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1. 发明授权

US4144243A 3-Pyrozolyl-4-triazolyl compounds 失效
标题翻译： 3-苯并噻唑基-4-三唑基化合物
公开(公告)号：US4144243A
公开(公告)日：1979-03-13
申请号：US443722
申请日：1974-02-19
申请人： Alfons Dorlars , Carl-Wolfgang Schellhammer
发明人： Alfons Dorlars , Carl-Wolfgang Schellhammer
IPC分类号： C07D231/16 , C08K5/00 , C07D405/14 , C09K1/02
CPC分类号： C07D231/16 , C08K5/0041
摘要： Coumarine compounds of the formula ##STR1## IN WHICH R.sub.1 and R.sub.2 denote hydrogen, alkyl, cycloalkyl, aralkyl, aryl, nitrile, carboxyl, carboxylic acid ester or carboxylic acid amide groups, or together form a nonaromatic 5-membered or 6-membered ring system, R.sub.3 represents hydrogen, or alkyl or aryl radicals and Hal represents bromine or preferably chlorine as well as their production and use as optical brighteners.
摘要翻译：其中R1和R2表示氢，烷基，环烷基，芳烷基，芳基，腈，羧基，羧酸酯或羧酸酰胺基团，或共同形成非芳香族5元或6元环的芳香化合物系统，R 3表示氢或烷基或芳基，Hal表示溴或优选氯，以及它们的生产和用作荧光增白剂。

2. 发明授权

US3784569A V-triazolyl coumarins 失效
标题翻译： V-TRIAZOLYL COUMARINS
公开(公告)号：US3784569A
公开(公告)日：1974-01-08
申请号：US3784569D
申请日：1968-02-12
申请人： CIBA GEIGY AG
发明人： KIRCHMAYR R , RODY J , HELLER H
IPC分类号： C08K5/3472 , C08K5/3475 , C09B57/02 , D01F1/06 , D01F1/10 , C07D405/04 , C09K1/02
CPC分类号： D01F1/06 , C08K5/3472 , C08K5/3475
摘要： 3-ARYL-7-(V-TRIAZOLYL)-COUMARINS IN WHICH THE TRIAZOLYL MOIETY IS OF THE FORMULA

4,5-(-A-)-2H-1,2,3-TRIAZOL-2-YL

AND A REPRESENTS AN OPTIONALLY ALKYL-SUBSTITUTED TETRAMETHYLENE GROUP OR AN OPTIONALLY ALKYL-SUBSTITUTED O,WPHENYLMETHYLENE OR O-W-PHENYLETHYLENE GROUP THE BENZENE RING OF WHICH MAY BE NON-CHROMOGENICALLY SUBSTITUTED, ARE USEFUL AS OPTICAL BRIGHTENERS FOR A GREAT VARIETY OF ORGANIC MATERIALS, E.G. NYLON, POLYETHYLENE GLYCOL TYPE POLYESTER, POLYAMIDE, CELLULOSIC FIBER MATERIALS, AND THE LIKE. A METHOD FOR OPTICALLY BRIGHTENING SUCH ORGANIC MATERIALS, WITH THE AID OF THE NEW COMPOUNDS, AND COMPOSITIONS, ESPECIALLY DETERGENT COMPOSITIONS, CONTAINING THEM HAS OPTICALLY BRIGHTENING INGREDIENTS, ARE ALSO DESCRIBED.

3. 发明授权

US3766061A Decorative iridescent compositions 失效
标题翻译：装饰性摄影组合物
公开(公告)号：US3766061A
公开(公告)日：1973-10-16
申请号：US3766061D
申请日：1971-09-20
申请人： DU PONT
发明人： MAHLER W , PANAR M
IPC分类号： A61K8/63 , A61Q3/02 , B44F1/14 , C09D5/36 , C09K19/36 , A61K7/02 , B44D5/06 , C09K1/02
CPC分类号： C09D5/36 , A61K8/63 , A61K2800/436 , A61Q3/02 , B44F1/14 , C09K19/36 , Y10T428/26
摘要： SOLID COMPOSITIONS HAVING CHOLESTERIC PROPERTIES, PARTICULARLY IRIDESCENCE ARE MADE BY ITIMATELY MIXING ESTERS OF CHOLESTEROL OR CHOLESTEROL-LIKE STEROLS, BY MELT OR SOLUTION METHODS. THE ESTER INCLUDE A SUBSTANTIAL PROPORTION OF HYDROGEN PHTHALATE ESTERS. THE REMAINING ESTERS PREFERABLY CONTAIN A CARBOCYCLIC RING. STEROLS OR STEROL 3BHALIDES CAN ALSO BE PRESENT IN THE MIXTURE. IF CINNAMATE ESTERS ARE EMPLOYDED ALL OR PART OF THE HYDROGEN PHTHALATE ESTERS CAN BE REPLACED WITH HYDROGEN ISOPHTHALATE ESTERS. THE COMPOSITIONS ARE USEFUL FOR DECORATIVE COATINGS.

