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1. 发明授权

US09079818B2 Process for synthesis of fluorinated olefins 有权
标题翻译：合成氟化烯烃的方法
公开(公告)号：US09079818B2
公开(公告)日：2015-07-14
申请号：US12249958
申请日：2008-10-12
申请人： Sudip Mukhopadhyay , Cheryl L. Bortz , Barbara A. Light , Cheryl L. Cantlon , Robert C. Johnson
发明人： Sudip Mukhopadhyay , Cheryl L. Bortz , Barbara A. Light , Cheryl L. Cantlon , Robert C. Johnson
IPC分类号： C07C21/00 , C07C17/00 , C07C17/21 , C07C17/23 , C07C17/25 , C07C21/18
CPC分类号： C07C17/21 , C07C17/23 , C07C17/25 , C07C21/18 , C07C19/08
摘要： Disclosed is a process for the synthesis of fluorinated olefins, and in particularly preferred embodiments tetrafluorinated olefins having F on an unsaturated, non-terminal carbon, such as 2,3,3,3-tetrafluoropropene. The preferred processes of the present invention in accordance with one embodiment generally comprise: (a) reacting a compound of formula (I) X1X2 (I) with a compound of formula (II) CX1X2X3CX1═CX1X2 (II) to produce a reaction product comprising a compound of formula (III) CF3CHX1CH2X2 (III), and (b) exposing said compound of formula (III) to reaction conditions effective to convert said compound of formula (III) to a compound of formula (IV) CF3CZ═CH2 (IV) wherein X1, X2, and X3 are each independently selected from the group consisting of hydrogen, chlorine, bromine, fluorine and iodine, provided that X1 and X2 in formula (I) are not both hydrogen and Z is Cl, I, Br, or F.
摘要翻译：公开了用于合成氟化烯烃的方法，特别优选的实施方案中，在不饱和的非末端碳上具有F的四氟化烯烃如2,3,3,3-四氟丙烯。根据一个实施方案的本发明的优选方法通常包括：（a）使式（I）X1X2（I）化合物与式（II）化合物CX1X2X3CX1 = CX1X2（II）反应以产生反应产物，其包含式（III）化合物，CF 3 CHX 1 CH 2 X 2（III）的化合物，和（b）将式（III）化合物暴露于有效将式（III）化合物转化成式（IV）化合物的反应条件：CF 3 CZ = CH 2 ）其中X1，X2和X3各自独立地选自氢，氯，溴，氟和碘，条件是式（I）中的X1和X2不同时为氢，Z为Cl，I，Br，或F.

2. 发明申请

US20090099396A1 PROCESS FOR SYNTHESIS OF FLUORINATED OLEFINS 有权
标题翻译：合成氟化烯烃的方法
公开(公告)号：US20090099396A1
公开(公告)日：2009-04-16
申请号：US12249958
申请日：2008-10-12
申请人： Sudip Mukhopadhyay , Cheryl L. Bortz , Barbara A. Light , Cheryl L. Cantlon , Robert C. Johnson
发明人： Sudip Mukhopadhyay , Cheryl L. Bortz , Barbara A. Light , Cheryl L. Cantlon , Robert C. Johnson
IPC分类号： C07C17/20
CPC分类号： C07C17/21 , C07C17/23 , C07C17/25 , C07C21/18 , C07C19/08
摘要： Disclosed is a process for the synthesis of fluorinated olefins, and in particularly preferred embodiments tetrafluorinated olefins having F on an unsaturated, non-terminal carbon, such as 2,3,3,3-tetrafluoropropene. The preferred processes of the present invention in accordance with one embodiment generally comprise: (a) reacting a compound of formula (I) X1X2 (I) with a compound of formula (II) CX1X2X3CX1═CX1X2 (II) to produce a reaction product comprising a compound of formula (III) CF3CHX1CH2X2 (III), and (b) exposing said compound of formula (III) to reaction conditions effective to convert said compound of formula (III) to a compound of formula (IV) CF3CZ=CH2 (IV) wherein X1, X2, and X3 are each independently selected from the group consisting of hydrogen, chlorine, bromine, fluorine and iodine, provided that X1 and X2 in formula (I) are not both hydrogen and Z is Cl, I, Br, or F.
摘要翻译：公开了用于合成氟化烯烃的方法，特别优选的实施方案中，在不饱和的非末端碳上具有F的四氟化烯烃如2,3,3,3-四氟丙烯。根据一个实施方案的本发明的优选方法通常包括：（a）使式（I）化合物<？in-line-formula description =“In-Line Formulas”end =“lead”→> X1X2 I）<？in-line-formula description =“In-line formula”end =“tail”？>与式（II）的化合物<？in-line-formula description =“In-line Formulas”end =“ 引线“→CX1X2X3CX1-CX1X2（II）<？在线公式描述=”内联式“末端=”尾“→产生包含式（III）化合物的反应产物 -formulae description =“In-line Formulas”end =“lead”？> CF3CHX1CH2X2（III）和<？in-line-formula description =“In-line Formulas”end =“tail”？>（b）式（III）化合物与有效将所述式（III）化合物转化成式（IV）化合物的反应条件<β在线式描述=“在线式”末端=“铅”→CF 3 CZ = CH2（IV）<？in-line-formula description =“In-line Formulas”end =“tail”？>其中X1，X2和X3各自独立式（I）中的X 1和X 2不同时为氢，Z为Cl，I，Br或F时，选自氢，氯，溴，氟和碘组成的组。

