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1. 发明授权

US08083951B2 Method for purifying quench water and scrubbing water from MTO by mini-hydrocyclone and apparatus used for same 有权
标题翻译：通过微型水力旋流器及其使用的设备净化淬火水和从MTO洗涤水的方法
公开(公告)号：US08083951B2
公开(公告)日：2011-12-27
申请号：US12427578
申请日：2009-04-21
申请人： Hualin Wang , Yanhong Zhang , Qiang Yang , Ji Ma , Zhishan Bai , Yu Liu , Longhu Liang , Lei Shi , Jie Zhang
发明人： Hualin Wang , Yanhong Zhang , Qiang Yang , Ji Ma , Zhishan Bai , Yu Liu , Longhu Liang , Lei Shi , Jie Zhang
IPC分类号： C07C1/00 , C07C7/00 , B01D21/26
CPC分类号： C07C1/20 , C02F1/385 , C02F2101/10 , C02F2103/365 , C10G3/42 , C10G2300/805 , H01L2924/01006 , H01L2924/01012 , H01L2924/01033 , H01L2924/01082 , Y02P30/20 , C07C11/02
摘要： The invention provides a method for purifying MTO quench water and scrubbing water via mini-hydrocyclone separation, comprising: removing the entrapped catalyst particles from the MTO quench water via mini-hydrocyclone separation; cooling the quench water purified by mini-hydrocyclone separation so as to effect the recycling of water; removing the entrapped catalyst particles from the MTO quench water to be stripped via mini-hydrocyclone separation, so as to reduce the deposition of the catalyst particles within the stripping tower; removing the entrapped catalyst particles from the MTO scrubbing water via mini-hydrocyclone separation; and cooling the scrubbing water purified via mini-hydrocyclone separation so as to effect the recycling of water. The invention also provides an apparatus for purifying MTO quench water and scrubbing water via mini-hydrocyclone separation.
摘要翻译：本发明提供了一种通过微型水力旋流分离净化MTO骤冷水和洗涤水的方法，包括：通过微型水力旋流分离从MTO骤冷水中除去捕获的催化剂颗粒; 冷却通过微型水力旋流分离纯化的骤冷水，以实现水的再循环; 通过微型水力旋流分离从待分离的MTO骤冷水中除去夹带的催化剂颗粒，以减少催化剂颗粒在汽提塔内的沉积; 通过微型水力旋流分离从MTO洗涤水中除去捕获的催化剂颗粒; 并通过微型水力旋流分离器冷却洗涤水，从而实现水的再循环。本发明还提供了一种用于通过微型水力旋流分离器净化MTO骤冷水和洗涤水的装置。

2. 发明申请

US20100059456A1 METHOD FOR PURIFYING QUENCH WATER AND SCRUBBING WATER FROM MTO BY MINI-HYDROCYCLONE AND APPARATUS USED FOR SAME 有权
标题翻译：通过微型盐酸盐从MTO中净化QU水和洗涤水的方法和用于其的装置
公开(公告)号：US20100059456A1
公开(公告)日：2010-03-11
申请号：US12427578
申请日：2009-04-21
申请人： Hualin WANG , Yanhong Zhang , Qiang Yang , Ji Ma , Zhishan Bai
发明人： Hualin WANG , Yanhong Zhang , Qiang Yang , Ji Ma , Zhishan Bai
IPC分类号： C02F1/38
CPC分类号： C07C1/20 , C02F1/385 , C02F2101/10 , C02F2103/365 , C10G3/42 , C10G2300/805 , H01L2924/01006 , H01L2924/01012 , H01L2924/01033 , H01L2924/01082 , Y02P30/20 , C07C11/02
摘要： The invention provides a method for purifying MTO quench water and scrubbing water via mini-hydrocyclone separation, comprising: removing the entrapped catalyst particles from the MTO quench water via mini-hydrocyclone separation; cooling the quench water purified by mini-hydrocyclone separation so as to effect the recycling of water; removing the entrapped catalyst particles from the MTO quench water to be stripped via mini-hydrocyclone separation, so as to reduce the deposition of the catalyst particles within the stripping tower; removing the entrapped catalyst particles from the MTO scrubbing water via mini-hydrocyclone separation; and cooling the scrubbing water purified via mini-hydrocyclone separation so as to effect the recycling of water. The invention also provides an apparatus for purifying MTO quench water and scrubbing water via mini-hydrocyclone separation.
摘要翻译：本发明提供了一种通过微型水力旋流分离净化MTO骤冷水和洗涤水的方法，包括：通过微型水力旋流分离从MTO骤冷水中除去捕获的催化剂颗粒; 冷却通过微型水力旋流分离纯化的骤冷水，以实现水的再循环; 通过微型水力旋流分离从待分离的MTO骤冷水中除去夹带的催化剂颗粒，以减少催化剂颗粒在汽提塔内的沉积; 通过微型水力旋流分离从MTO洗涤水中除去捕获的催化剂颗粒; 并通过微型水力旋流分离器冷却洗涤水，从而实现水的再循环。本发明还提供了一种用于通过微型水力旋流分离器净化MTO骤冷水和洗涤水的装置。

