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1. 发明授权

US07473658B2 Partially fluorinated amino acid derivatives as gelling and surface active agents 失效
标题翻译：部分氟化氨基酸衍生物作为胶凝剂和表面活性剂
公开(公告)号：US07473658B2
公开(公告)日：2009-01-06
申请号：US11598293
申请日：2006-11-13
申请人： Erick Jose Acosta , Anilkumar Raghavanpillai , Sheng Peng , Stefan Reinartz , Sunti Moudgil
发明人： Erick Jose Acosta , Anilkumar Raghavanpillai , Sheng Peng , Stefan Reinartz , Sunti Moudgil
IPC分类号： B32B5/02 , C08L27/12
CPC分类号： D21H17/11 , C04B41/4842 , D06M13/236 , D06M13/372 , D06M13/408 , D06M13/419 , D06M13/428 , D06M13/432 , D06M13/513 , D06M2200/11 , D06M2200/12 , D21H21/16 , Y10T428/249981 , Y10T442/2139 , Y10T442/2279 , Y10T442/2287
摘要： Disclosed are partially fluorinated amino acid derivatives useful as organogelators and surface treatment materials to provide oil- and water-repellency properties to substrates. Also disclosed are composite materials, comprising a porous support and a porous nanoweb. The porous nanoweb contains fibrous structures of about 10 nm to about 1000 nm effective average fiber diameter as determined with electron microscopy.
摘要翻译：公开了部分氟化的氨基酸衍生物，其可用作有机凝胶和表面处理材料，以为基材提供防油和拒水性能。还公开了包含多孔载体和多孔纳米网的复合材料。多孔纳米纤维网包含用电子显微镜测定的约10nm至约1000nm有效平均纤维直径的纤维结构。

2. 发明授权

US07842626B2 Partially fluorinated compositions and surface active agents 失效
标题翻译：部分氟化组合物和表面活性剂
公开(公告)号：US07842626B2
公开(公告)日：2010-11-30
申请号：US11598407
申请日：2006-11-13
申请人： Erick Jose Acosta , Anilkumar Raghavanpillai , Sheng Peng , Stefan Reinartz
发明人： Erick Jose Acosta , Anilkumar Raghavanpillai , Sheng Peng , Stefan Reinartz
IPC分类号： B32B5/02 , C08L27/12
CPC分类号： C07C237/22 , C07C271/22 , C07C275/08 , C07C275/30 , Y10T428/31725 , Y10T442/2189 , Y10T442/2213 , Y10T442/2221 , Y10T442/2262 , Y10T442/2287
摘要： Partially fluorinated amino acid derivatives are provided that are useful as organogelators and surface treatment materials to provide oil- and water- repellency properties to substrates. Also provided are composite materials comprising a porous support and a porous nanoweb. The porous nanoweb contains fibrous structures of about 10 nm to about 1000 nm effective average fiber diameter.
摘要翻译：提供部分氟化的氨基酸衍生物，其可用作有机凝胶剂和表面处理材料，以为基材提供防油和防水性能。还提供了包含多孔载体和多孔纳米网的复合材料。多孔纳米纤维网含有约10nm至约1000nm有效平均纤维直径的纤维结构。

3. 发明申请

US20080113573A1 Partially fluorinated amino acid derivatives as gelling and surface active agents 失效
标题翻译：部分氟化氨基酸衍生物作为胶凝剂和表面活性剂
公开(公告)号：US20080113573A1
公开(公告)日：2008-05-15
申请号：US11598293
申请日：2006-11-13
申请人： Erick Jose Acosta , Anilkumar Raghavanpillai , Sheng Peng , Stefan Reinartz , Suniti Moudgil
发明人： Erick Jose Acosta , Anilkumar Raghavanpillai , Sheng Peng , Stefan Reinartz , Suniti Moudgil
IPC分类号： C08F8/00 , B32B5/18
CPC分类号： D21H17/11 , C04B41/4842 , D06M13/236 , D06M13/372 , D06M13/408 , D06M13/419 , D06M13/428 , D06M13/432 , D06M13/513 , D06M2200/11 , D06M2200/12 , D21H21/16 , Y10T428/249981 , Y10T442/2139 , Y10T442/2279 , Y10T442/2287
摘要： Disclosed are partially fluorinated amino acid derivatives useful as organogelators and surface treatment materials to provide oil- and water-repellency properties to substrates. Also disclosed are composite materials, comprising a porous support and a porous nanoweb. The porous nanoweb contains fibrous structures of about 10 nm to about 1000 nm effective average fiber diameter as determined with electron microscopy.
摘要翻译：公开了部分氟化的氨基酸衍生物，其可用作有机凝胶和表面处理材料，以为基材提供防油和拒水性能。还公开了包含多孔载体和多孔纳米网的复合材料。多孔纳米纤维网包含用电子显微镜测定的约10nm至约1000nm有效平均纤维直径的纤维结构。