4. 发明授权

US3753921A Novel daylight fluorescent pigments and process for preparing them 失效
标题翻译：新型日光荧光颜料及其制备方法
公开(公告)号：US3753921A
公开(公告)日：1973-08-21
申请号：US3753921D
申请日：1972-01-31
申请人： HOECHST AG
发明人： NOETZEL S , FISCHER E
IPC分类号： C09D5/22 , C09K11/06 , C09K1/02
CPC分类号： C09K11/06 , C09D5/22
摘要： NEW DAYLIGHT FLUORESCENT PIGMENTS WHICH CONTAIN AN ORGANIC FLUORESCENT DYESTUFF AND AS RESIN A CONDENSATION RESIN, CONSISTING OF COPOLYMERIZATES OF OLEFINICALLY UNSATURATED COMPOUNDS CONTAINING EPOXY GROUPS AND HENCE COPOLYMERIZABLE VINYL COMPOUNDS WHICH ARE CROSS-LINKED WITH DI- OR POLYCARBOXYLIC ACIDS OR THE ANYDRIDES THEREOF AND A PROCESS FOR THEIR PREPARATION WHICH COMPRISES INCORPORATING THE ORGANIC FLURRESCENT DYESTUFF INTO THE CONDENSATION RESIN. THESE DAYLIGHT FLURESCENT PIGMENTS MAY BE EMPLOYED FOR PREPARING FLURESCENT PAINTS, FOR EXAMPLE AIR-AIR-DRYING LACQUERS ON THE BASIS OF AKYL RESIN OR PHYSICALLY DRYING LACQUERS ON THE BASIS OF ACRYLIC RESINS, AS WELL AS FOR PREPARING FLURESCENT PRINTING INKS SUCH AS INKS FOR SCREEN PRINTING INTAGLIO PRINTING, BOOK PRINTING AND OFFSET-LITHO PRINTING. DE TO THEIR HIGH RESISTANCE TO HEAT, THEY ARE PARTICULARLY SUITABLE FOR FLUORESCENT DYEING OF PLASTICS AND ENAMELS.

5. 发明授权

US3741907A Fluorescent pigments having an isocyanate resin base 失效
标题翻译：具有异氰酸酯树脂基质的荧光颜料
公开(公告)号：US3741907A
公开(公告)日：1973-06-26
申请号：US3741907D
申请日：1971-03-16
申请人： GIEGLE G & CO GMBH
发明人： BEYERLIN H
IPC分类号： C08G18/32 , C08G18/38 , C08G18/73 , C08G18/75 , C08K5/00 , C09K1/00 , C09K1/02
CPC分类号： C08G18/75 , C08G18/3203 , C08G18/3855 , C08G18/3861 , C08G18/73 , C08K5/0041 , C08L75/00
摘要： BRITTLE RESINS SUITABLE AS BASES FOR FLUORESCENT PIGMENTS ARE PREPARED FROM DIISOCYANATES BY POLYADDITION REACTIONS WITH SULFONAMIDES AND/OR POLYOLS. THE COLORING MATTER MAY BE DISPERSED IN THE POLYMERIZATION MIXTURE OF THE COMMINUTED RESINS MAY BE DYED IN AN ACID DYE BATH. THE RESINS ARE READILY PULVERIZED, RESIST ELEVATED TEMPERATURES WITHOUT SOFTENING OR DECOMPOSING, AND ARE INSOLUBLE OR PARACTICALLY INSOLUBLE IN THE SOLVENTS USUALLY EMPLOYED IN MAKING ORGANIC COATING COMPOSITIONS AND INKS.