3. 发明授权

US08221634B2 Process and apparatus for separating and recovering waste alkali from cyclohexane oxidation solution 有权
标题翻译：从环己烷氧化溶液中分离回收废碱的工艺和设备
公开(公告)号：US08221634B2
公开(公告)日：2012-07-17
申请号：US12358004
申请日：2009-01-22
申请人： Zhishan Bai , Zhuoqun Qian , Ji Ma , Ping Zhou , Yanhong Zhang , Hualin Wang
发明人： Zhishan Bai , Zhuoqun Qian , Ji Ma , Ping Zhou , Yanhong Zhang , Hualin Wang
IPC分类号： C07C49/00 , C07C29/20 , B01D21/00 , B01D35/18 , B01D11/00
CPC分类号： C07C45/33 , B01D17/0214 , C07C2601/14 , Y10S210/908 , C07C49/403
摘要： A process and an apparatus for separating and recovering waste alkali from a cyclohexane oxidation solution are provided. A gradient combination of the gravity separation technique, the vortex separation technique and the coalescence separation technique is used to carry out fine separation of the waste alkali liquor from the cyclohexane oxidation solution. The purified cyclohexane oxidation solution is fed into a down-stream apparatus. Most of the waste alkali liquor thus separated is recycled, while the remaining is expelled. The expelled waste alkali liquor is incinerated in an incinerator, followed by recovering the molten species using a pneumatic pulverization process.
摘要翻译：提供了一种用于从环己烷氧化溶液中分离和回收废碱的方法和装置。使用重力分离技术，涡流分离技术和聚结分离技术的梯度组合进行废碱液与环己烷氧化溶液的精细分离。将纯化的环己烷氧化溶液进料到下游装置中。大部分如此分离的废碱液体被回收，而其余的被排出。将排出的废碱液在焚化炉中焚烧，然后使用气动粉碎法回收熔融物质。

4. 发明申请

US20100126938A1 PROCESS AND APPARATUS FOR SEPARATING AND RECOVERING WASTE ALKALI FROM CYCLOHEXANE OXIDATION SOLUTION 有权
标题翻译：从环己烷氧化溶液中分离和回收废物碱的工艺和装置
公开(公告)号：US20100126938A1
公开(公告)日：2010-05-27
申请号：US12358004
申请日：2009-01-22
申请人： Zhishan BAI , Zhuoqun Qian , Ji Ma , Ping Zhou , Yanhong Zhang , Hualin Wang
发明人： Zhishan BAI , Zhuoqun Qian , Ji Ma , Ping Zhou , Yanhong Zhang , Hualin Wang
IPC分类号： B01D21/00
CPC分类号： C07C45/33 , B01D17/0214 , C07C2601/14 , Y10S210/908 , C07C49/403
摘要： The present invention relates to a process and an apparatus for separating and recovering the waste alkali from a cyclohexane oxidation solution, and provides a process and an apparatus for separating and recovering the waste alkali from a cyclohexane oxidation solution. According to the invention, a gradient combination of the gravity separation technique, the vortex separation technique and the coalescence separation technique is used to carry out fine separation of the waste alkali liquor from the cyclohexane oxidation solution. The purified cyclohexane oxidation solution is fed into a down-stream apparatus. Most of the waste alkali liquor thus separated is recycled, while the remaining is expelled. The expelled waste alkali liquor is incinerated in an incinerator, followed by recovering the molten species using a pneumatic pulverization process. According to the invention, the content of Na+ in the cyclohexane oxidation solution fed into the alkane tower can be lowered to less than 3 mg/L, and the molten species resulting from incineration can be recovered 100%. Thus, risk of environmental pollution by the waste alkali liquor is substantially eliminated. While the invention is well suited to separate and recover the waste alkali liquor from a cyclohexane oxidation solution, it may be adapted to other chemical engineering systems for separating and recovering waste alkali liquor as well.
摘要翻译：本发明涉及从环己烷氧化溶液中分离回收废碱的方法和装置，提供了从环己烷氧化溶液中分离回收废碱的方法和装置。根据本发明，使用重力分离技术，涡流分离技术和聚结分离技术的梯度组合来进行废碱液与环己烷氧化溶液的精细分离。将纯化的环己烷氧化溶液进料到下游装置中。大部分如此分离的废碱液体被回收，而其余的被排出。将排出的废碱液在焚化炉中焚烧，然后使用气动粉碎法回收熔融物质。根据本发明，进料到烷烃塔中的环己烷氧化溶液中的Na +含量可以降低到小于3mg / L，焚烧产生的熔融物质可以回收100％。因此，废碱液的环境污染的风险基本上被消除。尽管本发明非常适合于从环己烷氧化溶液中分离和回收废碱液体，但是也可以适用于用于分离和回收废碱液的其它化学工程系统。