4. 发明申请

US20080113172A1 Partially fluorinated compositions and surface active agents 失效
标题翻译：部分氟化组合物和表面活性剂
公开(公告)号：US20080113172A1
公开(公告)日：2008-05-15
申请号：US11598407
申请日：2006-11-13
申请人： Erick Jose Acosta , Anilkumar Raghavanpillai , Sheng Peng , Stefan Reinartz
发明人： Erick Jose Acosta , Anilkumar Raghavanpillai , Sheng Peng , Stefan Reinartz
IPC分类号： B32B5/18 , C07C233/00 , C07D249/04
CPC分类号： C07C237/22 , C07C271/22 , C07C275/08 , C07C275/30 , Y10T428/31725 , Y10T442/2189 , Y10T442/2213 , Y10T442/2221 , Y10T442/2262 , Y10T442/2287
摘要： Partially fluorinated amino acid derivatives are provided that are useful as organogelators and surface treatment materials to provide oil- and water-repellency properties to substrates. Also provided are composite materials comprising a porous support and a porous nanoweb. The porous nanoweb contains fibrous structures of about 10 nm to about 1000 nm effective average fiber diameter.
摘要翻译：提供部分氟化的氨基酸衍生物，其可用作有机凝胶剂和表面处理材料以提供对基材的拒油和拒水性能。还提供了包含多孔载体和多孔纳米网的复合材料。多孔纳米纤维网含有约10nm至约1000nm有效平均纤维直径的纤维结构。

5. 发明授权

US07385077B1 Fluoroalkyl surfactants 失效
标题翻译：氟烷基表面活性剂
公开(公告)号：US07385077B1
公开(公告)日：2008-06-10
申请号：US11728832
申请日：2007-03-27
申请人： Erick Jose Acosta , Stefan Reinartz
发明人： Erick Jose Acosta , Stefan Reinartz
IPC分类号： C07C229/00 , B01F17/36
CPC分类号： B01F17/0035 , C07C229/08 , C07C229/12 , C07C229/24 , C08K5/17
摘要： Surfactants of formula (I) wherein each R is independently hydrogen or a C1 to C4 alkyl group; A is independently hydrogen or —C(O)—O—B; Ro is a linear, branched or cyclic aliphatic group, or combination thereof, having from about 2 to about 100 carbon atoms, interrupted or substituted by 1 to about 50 hydrophilic groups, said hydrophilic groups selected from the group consisting of hydroxyl, amino, ether and mixtures thereof; wherein specific ratios of and bonding of hydrophilic groups to carbon atoms is required; each B is independently of specific formulae containing perfluoroalkyl and —S(CH2)t—, and m, d, n, and t are 0 or integers with specific limitations.
摘要翻译：式（I）的表面活性剂，其中每个R独立地为氢或C 1至C 4烷基; A独立地是氢或-C（O）-O-B; R 2是具有约2至约100个碳原子的直链，支链或环状脂族基团或其组合，被1至约50个亲水基团间隔或取代，所述亲水基团选自由羟基，氨基，醚及其混合物组成的组; 其中需要亲水基团与碳原子的特定比例和键合; 每个B独立于含有全氟烷基和-S（CH 2）n - 的具体式，m，d，n和t为0或具有特定限制的整数。

