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1. 发明授权

US5562740A Process for preparing reduced odor and improved brightness individualized, polycarboxylic acid crosslinked fibers 失效
标题翻译：用于制备减少气味和改善亮度的方法单独的多元羧酸交联纤维
公开(公告)号：US5562740A
公开(公告)日：1996-10-08
申请号：US490793
申请日：1995-06-15
申请人： Jeffery T. Cook , Walter D. Daniels , Pedro A. Rodriguez , Peter A. Graef , Clifford R. Bolstad , William L. Duncan
发明人： Jeffery T. Cook , Walter D. Daniels , Pedro A. Rodriguez , Peter A. Graef , Clifford R. Bolstad , William L. Duncan
IPC分类号： A61F13/53 , A61F5/44 , A61F13/15 , A61F13/472 , A61F13/49 , A61L15/24 , A61L15/28 , A61L15/46 , D06M11/38 , D06M11/50 , D06M13/02 , D06M13/192 , D06M13/207 , D06M101/06 , D21C9/00 , D21H11/20 , D21H13/06 , D21H21/22
CPC分类号： A61L15/46 , A61L15/24 , A61L15/28 , D06M11/38 , D06M11/50 , D06M13/192 , D06M13/207 , D21C9/005 , A61L2300/11
摘要： Disclosed is a process for making reduced odor individualized, crosslinked fibers which includes the steps of providing cellulosic fibers, contacting the fibers with a solution containing a C.sub.2 -C.sub.9 polycarboxylic acid crosslinking agent, mechanically separating the fibers into substantially individual form, drying the fibers and reacting the crosslinking agent with the individualized fibers to form intrafiber crosslink bonds. The individualized cellulosic fibers are then contacted with a strong alkaline solution and strong oxidizing agent to reduce the odor and increase the brightness. Preferably, the crosslinking agent is citric acid, and preferably, between about 1.0 weight % and about 12.0 weight % of the crosslinking agent reacts to form the intrafiber crosslink bonds. Preferably, the alkaline solution is an aqueous solution of sodium hydroxide, and preferably, about 0.09 weight % of the sodium hydroxide, on a dry fiber weight basis, is applied to the crosslinked fibers. Preferably, the oxidizing agent is hydrogen peroxide, and preferably, about 0.04 weight % of the hydrogen peroxide, on a dry fiber weight basis, is applied to the crosslinked fiber. The reduced odor individualized, crosslinked fibers are useful in a variety of absorbent structure applications.
摘要翻译：公开了一种制备减少气味的个体化交联纤维的方法，其包括以下步骤：提供纤维素纤维，使纤维与含有C 2 -C 9多元羧酸交联剂的溶液接触，将纤维机械分离成基本上单独的形式，干燥纤维和使交联剂与各自的纤维反应形成纤维内交联键。然后将个体化纤维素纤维与强碱性溶液和强氧化剂接触以降低气味并增加亮度。优选地，交联剂是柠檬酸，并且优选约1.0重量％至约12.0重量％的交联剂反应以形成纤维内交联键。优选地，碱性溶液是氢氧化钠的水溶液，优选将基于干纤维重量的约0.09重量％的氢氧化钠施加到交联纤维上。优选地，氧化剂是过氧化氢，优选地，基于干纤维重量的约0.04重量％的过氧化氢施加到交联纤维上。减少的气味个性化的交联纤维可用于各种吸收结构应用。