5. 发明申请

US20100104498A1 SHORT-FLOW PROCESS FOR DESULFURIZATION OF CIRCULATING HYDROGEN AND DEVICE FOR THE SAME 有权
标题翻译：循环氢和其装置脱硫的短流程
公开(公告)号：US20100104498A1
公开(公告)日：2010-04-29
申请号：US12557320
申请日：2009-09-10
申请人： Hualin Wang , Ji Ma , Zhuoqun Qian , Yanhong Zhang , Liquan Li , Qian Zeng , Chonggang Chen , Qiang Yang , Xiaomei Xu , Xin Cui
发明人： Hualin Wang , Ji Ma , Zhuoqun Qian , Yanhong Zhang , Liquan Li , Qian Zeng , Chonggang Chen , Qiang Yang , Xiaomei Xu , Xin Cui
IPC分类号： C01B3/50 , B01D19/00
CPC分类号： C01B3/50 , B01D53/485 , B01D53/52 , B01D2256/16 , B01D2257/304 , C01B3/52 , C01B2203/0415 , C01B2203/0465 , C01B2203/0485 , C01B2203/0495
摘要： The invention relates to a short-flow process for desulfurization of circulating hydrogen and a device for the same. A short-flow process for desulfurization of circulating hydrogen is provided, comprising: (a) removing hydrocarbons from the circulating hydrogen mixture, so that the liquid drops of the heavy hydrocarbons in the dispersion phase are separated from the circulating hydrogen in the continuous phase, and a heavy hydrocarbon phase and a mixture phase of circulating hydrogen containing sulfur are obtained; (b) further separating the resultant mixture phase to remove the sulfides therein, so that circulating hydrogen without sulfur is obtained; (c) further separating the resultant circulating hydrogen without sulfur to remove the amine solution therein, so that purified circulating hydrogen is obtained. The invention also provides a device for desulfurization of circulating hydrogen.
摘要翻译：本发明涉及循环氢脱硫的短流程及其设备。提供了循环氢脱硫的短流程，包括：（a）从循环氢混合物中除去烃，使得分散相中的重质烃的液滴在连续相中与循环氢分离，得到重质烃相和循环含硫硫的混合相; （b）进一步分离所得混合物相以除去其中的硫化物，从而获得不含硫的循环氢; （c）进一步分离所得的无硫的循环氢，以除去其中的胺溶液，从而获得纯化的循环氢。本发明还提供了一种循环氢脱硫装置。