6. 发明授权

US07638589B2 Triazole-containing fluorocarbon-grafted polysiloxanes 失效
标题翻译：含三氟乙烯的氟碳接枝聚硅氧烷
公开(公告)号：US07638589B2
公开(公告)日：2009-12-29
申请号：US11311077
申请日：2005-12-19
申请人： Erick Jose Acosta , Axel Hans-Joachim Herzog , Martial Jean-Jacques Pabon
发明人： Erick Jose Acosta , Axel Hans-Joachim Herzog , Martial Jean-Jacques Pabon
IPC分类号： C08G77/08
CPC分类号： C08G77/26 , C08G77/24 , C08G77/388 , Y10T428/31663
摘要： A polymer for imparting repellency and stain resistance to substrates is disclosed of Formula 1: (W)a(R2)bSi(R1)2—O—[Si(R1)2—O]n—[Si(W)c(R1)d(R2)e—O]m—Si(R1)2—(W)f(R2)g 1 wherein: a, b, c, d, e, f and g are each independently 0 or 1, provided that (a+b) is 1, (f+g) is 1, and (c+d+e) is 2, each R1 is a C1 to C8 alkyl, each R2 is independently H or C1 to C8 alkyl, optionally containing oxygen, nitrogen, or sulfur, or a combination thereof, and n=0 to 500, m=1 to 100, each W is independently (Rf—X—A—X)p—Y—X— wherein: Rf is a straight or branched perfluoroalkyl group having from about 2 to about 20 carbon atoms, or a mixture thereof, which is optionally interrupted by at least one oxygen atom, each X is independently an organic divalent linking group having from about 1 to about 20 carbon atoms, optionally containing oxygen, nitrogen, or sulfur, or a combination thereof, A is a 1,2,3-triazole, p=1 to 2, Y is O, N, or NR wherein R is H or C1 to C20 alkyl, optionally containing oxygen, nitrogen, or sulfur, or a combination thereof.
摘要翻译：式（1）公开了：（W）a（R2）bSi（R1）2-O- [Si（R1）2-O] n- [Si（W）c（R1））d（R2）eO] m-Si（R1）2-（W）f（R2）g1其中：a，b，c，d，e，f和g各自独立地为0或1，条件是（a + b）为1，（f + g）为1，（c + d + e）为2，每个R 1为C 1至C 8烷基，每个R 2独立地为H或C 1至C 8烷基，任选地含有氧，氮，或硫，或其组合，n = 0〜500，m = 1〜100，各W独立地为（Rf-XAX）pYX-，其中：Rf为直链或支链的全氟烷基，其具有约2至约20 碳原子或其混合物，其任选被至少一个氧原子间隔，每个X独立地为具有约1至约20个碳原子的有机二价连接基团，任选地含有氧，氮或硫，或组合其中A为1,2,3-三唑，p = 1至2，Y为O，N或NR，其中R为H或C 1至C 20烷基，任选含有氧，硝基烯或硫，或其组合。

7. 发明申请

US20090038510A1 Mixed fluoroalkyl-alkyl surfactants 有权
标题翻译：混合氟代烷基 - 烷基表面活性剂
公开(公告)号：US20090038510A1
公开(公告)日：2009-02-12
申请号：US11890414
申请日：2007-08-06
申请人： Erick Jose Acosta , Charles Kenneth Taylor
发明人： Erick Jose Acosta , Charles Kenneth Taylor
IPC分类号： C07F9/06 , C09D5/00
CPC分类号： C07F9/091 , C11D1/004 , C11D1/345
摘要： A compound of Formula 1 Rf-A-OP(O)(O−M+)(O—RH) Formula 1 wherein Rf is a C2 to C6 linear or branched perfluoroalkyl optionally interrupted by one, two or three ether oxygen atoms; A is (CH2CF2)m(CH2)n—, (CH2)oSO2N(CH3)(CH2)p—, O(CF2)q(CH2)r—, or OCHFCF2OE-;m is 1 to 4; n, o, p, and r are each independently 2 to 20; q is 2;E is a C2 to C20 linear or branched alkyl group optionally interrupted by oxygen, sulfur, or nitrogen atoms; a cyclic alkyl group, or a C6 to C10 aryl group;M is a Group I metal or an ammonium cation (NHxR2y)+ wherein R2 is a C1 to C4 alkyl, x is 1 to 4, y is 0 to 3 and x+y is 4; andRH is a C1 to C20 linear, branched, or cyclic alkyl, or a C6 to C10 aryl, and its use as a surfactant is disclosed.
摘要翻译：式1化合物<？in-line-formula description =“In-line Formulas”end =“lead”→Rf-A-OP（O）（O-M +）（O-RH） -line-formula description =“In-line Formulas”end =“tail”？>其中Rf是任选被一个，两个或三个醚氧原子间隔的C2至C6直链或支链全氟烷基; A是（CH 2 CF 2）m（CH 2）n - ，（CH 2）o SO 2 N（CH 3）（CH 2）p - ，O（CF 2）q（CH 2）r - 或OCHFCF 2 OE-; m为1〜4; n，o，p和r各自独立地为2〜20; q是2; E是任选被氧，硫或氮原子间隔的C2至C20直链或支链烷基; 环状烷基或C6〜C10芳基; M为I族金属或铵阳离子（NH x R 2y）+，其中R 2为C 1至C 4烷基，x为1至4，y为0至3，x + y为4; 并且RH是C1至C20直链，支链或环状烷基或C6至C10芳基，并且其用作表面活性剂。