2. 发明授权

US06436231B1 Method and apparatus for crosslinking individualized cellulose fibers 失效
标题翻译：用于交联个体化纤维素纤维的方法和设备
公开(公告)号：US06436231B1
公开(公告)日：2002-08-20
申请号：US08509401
申请日：1995-07-31
申请人： Peter A. Graef , Colin Elston , Fred E. Olmstead , Clifford R. Bolstad , Mark W. Bowns , Frank R. Hunter , Allan R. Carney
发明人： Peter A. Graef , Colin Elston , Fred E. Olmstead , Clifford R. Bolstad , Mark W. Bowns , Frank R. Hunter , Allan R. Carney
IPC分类号： D21C900
CPC分类号： A61F13/15707 , A61F13/53 , A61F2013/530007 , A61F2013/530474 , A61L15/28 , D04H1/54 , D04H1/655 , D06M11/30 , D06M13/137 , D06M13/1845 , D06M13/192 , D06M13/262 , D06M13/418 , D06M13/419 , D06M13/432 , D06M13/438 , D06M13/44 , D06M13/52 , D21B1/066 , D21C9/005 , D21H11/20 , D21H15/10 , D21H17/05 , D21H17/06 , D21H17/07 , D21H17/10 , D21H21/06 , D21H21/24 , D21H23/04 , D21H23/18 , D21H23/20 , D21H23/28 , D21H25/005 , D21H25/02 , C08L1/02
摘要： An apparatus is disclosed for preparing a quantity of individual treated fibers from one or more fiber mats. The apparatus comprises a fiber treatment zone, and a conveyor for conveying each mat through the fiber treatment zone. In the treatment zone each mat is impregnated by an applicator with a treatment material, such as a crosslinking substance, and conveyed directly to an attrition device. The attrition device fiberizes the mats to form a fiber output having a low nit level, such as no more than about three, and a dryer both dries the fiber output and cures the crosslinking substance. The fiberizer is configured to minimize the accumulation of fiber at locations therein. Fiber is transported from the attrition device to the dryer at a high velocity under reduced pressure to promote drying. A heated retention bin is provided after drying to increase curing time in the system. A thermobonding agent may be added to the dried and cured fibers to enhance the wet strength of webs made from the fiber.
摘要翻译：公开了一种用于从一个或多个纤维垫制备一批单独处理的纤维的装置。该设备包括纤维处理区和用于将每个垫传送通过纤维处理区的输送机。在处理区中，每个垫通过涂布器用诸如交联物质的处理材料浸渍，并直接输送到磨耗装置。磨耗装置使垫子纤维化以形成具有低nit水平（例如不超过约3个）的纤维输出，并且干燥器既干燥纤维输出并固化交联物质。纤维化器被配置为使纤维在其中的位置处的聚集最小化。纤维在减压下以高速度从磨耗装置输送到干燥器以促进干燥。在干燥后提供加热的保存箱，以增加系统中的固化时间。可以将热粘合剂添加到干燥和固化的纤维中，以增强由纤维制成的织物的湿强度。