6. 发明授权

US09302910B2 Short-flow process for desulfurization of circulating hydrogen and device for the same 有权
标题翻译：循环氢和脱硫设备的短流程相同
公开(公告)号：US09302910B2
公开(公告)日：2016-04-05
申请号：US12557320
申请日：2009-09-10
申请人： Hualin Wang , Ji Ma , Zhuoqun Qian , Yanhong Zhang , Liquan Li , Qian Zeng , Chonggang Chen , Qiang Yang , Xiaomei Xu , Xin Cui
发明人： Hualin Wang , Ji Ma , Zhuoqun Qian , Yanhong Zhang , Liquan Li , Qian Zeng , Chonggang Chen , Qiang Yang , Xiaomei Xu , Xin Cui
IPC分类号： B01D19/00 , C01B3/50 , B01D53/48 , B01D53/52 , C01B3/52
CPC分类号： C01B3/50 , B01D53/485 , B01D53/52 , B01D2256/16 , B01D2257/304 , C01B3/52 , C01B2203/0415 , C01B2203/0465 , C01B2203/0485 , C01B2203/0495
摘要： The invention relates to a short-flow process for desulfurization of circulating hydrogen and a device for the same. A short-flow process for desulfurization of circulating hydrogen is provided, comprising: (a) removing hydrocarbons from the circulating hydrogen mixture, so that the liquid drops of the heavy hydrocarbons in the dispersion phase are separated from the circulating hydrogen in the continuous phase, and a heavy hydrocarbon phase and a mixture phase of circulating hydrogen containing sulfur are obtained; (b) further separating the resultant mixture phase to remove the sulfides therein, so that circulating hydrogen without sulfur is obtained; (c) further separating the resultant circulating hydrogen without sulfur to remove the amine solution therein, so that purified circulating hydrogen is obtained. The invention also provides a device for desulfurization of circulating hydrogen.
摘要翻译：本发明涉及循环氢脱硫的短流程及其设备。提供了循环氢脱硫的短流程，包括：（a）从循环氢混合物中除去烃，使得分散相中的重质烃的液滴在连续相中与循环氢分离，得到重质烃相和循环含硫硫的混合相; （b）进一步分离所得混合物相以除去其中的硫化物，从而获得不含硫的循环氢; （c）进一步分离所得的无硫的循环氢，以除去其中的胺溶液，从而获得纯化的循环氢。本发明还提供了一种循环氢脱硫装置。

7. 发明申请

US20130239810A1 Process and Apparatus for Optimized Combination of Purification and Separation of MTO Reaction Gas Containing Catalyst Fine Powder 审中-公开
标题翻译：用于优化组合含有催化剂细粉末的MTO反应气体的净化和分离的方法和装置
公开(公告)号：US20130239810A1
公开(公告)日：2013-09-19
申请号：US13496286
申请日：2011-04-13
申请人： Qiang Yang , Hualin Wang , Zhiming Li , Yanhong Zhang , Xin Cui , Dejian Xu , Wenjie Lv , Xiaomei Xu
发明人： Qiang Yang , Hualin Wang , Zhiming Li , Yanhong Zhang , Xin Cui , Dejian Xu , Wenjie Lv , Xiaomei Xu
IPC分类号： B01D53/14
CPC分类号： B01D53/14 , B01D21/262 , B01D21/267 , B01D47/06 , B01D2247/04 , B01D2247/101 , C07C1/20 , C10G3/00 , C10G3/42 , C10K1/02 , C10K1/024 , C10K1/026 , C10K1/04 , C10K1/08 , C07C11/02
摘要： The invention relates to a process and an apparatus for optimized combination of purification and separation of MTO reaction gas containing catalyst fine powder. In particular, the invention provides a process for optimized combination of purification and separation of MTO reaction gas containing catalyst fine powder, comprising (a) scrubbing, purifying and cooling the MTO reaction gas containing catalyst fine powder, and separating and recovering the mist entrained in the scrubbed reaction gas and the catalyst fine powder that is not scrubbed off; (b) subjecting the scrubbing liquid containing catalyst fine powder to solid-liquid separation, and the purified scrubbing liquid after separation to repeated use after subsequent heat exchange and stripping treatment; and (c) subjecting the scrubbing liquid containing catalyst fine powder to solid-liquid separation, and further concentrating the scrubbing liquid containing catalyst fine powder after separation before the catalyst fine powder is finally recovered in solid form by centrifugal dewatering or drying. The invention also provides an apparatus for optimized combination of purification and separation of MTO reaction gas containing catalyst fine powder.
摘要翻译：本发明涉及一种用于优化组合含有催化剂细粉末的MTO反应气体的净化和分离的方法和装置。特别地，本发明提供了一种用于优化组合含有催化剂细粉末的MTO反应气体的组合的方法，其包括（a）洗涤，纯化和冷却含有催化剂细粉末的MTO反应气体，以及分离和回收夹带在洗涤反应气体和未被洗涤的催化剂细粉末; （b）使含有催化剂细粉末的洗涤液进行固液分离，然后在后续的热交换和汽提处理之后分离后重复使用的纯化洗涤液; 和（c）将含有催化剂细粉末的洗涤液进行固液分离，并在分离后进一步浓缩含有催化剂细粉末的洗涤液，然后通过离心脱水或干燥最终以固体形式回收催化剂细粉末。本发明还提供了用于优化组合含有催化剂细粉末的MTO反应气体的净化和分离的装置。