8. 发明授权

US08263670B2 Mixed fluoroalkyl-alkyl surfactants 有权
标题翻译：混合氟代烷基 - 烷基表面活性剂
公开(公告)号：US08263670B2
公开(公告)日：2012-09-11
申请号：US11890414
申请日：2007-08-06
申请人： Erick Jose Acosta , Charles Kenneth Taylor
发明人： Erick Jose Acosta , Charles Kenneth Taylor
IPC分类号： B01D12/00 , B01F17/14 , C09D5/00 , C09D7/06 , C09D7/12 , C07F9/09 , C09K3/18 , C11D1/34 , C08L21/02 , C09D201/00
CPC分类号： C07F9/091 , C11D1/004 , C11D1/345
摘要： A compound of Formula 1 Rf-A-OP(O)(O−M+)(O—RH) Formula 1 wherein Rf is a C2 to C6 linear or branched perfluoroalkyl optionally interrupted by one, two or three ether oxygen atoms; A is (CH2CF2)m(CH2)n—, (CH2)oSO2N(CH3)(CH2)p—, O(CF2)q(CH2)r—, or OCHFCF2OE-; m is 1 to 4; n, o, p, and r are each independently 2 to 20; q is 2; E is a C2 to C20 linear or branched alkyl group optionally interrupted by oxygen, sulfur, or nitrogen atoms; a cyclic alkyl group, or a C6 to C10 aryl group; M is a Group I metal or an ammonium cation (NHxR2y)+ wherein R2 is a C1 to C4 alkyl, x is 1 to 4, y is 0 to 3 and x+y is 4; and RH is a C1 to C20 linear, branched, or cyclic alkyl, or a C6 to C10 aryl, and its use as a surfactant is disclosed.
摘要翻译：式1的化合物Rf-A-OP（O）（O-M +）（O-RH）式1其中Rf是任选被一个，两个或三个醚氧原子间隔的C2至C6直链或支链全氟烷基; A是（CH 2 CF 2）m（CH 2）n - ，（CH 2）o SO 2 N（CH 3）（CH 2）p - ，O（CF 2）q（CH 2）r - 或OCHFCF 2 OE-; m为1〜4; n，o，p和r各自独立地为2〜20; q是2; E是任选被氧，硫或氮原子间隔的C2至C20直链或支链烷基; 环状烷基或C6〜C10芳基; M为I族金属或铵阳离子（NH x R 2y）+，其中R 2为C 1至C 4烷基，x为1至4，y为0至3，x + y为4; 并且RH是C1至C20直链，支链或环状烷基或C6至C10芳基，并且其用作表面活性剂。