3. 发明授权

US5437418A Apparatus for crosslinking individualized cellulose fibers 失效
标题翻译：用于交联个体化纤维素纤维的装置
公开(公告)号：US5437418A
公开(公告)日：1995-08-01
申请号：US820323
申请日：1992-01-13
申请人： Peter A. Graef , Colin Elston , Fred E. Olmstead , Clifford R. Bolstad , Mark W. Bowns , Frank R. Hunter , Allan R. Carney
发明人： Peter A. Graef , Colin Elston , Fred E. Olmstead , Clifford R. Bolstad , Mark W. Bowns , Frank R. Hunter , Allan R. Carney
IPC分类号： A61F13/15 , A61L15/28 , D04H1/58 , D04H1/64 , D06M11/30 , D06M13/137 , D06M13/184 , D06M13/192 , D06M13/262 , D06M13/418 , D06M13/419 , D06M13/432 , D06M13/438 , D06M13/44 , D06M13/52 , D21B1/06 , D21C9/00 , D21H11/20 , D21H15/10 , D21H17/05 , D21H17/06 , D21H17/07 , D21H17/10 , D21H21/06 , D21H21/24 , D21H23/04 , D21H23/18 , D21H23/20 , D21H23/28 , D21H25/00 , D21H25/02 , B02C11/08
CPC分类号： A61F13/15707 , A61F13/53 , A61L15/28 , D04H1/54 , D04H1/655 , D06M11/30 , D06M13/137 , D06M13/1845 , D06M13/192 , D06M13/262 , D06M13/418 , D06M13/419 , D06M13/432 , D06M13/438 , D06M13/44 , D06M13/52 , D21B1/066 , D21C9/005 , D21H11/20 , D21H15/10 , D21H17/05 , D21H17/06 , D21H17/07 , D21H17/10 , D21H21/06 , D21H21/24 , D21H23/04 , D21H23/18 , D21H23/20 , D21H23/28 , D21H25/005 , D21H25/02 , A61F2013/530007 , A61F2013/530474
摘要： An apparatus is disclosed for preparing a quantity of individual treated fibers from one or more fiber mats. The apparatus comprises a fiber treatment zone, and a conveyor for conveying each mat through the fiber treatment zone. In the treatment zone each mat is impregnated by an applicator with a treatment material, such as a crosslinking substance, and conveyed directly to an attrition device. The attrition device fiberizes the mats to form a fiber output having a low nit level, such as no more than about three, and a dryer both dries the fiber output and cures the crosslinking substance. The fiberizer is configured to minimize the accumulation of fiber at locations therein. Fiber is transported from the attrition device to the dryer at a high velocity under reduced pressure to promote drying. A heated retention bin is provided after drying to increase curing time in the system. A thermobonding agent may be added to the dried and cured fibers to enhance the wet strength of webs made from the fiber.
摘要翻译：公开了一种用于从一个或多个纤维垫制备一批单独处理的纤维的装置。该设备包括纤维处理区和用于将每个垫传送通过纤维处理区的输送机。在处理区中，每个垫通过涂布器用诸如交联物质的处理材料浸渍，并直接输送到磨耗装置。磨耗装置使垫子纤维化以形成具有低nit水平（例如不超过约3个）的纤维输出，并且干燥器既干燥纤维输出并固化交联物质。纤维化器被配置为使纤维在其中的位置处的聚集最小化。纤维在减压下以高速度从磨耗装置输送到干燥器以促进干燥。在干燥后提供加热的保存箱，以增加系统中的固化时间。可以将热粘合剂加入到干燥和固化的纤维中，以增强由纤维制成的织物的湿强度。

4. 发明授权

US5253815A Fiberizing apparatus 失效
标题翻译：纤维化设备
公开(公告)号：US5253815A
公开(公告)日：1993-10-19
申请号：US607312
申请日：1990-10-31
申请人： Mark W. Bowns , Fred E. Olmstead , Peter A. Graef , Clifford R. Bolstad
发明人： Mark W. Bowns , Fred E. Olmstead , Peter A. Graef , Clifford R. Bolstad
IPC分类号： D21B1/06 , D21D1/32 , B02C13/04 , B02C13/12
CPC分类号： D21B1/066 , D21D1/32
摘要： A fiberizer is described having a rotor to which plural hammers are mounted for fiberizing a sheet of fibers delivered to the rotor as the rotor is rotated. A feed mechanism utilizing a pair of seal rollers, at least one of which is driven, is configured for effective delivery of both wet or dry sheets to the fiberizer. The hammers are configured to minimize dead spaces within the fiberizer. In addition, air flow is directed through the fiberizer to minimize accumulations of fibers therein. Furthermore, an optional liquid flushing mechanism is provided for periodically cleaning the fiberizer during use.
摘要翻译：描述了一种纤维化器，其具有转子，多个锤安装成用于使转子旋转时输送到转子的纤维片纤维化。使用一对密封辊（其中至少一个被驱动）的进给机构构造成有效地将湿纸张或干纸张传送到纤维化器。锤被配置成最小化纤维化器内的死空间。此外，空气流引导通过纤维化器以最小化其中纤维的积聚。此外，提供了可选的液体冲洗机构，用于在使用期间周期性地清洁纤维化器。