8. 发明申请

US20150218463A1 Process and Device for Treating Catalyst Discharged from Bubbling Bed Hydrogenation of Residual Oil 审中-公开
标题翻译：用于处理从起泡床中排出的催化剂残余油氢化的方法和装置
公开(公告)号：US20150218463A1
公开(公告)日：2015-08-06
申请号：US14398059
申请日：2012-07-25
申请人： Jianping Li , Jiangang Wang , Hualin Wang , Yanhong Zhang , Xin Cui , Ling Shen , Liquan Li , Chonggang Chen , Qian Zeng , Ying Zhao
发明人： Jianping Li , Jiangang Wang , Hualin Wang , Yanhong Zhang , Xin Cui , Ling Shen , Liquan Li , Chonggang Chen , Qian Zeng , Ying Zhao
IPC分类号： C10G53/02 , B01J38/48
CPC分类号： C10G53/02 , B01J23/90 , B01J38/48 , C10G47/26 , C10G49/12 , C10G53/04 , C10G2300/107 , C10G2300/1077 , C10G2300/4081 , C10G2300/70
摘要： The invention relates to a process and a device for treating a catalyst discharged from bubbling bed hydrogenation of residual oil. Provided is a process for treating a catalyst discharged from bubbling bed hydrogenation of residual oil, comprising the following steps: (1) adjustment and control to reduce viscosity; (2) desorption and separation by rotational flow; and (3) separation and resource utilization of an oil-water-catalyst three phase. Also provided is a device for treating a catalyst discharged from bubbling bed hydrogenation of residual oil.
摘要翻译：本发明涉及一种用于处理从起泡床氢残余油中排出的催化剂的方法和装置。提供了一种处理从起泡床氢残余油中排出的催化剂的方法，包括以下步骤：（1）调节和控制以降低粘度; （2）通过旋转流解吸和分离; 和（3）油水催化剂三相的分离和资源利用。还提供了用于处理从起泡床氢残余油排出的催化剂的装置。

9. 发明授权

US09533247B2 Method and apparatus for micro-hydrocyclone purification for flue gas carbon dioxide capture system 有权
标题翻译：用于烟气二氧化碳捕集系统的微水力旋流器净化方法和装置
公开(公告)号：US09533247B2
公开(公告)日：2017-01-03
申请号：US13984406
申请日：2011-08-25
申请人： Hualin Wang , Songbai Mao , Qisong Shen , Ning Ye , Yanhong Zhang , Jiangang Wang , Ling Shen , Xin Cui
发明人： Hualin Wang , Songbai Mao , Qisong Shen , Ning Ye , Yanhong Zhang , Jiangang Wang , Ling Shen , Xin Cui
IPC分类号： B01D45/16 , B01D53/14 , B01D53/18 , B01D53/62
CPC分类号： B01D45/16 , B01D53/1418 , B01D53/1475 , B01D53/18 , B01D53/62 , B01D2258/0283 , Y02A50/2342 , Y02C10/04 , Y02C10/06
摘要： Provided are a method and an apparatus for micro-hydrocyclone purification for a flue gas carbon dioxide capture system. The method comprises: performing gas-liquid micro-hydrocylone separation with ultralow pressure drop on scrubbed flue gas, to remove aerosol particulates entrained in the flue gas; performing gas-liquid micro hydrocyclone separation with ultralow pressure drop on off-gas vented from the top of an absorption column, to remove entrained aerosol particulates; performing gas-liquid micro hydrocyclone separation with ultralow pressure drop on cooled regeneration gas, to remove entrained aerosol particulates; and performing liquid-solid and liquid-liquid two-stage micro-hydrocyclone separation on a mixed amine solution lean for carbon dioxide discharged from regeneration column, to remove entrained solid particulates and machine oil. The apparatus comprises: a water scrubbing column, rotation flow separators, liquid-solid micro-hydrocyclone separator sets, a water scrubbing tank, a absorption column, a regeneration column, liquid-solid micro-hydrocyclones and liquid-liquid micro-hydrocyclones.
摘要翻译：提供了用于烟道气二氧化碳捕获系统的微水力旋流器净化的方法和装置。该方法包括：在经过洗涤的烟道气上进行超低压降的气 - 液微水龙胆分离，除去夹带在烟气中的气溶胶微粒; 在从吸收塔顶部排出的废气上进行超低压降的气液微型水力旋流分离器，以除去夹带的气溶胶颗粒物; 在冷再生气体上进行超低压气滴分离，清除夹带的气溶胶微粒; 并在从再生塔排出的稀二氧化碳的混合胺溶液中进行液固两液微旋流分离，除去夹带的固体微粒和机油。该装置包括：水洗柱，旋转流分离器，液固微型水力旋流分离器组，水洗涤槽，吸收塔，再生塔，液固微流体旋流器和液 - 液微水力旋流器。