9. 发明申请

US20090042996A1 Mixed fluoroalkyl-alkyl surfactants 有权
标题翻译：混合氟代烷基 - 烷基表面活性剂
公开(公告)号：US20090042996A1
公开(公告)日：2009-02-12
申请号：US11890395
申请日：2007-08-06
申请人： Charles Kenneth Taylor , Michael Joseph Michalczyk , Erick Jose Acosta
发明人： Charles Kenneth Taylor , Michael Joseph Michalczyk , Erick Jose Acosta
IPC分类号： A61K31/045 , A61K31/66 , C07C309/63 , C07C31/125 , C07C311/01 , C07C69/00 , C07F7/02 , C07F9/02 , C09G1/06 , C09K13/00 , C09K3/00 , C11D1/00 , C11D1/04 , C11D1/34 , C11D3/20
CPC分类号： C07C69/675 , C07C43/137 , C07C309/65 , C07F7/0838 , C07F7/1804 , C07F9/091 , C11D1/004
摘要： A surfactant of formula 1 (Rf-A)a-Q-([B]k—R)b Formula 1 wherein a and b are each independently 1 or 2; Rf is a linear or branched perfluoroalkyl radical having from 2 to about 20 carbon atoms, optionally interrupted with at least one oxygen; R is a C1 to C20 linear, branched or cyclic alkyl, or a C6 to C10 aryl; B is —(CH2CHR1O)x—, k is 0 or 1, x is 1 to about 20, A is —(CH2)m[(CHR1CH2O)]s—[(CH2)m(CH)tCHOH(CH2)m]e—, wherein each m is independently 0 to 3, s is 0 to about 30, t is 0 or 1, and e is 0 or 1, R1 is H or CH3, Q is: —OP(O)(O−M+)(O)—, —O—, —S—(CH2)m—C(O)—O—, —SO2—O— —CH2CH2O—C(O)CH2C(OH)(V)CH2C(O)O—; —(CH2CH2O)xCH2CH(OH)—(CH2CH2O)x—(CH2)m—Si[OSi(R2)3]2—, —SO2NR2—, —(CH2CH2O)zC(O)CH(SO3−M+)CH2C(O)(OCH2CH2)z— wherein z is 1 to about 15, or a bond when s is a positive integer, V is —C(O)OR3 and R3 is H, CH3 or Rf; R2 is C1 to C4 alkyl, and M+ is a Group 1 metal or an ammonium (NHxR2y)+ cation wherein x+y=4, and R2 is C1 to C4 alkyl, provided that when Q is —OP(O)(O−M+)(O)— or when Q is —(CH2CH2O)z—C(O)CH(SO3−M+)CH2C(O)(OCH2CH2)z—, then at least one of s or e is a positive integer.
摘要翻译：（Rf-A）aQ - （[B] kR）b式1 <？在线公式“=”在线公式“end =”lead“ description =“In-line Formulas”end =“tail”？>其中a和b各自独立地为1或2; Rf是具有2至约20个碳原子的直链或支链全氟烷基，任选被至少一个氧中断; R为C1至C20直链，支链或环状烷基或C6至C10芳基; B是 - （CH 2 CHR 1 O）x - ，k是0或1，x是1至约20，A是 - （CH 2）m [（CHR 1 CH 2 O）] s - [（CH 2）m（CH）t CHOH（CH 2）m] e-，其中每个m独立地为0至3，s为0至约30，t为0或1，e为0或1，R 1为H或CH 3，Q为：-OP（O）（O-M + ）（O） - ， - O - ， - S-（CH 2）m C（O）-O-，-SO 2 -O-CH 2 CH 2 O-C（O）CH 2 C（OH）（V）CH 2 C（O） - （CH2CH2O）xCH2CH（OH） - （CH2CH2O）x-（CH2）m-Si [OSi（R2）3] 2-，-SO2NR2-， - （CH2CH2O）zC（O）CH（SO3-M +）CH2C O）（OCH 2 CH 2）z - ，其中z为1至约15，或当s为正整数时为键，V为-C（O）OR 3且R 3为H，CH 3或R f; R2是C1-C4烷基，M +是1价金属或铵（NHxR2y）+阳离子，其中x + y = 4，R2是C1-C4烷基，条件是当Q是-OP（O） M +）（O） - 或Q为 - （CH 2 CH 2 O）z C（O）CH（SO 3 -M +）CH 2 C（O）（OCH 2 CH 2）z - 时，则s或e中的至少一个为正整数。

