND IN THE PRESENCE OF AN OXIDISING AGNET. THE NEW BENZOFURANS ARE USEFUL AS BRIGHTENERS OR ORGANIC HIGH-MOLECULAR MATERIALS.

3. 发明授权

US3862179A 2-stilbenyl-4-styryl-v-triazoles 失效
标题翻译： 2-苯乙烯-4-苯乙烯-V-三唑
公开(公告)号：US3862179A
公开(公告)日：1975-01-21
申请号：US23720472
申请日：1972-03-22
申请人： CIBA GEIGY AG
发明人： KABAS GUGLIELMO , SCHLAEPFER HANS , FLETCHER IAN JOHN
IPC分类号： C09B57/00 , C07D249/06 , C11D3/42 , C07D55/02
CPC分类号： C11D3/42 , C07D249/06
摘要： WHEREIN X1 denotes hydrogen, halogen, methyl or optionally substituted phenyl, R1 denotes hydrogen, halogen, alkyl with 1 to 4 carbon atoms, optionally substituted phenyl or alkoxy with 1 to 4 carbon atoms, or together with R2 in the o-position denotes a fused benzene ring, R2 denotes hydrogen, halogen, alkyl with 1 to 4 carbon atoms or alkoxy with 1 to 4 carbon atoms, or together with R1 in the o-position denotes a fused benzene ring, R3 denotes hydrogen, a nitrile group, an optionally functionally modified sulpho group or an optionally functionally modified carboxyl group, R4 denotes hydrogen, halogen, a nitrile group, alkyl with 1 to 4 carbon atoms, optionally substituted phenyl, alkoxy with 1 to 4 carbon atoms, optionally functionally modified carboxyl or an optionally functionally modified sulpho group and R5 denotes hydrogen, alkyl with 1 to 4 carbon atoms or alkoxy with 1 to 4 carbon atoms. The new compounds are useful as optical brighteners for organic materials.

The present invention relates to new v-triazoles of the formula
摘要翻译：本发明涉及下式的新的v-三唑：其中X 1表示氢，卤素，甲基或任选取代的苯基，R 1表示氢，卤素，具有1至4个碳原子的烷基，任选取代的苯基或具有1至4个碳原子的烷氧基或与o位置的R2一起表示稠合苯环，R 2表示氢，卤素，具有1至4个碳原子的烷基或具有1至4个碳原子的烷氧基，或与o位置的R 1一起表示稠合的苯环，R 3表示氢，腈基，任意官能改性的磺基或任选的官能改性的羧基，R4表示氢，卤素，腈基，具有1至4个碳原子的烷基，任选取代的苯基，烷氧基与1 至4个碳原子，任选功能修饰的羧基或任选的功能修饰的磺基，R 5表示氢，具有1至4个碳原子的烷基或具有1至4个碳原子的烷氧基。

4. 发明授权

US3898234A 4,4{40 -Dinaphthyl-1,1{40 ,8,8{40 -tetracarboxylic acid diimides 失效
标题翻译： 4,4 {40-二萘基-1,1 {40,8,8（40-四羧酸二酰亚胺）
公开(公告)号：US3898234A
公开(公告)日：1975-08-05
申请号：US33016173
申请日：1973-02-06
申请人： CIBA GEIGY AG
发明人： BURDESKA KURT , KABAS GUGLIELMO , PUGIN ANDRE , KORMANY GEZA , ZWEIDLER REINHARD
IPC分类号： C08K5/00 , C07D221/14 , C08K5/3412 , C08K5/41 , C08L1/00 , C08L23/00 , C08L27/00 , C08L67/00 , C08L77/00 , C08L101/00 , C09B57/08 , C07D39/00
CPC分类号： C07D221/14
摘要： New 4,4''-dinaphthyl-1,1'',8,8''-tetracarboxylic acid diimides of the formula

WHEREIN R and R'' independently of one another denote (a) hydrogen, (b) alkyl with 2 to 18 carbon atoms, (c) cycloalkyl containing 5 or 6 ring members and having 5 to 10 carbon atoms, (d) alkyl with 1 to 18 carbon atoms, substituted by hydroxyl, alkoxy with 1 to 12 carbon atoms, optionally halogen-, methyl- or methoxy-substituted phenyl, carboxyl, carbalkoxy with 2 to 13 carbon atoms, carbamoyl optionally substituted at the nitrogen by alkyl with 1 to 12 carbon atoms or phenyl, an optionally quaternised heterocyclic structure with 5 or 6 ring members, wherein 1 to 3 ring members represent nitrogen atoms, the sulpho group or its salts or optionally quaternised dialkylamine with 1 to 12 carbon atoms per alkyl part, (e) optionally halogen-, methyl- or methoxy-substituted phenyl or (f) an optionally quaternised heterocyclic structure with 5 or 6 ring members, wherein 1 to 3 ring members represent nitrogen atoms, and X and X'' independently of one another denote alkoxy with 1 to 4 carbon atoms, or halogen, located in the 3- and 3''-position respectively, Y and Y'' independently of one another denote alkoxy with 1 to 4 carbon atoms, acyloxy with 1 to 4 carbon atoms, benzoyloxy or halogen, located in the 6- and 6''-position respectively, t, u, v and w independently of one another denote the number 1 or 0 and Z and Z'' independently of one another denote hydrogen or the sulpho group or its salts. These compounds are particularly useful as optical brighteners.
摘要翻译：式WHEREIN R和R'彼此独立的新的4,4'-二萘基-1,1'，8,8'-四羧酸二酰亚胺表示（a）氢，（b）具有2至18个碳原子的烷基，（c）含有5或6个环成员并具有5-10个碳原子的环烷基，（d）具有1至18个碳原子的烷基，被羟基取代，具有1至12个碳原子的烷氧基，任选的卤素，甲基或甲氧基 - 具有2至13个碳原子的取代的苯基，羧基，烷氧羰基，在氮下任选被具有1至12个碳原子的烷基取代的氨基甲酰基，或具有5或6个环成员的任选季铵化的杂环结构，其中1至3个环成员表示氮烷基部分具有1至12个碳原子的季铵化二烷基胺，（e）任选卤素，甲基或甲氧基取代的苯基或（f）任选季铵化的具有5或6个环的杂环结构成员，其中1至3个环成员表示氮原子 X和X'彼此独立地表示分别位于3-和3'-位的具有1至4个碳原子的烷氧基或卤素，Y和Y'彼此独立地表示具有1至4个碳原子的烷氧基，酰氧基分别具有1至4个碳原子的苯并氧基或卤素，分别位于6和6'-位，t，u，v和w彼此独立地表示数1或0，Z和Z'彼此独立地表示氢或磺基或其盐。这些化合物特别可用作荧光增白剂。

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