5. 发明授权

US06630054B1 Methods for forming a fluted composite 失效
标题翻译：形成槽纹复合材料的方法
公开(公告)号：US06630054B1
公开(公告)日：2003-10-07
申请号：US09664576
申请日：2000-09-18
申请人： Peter A. Graef , Clifford R. Bolstad , Fred B. Howard , Charles E. Miller , Daniel T. Bunker
发明人： Peter A. Graef , Clifford R. Bolstad , Fred B. Howard , Charles E. Miller , Daniel T. Bunker
IPC分类号： D21H1100
CPC分类号： D21H11/20 , A61F13/15617 , A61F13/15658 , A61F13/15699 , A61F13/534 , A61F13/536 , A61F2013/1539 , A61F2013/4581 , A61F2013/530386 , A61F2013/530481 , D21C9/002 , D21F9/006 , D21F11/002 , D21F11/006 , D21F11/04 , D21F11/14
摘要： Methods for forming an absorbent fibrous composite containing absorbent material dispersed in bands through the composite and along the composite's length are disclosed. The methods generally include depositing a fibrous slurry on a foraminous support to form a web and depositing or injecting absorbent material into the web across its width to provide a web having absorbent material in bands along the composite's length. Drying the web provides a fluted absorbent composite. In one embodiment, the method is a wetlaid method and in another embodiment, the method is a foam-forming method. Preferably, the methods are twin-wire forming methods.
摘要翻译：公开了形成吸收性纤维复合材料的方法，所述吸收性纤维复合材料含有通过所述复合材料分散在带中并沿着所述复合材料的长度的吸收材料。所述方法通常包括在多孔载体上沉积纤维浆料以形成网状物并且将吸收材料沉积或注入到横跨其宽度的纤维网中以提供沿着复合材料的长度在带中具有吸收材料的网。干燥纤维网提供有槽的吸收性复合材料。在一个实施方案中，该方法是湿法成网法，在另一个实施方案中，该方法是泡沫形成方法。优选地，所述方法是双网形成方法。

6. 发明授权

US07166190B2 Methods for forming a fluted composite 失效
标题翻译：形成槽纹复合材料的方法
公开(公告)号：US07166190B2
公开(公告)日：2007-01-23
申请号：US11067857
申请日：2005-02-28
申请人： Peter A. Graef , Clifford R. Bolstad , Fred B. Howard , Charles E. Miller , Daniel T. Bunker
发明人： Peter A. Graef , Clifford R. Bolstad , Fred B. Howard , Charles E. Miller , Daniel T. Bunker
IPC分类号： D21H23/14 , D21H13/02
CPC分类号： D21H11/20 , A61F13/15617 , A61F13/15658 , A61F13/15699 , A61F13/534 , A61F13/536 , A61F2013/1539 , A61F2013/4581 , A61F2013/530386 , A61F2013/530481 , D21C9/002 , D21F9/006 , D21F11/002 , D21F11/006 , D21F11/04 , D21F11/14
摘要： Methods for forming an absorbent fibrous composite containing absorbent material dispersed in bands through the composite and along the composite's length are disclosed. The methods generally include depositing a fibrous slurry on a foraminous support to form a web and depositing or injecting absorbent material into the web across its width to provide a web having absorbent material in bands along the composite's length. Drying the web provides a fluted absorbent composite. In one embodiment, the method is a wetlaid method and in another embodiment, the method is a foam-forming method. Preferably, the methods are twin-wire forming methods.
摘要翻译：公开了形成吸收性纤维复合材料的方法，所述吸收性纤维复合材料含有通过所述复合材料分散在带中并沿着所述复合材料的长度的吸收材料。所述方法通常包括在多孔载体上沉积纤维浆料以形成网状物并且将吸收材料沉积或注入到横跨其宽度的纤维网中以提供沿着复合材料的长度在带中具有吸收材料的网。干燥纤维网提供有槽的吸收性复合材料。在一个实施方案中，该方法是湿法成网方法，在另一个实施方案中，该方法是泡沫形成方法。优选地，这些方法是双网形成方法。