10. 发明申请

US20140026752A1 Method and Apparatus for Micro-Hydrocyclone Purification For Flue Gas Carbon Dioxide Capture System 有权
标题翻译：用于烟道气二氧化碳捕集系统的微水力旋流器净化方法和装置
公开(公告)号：US20140026752A1
公开(公告)日：2014-01-30
申请号：US13984406
申请日：2011-08-25
申请人： Hualin Wang , Songbai Mao , Qisong Shen , Ning Ye , Yanhong Zhang , Jiangang Wang , Ling Shen , Xin Cui
发明人： Hualin Wang , Songbai Mao , Qisong Shen , Ning Ye , Yanhong Zhang , Jiangang Wang , Ling Shen , Xin Cui
IPC分类号： B01D45/16
CPC分类号： B01D45/16 , B01D53/1418 , B01D53/1475 , B01D53/18 , B01D53/62 , B01D2258/0283 , Y02A50/2342 , Y02C10/04 , Y02C10/06
摘要： Provided are a method and an apparatus for micro-hydrocyclone purification for a flue gas carbon dioxide capture system. The method comprises: performing gas-liquid micro-hydrocylone separation with ultralow pressure drop on scrubbed flue gas, to remove aerosol particulates entrained in the flue gas; performing gas-liquid micro hydrocyclone separation with ultralowpressure drop on off-gas vented from the top of an absorption column, to remove entrained aerosol particulates; performing gas-liquid micro hydrocyclone separation with ultralow pressure drop on cooled regeneration gas, to remove entrained aerosol particulates; and performing liquid-solid and liquid-liquid two-stage micro-hydrocyclone separation on a mixed amine solution lean for carbon dioxide discharged from regeneration column, to remove entrained solid particulates and machine oil. The apparatus comprises: a water scrubbing column, rotation flow separators, liquid-solid micro-hydrocyclone separator sets, a water scrubbing tank, a absorption column, a regeneration column, liquid-solid micro-hydrocyclones and liquid-liquid micro-hydrocyclones.
摘要翻译：提供了用于烟道气二氧化碳捕获系统的微水力旋流器净化的方法和装置。该方法包括：在经过洗涤的烟道气上进行超低压降的气 - 液微水龙胆分离，除去夹带在烟气中的气溶胶微粒; 在从吸收塔顶部排出的废气中进行超液压滴下的气液微型水力旋流器分离，以除去夹带的气溶胶颗粒物; 在冷再生气体上进行超低压气滴分离，清除夹带的气溶胶微粒; 并在从再生塔排出的稀二氧化碳的混合胺溶液中进行液固两液微旋流分离，除去夹带的固体微粒和机油。该装置包括：水洗柱，旋转流分离器，液固微型水力旋流分离器组，水洗涤槽，吸收塔，再生塔，液固微流体旋流器和液 - 液微水力旋流器。

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