6. 发明授权

US3690947A Process for the optical brightening of fibrous materials made from polyacrylonitrile 失效
标题翻译：从聚丙烯酸酯制成的纤维材料的光学加工方法
公开(公告)号：US3690947A
公开(公告)日：1972-09-12
申请号：US3690947D
申请日：1970-01-21
申请人： HOECHST AG
发明人： ROSCH GUNTER , LINKE WERNER , SMERZ OTTO , SCHINZEL ERICH
IPC分类号： C09B57/00 , C07D231/06 , D06L3/12 , D06M13/35 , C09K1/02
CPC分类号： C07D231/06 , D06L4/679 , D06M13/35
摘要： FIBROUS MATERIALS MADE OF POLYMERS CONTAINING AT LEAST 85% OF POLYACRYLATONITRILE CAN BE OPTICALLY BRIGHTENED IN A SAID MATERIAL WITH A LIQUOR CONTAINING A 1-(4''-B-ALKOXYETHYL SULFONYL)-PHENYL-3-B-CHLOROPHENYL-$2-PYRAZOLINE, ADJUSTING THE IMPREGNATED MATERIAL TO A LIQUOR CONTENT OF ABOUT 5 TO 120% BY WEIGHT REFERRED TO THE DRY-WEIGHT OF THE GOODS, AND HEATING IT FOR ABOUT 2 SECONDS TO 30 MINUTES TO A TEMPERATURE OF ABOUT 100 TO 150*C.
摘要翻译： 1288545荧光增白FARBWERKE HOECHST AG 19 Jan 1970 [30 Jan 1969] 4340/70标题DIP包含至少85％的聚丙烯腈的聚合物的纤维材料通过用含有通式光亮剂的液体浸渍材料进行光学增白，其中A代表支链或非支链C 2-4亚烷基，R SP 1表示C 1-4烷基，R SP 2表示C 1-4烷基或两个基团 R 2 与氮原子一起形成饱和杂环，X表示无色阴离子，n为1或2，将材料的液体含量调整为参考材料的5-120重量％并在100 <-150℃下加热，优选用蒸汽加热2秒至30分钟。如果亮面织物要立即印刷，则优选在50 <-150℃进行中间干燥。添加增稠剂例如淀粉醚，黄蓍胶，角豆粉和结晶胶，以防止在干燥过程中荧光增白剂的迁移。当增亮液中加入脂肪酸和氧乙基化氨的非离子缩合产物和/或脂肪酸和低分子量脂肪族多胺的季
缩合产物时，可实现增强的增亮。其中A，R 1，R 2，X和n具有上述含义的通式的第二增白剂显示绿蓝色荧光，并且当应用时与式II化合物的混合物，以补偿后者的淡红色。

7. 发明授权

US3679447A Tetravinyl-vinyl monomer paint composition and painting process 失效
标题翻译：四烯乙烯单体漆组合物和涂料工艺
公开(公告)号：US3679447A
公开(公告)日：1972-07-25
申请号：US3679447D
申请日：1969-08-04
申请人： FORD MOTOR CO
发明人： ARONOFF ELIHU , LABANA SANTOKH S
IPC分类号： C07C69/54 , B05D7/24 , C08F2/00 , C08F2/46 , C08F2/54 , C08F20/16 , C08F290/00 , C08F290/06 , C08F291/00 , C08F299/00 , C08F299/02 , C09D4/06 , C09D171/00 , C09K1/02
CPC分类号： B05D7/24 , C08F2/46 , C08F20/16 , C08F290/064 , C08F291/00 , C08F299/026 , C09D4/06 , Y10S106/901 , Y10T428/31855 , C08F220/20
摘要： (CH2=C(-CH3)-COO-CH(-CH2-OOC-C(-CH3)=CH2)-CH2-O-(1,4-

PHENYLENE))2-C(-CH3)2

A SUBSTRATE IS COATED WITH A FILM-FORMING COMPOSITION CONSISTING ESSENTIALLY OF VINYL MONOMERS AND A UNIQUE TETRAVINYL COMPOUND AND THE COATING IS CONVERTED TO A TENACIOUSLY ADHERING, SOLVENT-RESISTANT, WEAR AND WEATHERRESISTANT COATING BY EXPOSING THE COATED SUBSTRATE TO IONIZING RADIATION, PREFERABLY IN THE FORM OF AN ELECTRON BEAM. THIS TETRAVINYL COMPOUND IS FORMED BY FIRST REACTING A DIEPOXIDE WITH ACRYLIC ACID AND/OR METHACRYLIC ACID AND SUBSEQUENTLY REACTING THE RESULTANT ESTER ECONDENSATION PRODUCT WITH A VINYL UNSATURATED ACYL HALIDE.