7. 发明授权

US5324391A Method for crosslinking cellulose fibers 失效
标题翻译：交联纤维素纤维的方法
公开(公告)号：US5324391A
公开(公告)日：1994-06-28
申请号：US974365
申请日：1992-11-09
申请人： Allan R. Carney , Peter A. Graef , Mark W. Bowns , Clifford R. Bolstad , Fred E. Olmstead
发明人： Allan R. Carney , Peter A. Graef , Mark W. Bowns , Clifford R. Bolstad , Fred E. Olmstead
IPC分类号： D04H1/42 , A61F13/15 , D21B1/06 , D21H17/05
CPC分类号： D21B1/066 , A61F2013/530007 , A61F2013/530474
摘要： A method is disclosed for preparing a quantity of individual treated fibers from one or more fiber mats in a treatment apparatus. The apparatus comprises a fiber treatment zone, a conveyor for conveying each mat through the fiber treatment zone, wherein each mat is impregnated by an applicator with a crosslinking substance, and directly to an attrition device. The attrition device fiberizes the mats to form a fiber output having a low nit level, such as no more than about three, and a dryer for both drying the fiber output and curing the crosslinking substance. The fiberizer is configured to have minimize the accumulation of fiber at locations therein. An optional component of the fiberizer is a novel fluff generator comprised of multiple rotors each having plural longitudinally extended rows of radially extending rotor pins that rotate past groups of shorter pins mounted on the inside surface of the fluff generator housing.
摘要翻译：公开了一种用于在处理设备中从一个或多个纤维垫制备一批单独经处理的纤维的方法。该设备包括纤维处理区，用于通过纤维处理区输送每个垫的输送机，其中每个垫被具有交联物质的涂布器浸渍，并且直接用于磨耗装置。磨耗装置将垫子纤维化以形成具有低nit水平（例如不超过约3个）的纤维输出，以及用于干燥纤维输出并固化交联物质的干燥器。纤维化器被配置为使纤维在其中的位置处的积聚最小化。纤维化器的可选组件是由多个转子组成的新型绒毛发生器，每个转子具有多个纵向延伸的径向延伸的转子销的行，其经过安装在绒毛发生器壳体的内表面上的较短销组。

8. 发明授权

US5225047A Crosslinked cellulose products and method for their preparation 失效
标题翻译：交联纤维素产品及其制备方法
公开(公告)号：US5225047A
公开(公告)日：1993-07-06
申请号：US395208
申请日：1989-08-17
申请人： Peter A. Graef , Frank R. Hunter
发明人： Peter A. Graef , Frank R. Hunter
IPC分类号： A61F13/15 , D21H11/20 , D21H17/06 , D21H17/07 , D21H17/09 , D21H17/10 , D21H17/15 , D21H21/06 , D21H21/14 , D21H21/24 , D21H23/14 , D21H23/18 , D21H23/28
CPC分类号： D21H21/06 , D21H11/20 , D21H17/06 , D21H17/07 , D21H17/09 , D21H17/10 , D21H17/15 , D21H21/14 , D21H21/24 , D21H23/14 , D21H23/18 , D21H23/28 , A61F2013/530007 , A61F2013/530474
摘要： The invention is a method of making a wet formed, sheeted, readily reslurriable sheeted crosslinked cellulose and the products made by the method. Crosslinked wood pulp fibers tend to be quite brittle. If crosslinked while in sheeted form, the sheets cannot be readily defibered, either in a wet or dry state, without serious fiber degradation. The sheet products of the present invention can be easily redispersed or repulped in water without significant fiber breakage. The present products are made by including within the sheet, while still in wet form, a debonding or softening agent which is preferably added before the latent crosslinking reactant. Most preferably the debonder is added prior to the headbox of a paper machine and the crosslinking reactant is applied near the end of the forming wire or at the press section. The treated sheet is dried conventionally. Crosslinking may occur entirely during drying or during a period of additional heating, usually at a temperature in excess of 100.degree. C. for a short period of time. Conventional debonding agents and crosslinking reactants are suitable. The softening agent apparently reduces or prevents adhesive bonding between adjacent fibers caused by polymer formation external to the fiber under reaction conditions.
摘要翻译：本发明是一种制成湿成型，片状，易于再生的片状交联纤维素和通过该方法制备的产品的方法。交联的木浆纤维往往是相当脆的。如果以片状形式交联，则在湿或干的状态下，片材不能容易地脱纤维，而不会严重的纤维降解。本发明的片状产品可以容易地再分散或重新分配在水中而不会明显的纤维断裂。本产品通过在片状物中包含湿态形式，优选在潜在交联反应剂之前加入的脱粘剂或软化剂制成。最优选地，脱纸器在造纸机的流浆箱之前添加，并且交联反应物被施加在成形丝的端部附近或在压榨部分处。经处理的片材是常规干燥的。交联可能在干燥期间或在额外加热期间完全发生，通常在超过100℃的温度下短时间内完成。常规脱粘剂和交联反应物是合适的。在反应条件下，柔软剂明显降低或防止由纤维外部的聚合物形成引起的相邻纤维之间的粘结。