10. 发明申请

US20100267843A1 MIXED FLUOROALKYL-ALKYL SURFACTANTS 有权
标题翻译：混合的氟代烷基磺酸酯表面活性剂
公开(公告)号：US20100267843A1
公开(公告)日：2010-10-21
申请号：US12758280
申请日：2010-04-12
申请人： Charles Kenneth Taylor , Michael Joseph Michalczyk , Erick Jose Acosta
发明人： Charles Kenneth Taylor , Michael Joseph Michalczyk , Erick Jose Acosta
IPC分类号： A61K47/08 , C09G1/02 , C08K5/52 , C11D3/36 , C09D11/02 , C09G1/00 , B01F17/14 , C25D3/02 , C09K13/00 , C12N1/00 , D21H23/76 , C09K3/00
CPC分类号： C07C69/675 , C07C43/137 , C07C309/65 , C07F7/0838 , C07F7/1804 , C07F9/091 , C11D1/004
摘要： A surfactant of formula 1 (Rf-A)a-Q-([B]k—R)b Formula 1 wherein a and b are each independently 1 or 2; Rf is a linear or branched perfluoroalkyl radical having from 2 to about 20 carbon atoms, optionally interrupted with at least one oxygen; R is a C1 to C20 linear, branched or cyclic alkyl, or a C6 to C10 aryl; B is —(CH2CHR1O)x—, k is 0 or 1, x is 1 to about 20, A is —(CH2)m[(CHR1CH2O)]s—[(CH2)m(CH)tCHOH(CH2)m]e—, wherein each m is independently 0 to 3, s is 0 to about 30, t is 0 or 1, and e is 0 or 1, R1 is H or CH3, Q is: —OP(O)(O−M+)(O)—, —O—, —S—(CH2)m—C(O)—O—, —SO2—O— —CH2CH2O—C(O)CH2C(OH)(V)CH2C(O)O—; —(CH2CH2O)xCH2CH(OH)—(CH2CH2O)x—(CH2)m—Si[OSi(R2)3]2—, —SO2NR2—, —(CH2CH2O)zC(O)CH(SO3−M+)CH2C(O)(OCH2CH2)z— wherein z is 1 to about 15, or a bond when s is a positive integer, V is —C(O)OR3 and R3 is H, CH3 or Rf; R2 is C1 to C4 alkyl, and M+ is a Group 1 metal or an ammonium (NHxR2y)+ cation wherein x+y=4, and R2 is C1 to C4 alkyl, provided that when Q is —OP(O)(O−M+)(O)— or when Q is —(CH2CH2O)z—C(O)CH(SO3−M+)CH2C(O)(OCH2CH2)z—, then at least one of s or e is a positive integer.
摘要翻译：式1的表面活性剂（Rf-A）a-Q - （[B] k-R）b式1其中a和b各自独立地为1或2; Rf是具有2至约20个碳原子的直链或支链全氟烷基，任选被至少一个氧中断; R为C1至C20直链，支链或环状烷基或C6至C10芳基; B是 - （CH 2 CHR 1 O）x - ，k是0或1，x是1至约20，A是 - （CH 2）m [（CHR 1 CH 2 O）] s - [（CH 2）m（CH）t CHOH（CH 2）m] e-，其中每个m独立地为0至3，s为0至约30，t为0或1，e为0或1，R 1为H或CH 3，Q为：-OP（O）（O-M + ）（O） - ， - O - ， - S-（CH 2）m -C（O）-O-，-SO 2 -O-CH 2 CH 2 O-C（O）CH 2 C（OH） - ; - （CH2CH2O）xCH2CH（OH） - （CH2CH2O）x-（CH2）m-Si [OSi（R2）3] 2-，-SO2NR2-， - （CH2CH2O）zC（O）CH（SO3-M +）CH2C O）（OCH 2 CH 2）z - ，其中z为1至约15，或当s为正整数时为键，V为-C（O）OR 3且R 3为H，CH 3或R f; R2是C1-C4烷基，M +是1价金属或铵（NHxR2y）+阳离子，其中x + y = 4，R2是C1-C4烷基，条件是当Q是-OP（O） M +）（O） - 或Q为 - （CH 2 CH 2 O）z -C（O）CH（SO 3 -M +）CH 2 C（O）（OCH 2 CH 2）z - 时，则s或e中的至少一个为正整数。

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