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    • 8. 发明授权
    • Durable flame retardant finishes for textile materials
    • 耐用的阻燃涂料用于纺织材料
    • US4046701A
    • 1977-09-06
    • US660502
    • 1976-02-23
    • Ray E. Smith
    • Ray E. Smith
    • D06M13/44D06M13/02D06M13/144D06M13/21D06M13/224D06M13/236D06M13/244D06M13/282D06M13/285D06M13/322D06M13/325D06M13/328D06M13/33D06M13/332D06M13/338D06M13/345D06M13/35D06M13/355D06M13/358D06M13/364D06M13/402D06M13/432D06M15/673C09K3/28
    • D06M13/236D06M13/21D06M13/285D06M15/673
    • Novel flame retardant finishes comprising a water soluble quaternary phosphonium salt, a water soluble organic nitrogen containing compound, a halophthalate diol, water, and either an organic solvent characterized by having a flash point of at least 80.degree. F. and a boiling point within the range of about 300.degree. to about 350.degree. F. and an emulsifier having a hydrophile lipophile balance value of from about 10 to about 14 or an emulsifying agent which is capable of passing the following three tests: (1) Solubility (Compatability) Test: said emulsifying agent (20 parts by weight) must be soluble in 80 parts by weight of said phosphate ester at less than or equal to 80.degree. C.; (2) Shelf Life Test: a blend of said emulsifying agent and said phosphate ester prepared as in the Solubility Test must remain in one clear homogeneous phase at 22.degree. C. for at least one hour; (3) Finish Formulation Test: a flame retardant finish within the scope of this invention is prepared and must remain in one homogeneous phase for a minimum of one hour at 20.degree. C. These flame retardant finishes are excellent for flame retarding textile materials including polyester/cotton blend fabrics.
    • 新型阻燃整理剂,其包含水溶性季鏻盐,水溶性有机氮化合物,卤代邻苯二甲酸酯二醇,水和有机溶剂,其特征在于闪点至少为80°F,沸点在 范围为约300至约350°F,亲水亲油平衡值为约10至约14的乳化剂或能够通过以下三个试验的乳化剂:(1)溶解度(兼容性)试验: 所述乳化剂(20重量份)在小于或等于80℃时必须溶于80重量份的所述磷酸酯中。 (2)保质期测试:如在溶解度试验中制备的所述乳化剂和所述磷酸酯的共混物必须在22℃下保持在一个清澈的均匀相中至少1小时; (3)精制制剂试验:制备本发明范围内的阻燃整理剂,并且必须在20℃下保持一个均匀相至少1小时。这些阻燃整理剂对于阻燃纺织品(包括聚酯)是优异的 /棉混纺面料。