9. 发明授权

US06521812B1 Absorbent article containing a wetlaid unitary stratified composite 失效
标题翻译：含有湿润单层分层复合材料的吸收制品
公开(公告)号：US06521812B1
公开(公告)日：2003-02-18
申请号：US09621167
申请日：2000-07-21
申请人： Peter A. Graef , Colin Elston , Daniel T. Bunker , Fred B. Howard , Jeffrey D. Mathews , Shahrokh A. Naieni , Charles E. Miller
发明人： Peter A. Graef , Colin Elston , Daniel T. Bunker , Fred B. Howard , Jeffrey D. Mathews , Shahrokh A. Naieni , Charles E. Miller
IPC分类号： A61F1315
CPC分类号： B32B5/26 , A61F13/531 , A61F13/534 , A61F13/537 , A61F13/539 , B32B5/04 , B32B2262/0253 , B32B2262/0261 , B32B2262/0284 , B32B2262/04 , B32B2307/726 , B32B2307/73 , B32B2555/02
摘要： A unitary stratified composite composed of a first stratum and a second stratum integrally connected by a transition zone is disclosed. The first stratum serves as a liquid acquisition stratum that rapidly acquires and then transfers liquid to the second stratum. The second stratum serves to withdraw liquid from the first stratum and further serves as a temporary storage stratum. Methods for forming the unitary stratified composite are also disclosed.
摘要翻译：公开了由过渡区一体连接的第一层和第二层组成的整体分层复合材料。第一层作为液体采集层，迅速获得并将液体转移到第二层。第二层用于从第一层抽出液体，并进一步用作临时储存层。还公开了形成单一分层复合材料的方法。

10. 发明授权

US06518479B1 Absorbent article containing a foam-formed unitary stratified composite 失效
标题翻译：吸收制品包含泡沫形成的单一分层复合材料
公开(公告)号：US06518479B1
公开(公告)日：2003-02-11
申请号：US09620950
申请日：2000-07-21
申请人： Peter A. Graef , Colin Elston , Daniel T. Bunker , Fred B. Howard , Jeffrey D. Matthews , Shahrokh A. Naieni , Charles E. Miller
发明人： Peter A. Graef , Colin Elston , Daniel T. Bunker , Fred B. Howard , Jeffrey D. Matthews , Shahrokh A. Naieni , Charles E. Miller
IPC分类号： A61F1315
CPC分类号： B32B5/26 , A61F13/531 , A61F13/534 , A61F13/537 , A61F13/539 , B32B5/04 , B32B2262/0253 , B32B2262/0261 , B32B2262/0284 , B32B2262/04 , B32B2307/726 , B32B2307/73 , B32B2555/02
摘要： A unitary stratified composite composed of a first stratum and a second stratum integrally connected by a transition zone is disclosed. The first stratum serves as a liquid acquisition stratum that rapidly acquires and then transfers liquid to the second stratum. The second stratum serves to withdraw liquid from the first stratum and further serves as a temporary storage stratum. Methods for forming the unitary stratified composite are also disclosed.
摘要翻译：公开了由过渡区一体连接的第一层和第二层组成的整体分层复合材料。第一层作为液体采集层，迅速获得并将液体转移到第二层。第二层用于从第一层抽出液体，并进一步用作临时储存层。还公开了形成单一分层复合材料的方法。

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