8. 发明授权

US3676360A Liquid scintillators 失效
标题翻译：液体扫描仪
公开(公告)号：US3676360A
公开(公告)日：1972-07-11
申请号：US3676360D
申请日：1971-06-30
申请人： ADIL E SHAMOO
发明人： SHAMOO ADIL E
IPC分类号： G01T1/204 , G01T1/20 , C09K1/02
CPC分类号： G01T1/2042
摘要： The counting efficiency of liquid scintillators containing toluene as the solvent for a primary solute or activator and for a secondary solute or spectrum shifter is improved, particularly in the presence of water, for example, when the isotope to be detected is an aqueous solution, by adding to the liquid scintillator a hygroscopic substance which is soluble in toluene in an amount sufficient to absorb and/or emulsify the water that is present. Such hygroscopic additive is preferably cellulosic and may be selected from the group consisting of cellulose, carboxymethyl cellulose, cellulose phosphate, diethylaminoethyl cellulose, benzyl diethylaminoethyl cellulose and epichlorohydrin triethanolamine cellulose. The additive for improving the counting efficiency may advantageously include, apart from the cellulose and/or cellulose derivative, a small amount of sodium or calcium carbonate or bicarbonate. The improvement in counting efficiency resulting from the mentioned addition is particularly large when the scintillators liquid includes alcohol as well as toluene.
摘要翻译：含有甲苯作为一级溶质或活化剂和二级溶质或光谱移动剂的溶剂的液体闪烁体的计数效率得到改善，特别是在水的存在下，例如当待检测的同位素是水溶液时，由向液体闪烁体中加入可溶于甲苯的吸湿物质，其量足以吸收和/或乳化存在的水。这种吸湿添加剂优选为纤维素，并且可以选自纤维素，羧甲基纤维素，磷酸纤维素，二乙基氨基乙基纤维素，苄基二乙基氨基乙基纤维素和表氯醇三乙醇胺纤维素。除了纤维素和/或纤维素衍生物外，用于提高计数效率的添加剂可以有利地包括少量的碳酸钙或碳酸钙或碳酸钙。当闪烁体液体包括醇以及甲苯时，由所述添加产生的计数效率的改善特别大。

9. 发明授权

US3669896A Inorganic white pigments containing optical brighteners and process for their manufacture 失效
标题翻译：含有光学增亮剂的无机白色及其制造方法
公开(公告)号：US3669896A
公开(公告)日：1972-06-13
申请号：US3669896D
申请日：1969-12-02
申请人： CIBA GEIGY AG
发明人： PREININGER ERICH , GING DIETER
IPC分类号： C08K13/02 , C09C1/06 , C09C1/36 , C09C3/00 , D21H17/69 , C09K1/02
CPC分类号： D21H17/69 , C01P2002/52 , C08K13/02 , C09C1/06 , C09C1/3661 , C09C3/006 , C09C3/063 , C09C3/08
摘要： The invention concerns a process for the manufacture of inorganic white pigments containing optical brighteners, characterized in that, in an aqueous suspension of an inorganic white pigment which contains a dispersion of at least one optical brightener which is sparingly soluble in water, dispersed by means of non-ionic surface-active agents, property-improving auxiliary substances for such pigments are precipitated or adsorbed on these pigments in a manner which is in itself known by admixing the property-improving auxiliary or admixing the components for the formation of such a property-improving auxiliary if several components for its formation are necessary, and the pigments treated in such manner are separated from the aqueous phase, washed and dried. The invention provides a valuable method for homogeneously distributing optical brightening agents in combination with white pigments in plastics.
摘要翻译：本发明涉及一种制造含有荧光增白剂的无机白色颜料的方法，其特征在于在无机白色颜料的水性悬浮液中，其含有至少一种微溶于水的荧光增白剂的分散体，其通过以下方式分散：非离子表面活性剂，用于这些颜料的性能改进助剂为这些颜料的沉淀或吸附，其本身是通过混合改性助剂或混合用于形成这种性能的助剂，如果需要形成几种成分，则改善助剂，并且以这种方式处理的颜料与水相分离，洗涤并干燥。本发明提供了将荧光增白剂与塑料中的白色颜料组合均匀分布的有价值的方法。

10. 发明授权

US3658833A Benzofurans 失效
标题翻译： BENZOFURANS
公开(公告)号：US3658833A
公开(公告)日：1972-04-25
申请号：US3658833D
申请日：1970-06-15
申请人： CIBA GEIGY AG
发明人： KABAS GUGLIELMO , SCHLAPFER HANS
IPC分类号： C07C205/35 , C07D307/81 , C07D405/10 , C09B43/06 , C11D1/00 , D06L3/12 , D06M13/10 , D06M13/358 , C07D99/04 , C09K1/02
CPC分类号： C09B43/06 , C07C205/44 , C07D307/81
摘要： 1-(BENZOFUR-2-YL)-4-(4'',5''-DISUBSTITUTED-VTRIAZOLE-2''-YL)-PHENYLENES ARE PREPARED BY DIAZOTISING P(BENZOFUR-2-YL)-ANILINES AND (A) COUPLING THE OBTAINED DIAZONIUM COMPOUND WITH A KETONE, REACTING THE OBTAINED HYDROXYLAMINE TO AN OXIMEHYDRAZONE, CLOSING THE V-TRAZOLE RING BY OXIDISING AND REDUCING THE OBTAINED V-TRIAZOLE-1-OXIDE OR (B) COUPLING WITH AN ANILINE OR NAPHTHYLAMINE AND HEATING THE OBTAINED AZO COMPOUND IN THE PRESENCE OF AN OXIDISING AGNET. THE NEW BENZOFURANS ARE USEFUL AS BRIGHTENERS OR ORGANIC HIGH-MOLECULAR MATERIALS.

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