3. 发明授权

US07951982B2 Method for producing fluorinated organic compounds 有权
标题翻译：氟化有机化合物的制备方法
公开(公告)号：US07951982B2
公开(公告)日：2011-05-31
申请号：US11592842
申请日：2006-11-03
申请人： Sudip Mukhopadhyay , Haridasan K. Nair , Hsueh S. Tung , Michael Van Der Puy , Robert C. Johnson , Daniel C. Merkel
发明人： Sudip Mukhopadhyay , Haridasan K. Nair , Hsueh S. Tung , Michael Van Der Puy , Robert C. Johnson , Daniel C. Merkel
IPC分类号： C07C21/18
CPC分类号： C07C17/25 , B01J23/02 , B01J23/44 , B01J23/755 , B01J23/78 , B01J23/83 , B01J35/06 , C07C17/00 , C07C17/269 , C07C21/18 , C07C19/08
摘要： Disclosed is a process for the preparation of fluorinated olefins. In preferred embodiments C3 olefins are produced by methods comprising contacting a compound of the Formula (I) C(R1aR2bR3c) (I) with a compound of Formula (II) C(R1aR2bR3c)Cn(R1aR2bR3c) II wherein R1a, R2b, and R3c are independently a hydrogen atom or a halogen selected from the group consisting of fluorine; chlorine, bromine and iodine, provided that the compound of formula I has at least three halogen substituents and that said at three halogen substituents comprise at least one fluorine; a, b and c are independently=0, 1, 2 or 3 and (a+b+c)=2 or 3; and n is 0 or 1, under conditions effective to produce at least one C3 fluoroolefin.
摘要翻译：公开了一种制备氟化烯烃的方法。在优选实施方案中，C3烯烃通过以下方法制备：包括使式（I）C（R 1a R 2b b C 3）（I）的化合物与式（II）的化合物C（R1aR2bR3c）Cn（R1aR2bR3c）II的化合物接触，其中R1a，R2b和R3c 独立地为氢原子或选自氟的卤素; 氯，溴和碘，条件是式I化合物具有至少三个卤素取代基，并且在三个卤素取代基上含有至少一个氟; a，b和c独立地为= 0,1,2或3，（a + b + c）= 2或3; 在有效产生至少一种C3氟代烯烃的条件下，n为0或1。

4. 发明授权

US07026521B1 Methane and methyl chloride as selective reducing agent in the transformation of hydrochlorofluorocarbons or chlorofluorocarbons to hydrofluorocarbons 失效
标题翻译：甲烷和氯甲烷作为选择性还原剂，在氢氯氟烃或氯氟烃转化为氢氟碳化合物
公开(公告)号：US07026521B1
公开(公告)日：2006-04-11
申请号：US11091311
申请日：2005-03-28
申请人： Sudip Mukhopadhyay , HsuehSung Tung , Daniel C. Merkel , Robert C. Johnson
发明人： Sudip Mukhopadhyay , HsuehSung Tung , Daniel C. Merkel , Robert C. Johnson
IPC分类号： C07C17/00
CPC分类号： B01J23/04 , B01J23/02 , B01J37/0201 , C07C17/23 , C07C19/08
摘要： A gas phase reaction process for producing a hydrofluorocarbon from a hydrochlorofluorocarbon or chlorofluorocarbon reactant by contacting, in the presence of a catalyst, the hydrochlorofluorocarbon or chlorofluorocarbon reactant with a reducing agent selected from methane, methyl chloride and mixtures thereof, to produce the hydrofluorocarbon.
摘要翻译：一种用于由氢氯氟烃或氯氟烃反应物生产氢氟烃的气相反应方法，其中在催化剂存在下，将氢氯氟烃或氯氟烃反应物与选自甲烷，氯甲烷及其混合物的还原剂接触，制备氢氟烃。

5. 发明授权

US07880040B2 Method for producing fluorinated organic compounds 有权
标题翻译：氟化有机化合物的制备方法
公开(公告)号：US07880040B2
公开(公告)日：2011-02-01
申请号：US11592442
申请日：2006-11-03
申请人： Sudip Mukhopadhyay , Haridasan K. Nair , Hsueh S. Tung , Michael Van Der Puy , Rajiv R. Singh , Haiyou Wang , Robert C. Johnson , Rajesh K. Dubey
发明人： Sudip Mukhopadhyay , Haridasan K. Nair , Hsueh S. Tung , Michael Van Der Puy , Rajiv R. Singh , Haiyou Wang , Robert C. Johnson , Rajesh K. Dubey
IPC分类号： C07C19/08
CPC分类号： C07C17/25 , C07C21/18
摘要： Disclosed is a method for producing fluorinated organic compounds, including hydrofluoropropenes, which preferably comprises converting at least one compound of formula (I): CF3CFnCHmXa-m (I) to at least one compound of formula (II) CF3CZCHZ (II). where each X is independently Cl, I or Br; each Z is independently H or F; n is 1 or 2; m is 1, 2 or 3, provided that when n is 1, m is 1 or 2; a is 2 or 3, and a-m≧0. Certain embodiments include the step of reacting fluorinated C2 olefin, such as tetrafluoroethylene, with a C1 addition agent under conditions effective to produce a compound of formula (I).
摘要翻译：公开了一种制备氟化有机化合物的方法，包括氢氟丙烯，其优选包括将至少一种式（I）化合物：CF 3 CF n CH m X a-m（I）转化为至少一种式（II）CF 3 CZCHZ（II）化合物。其中每个X独立地为Cl，I或Br; 每个Z独立地为H或F; n为1或2; m为1,2或3，条件是当n为1时，m为1或2; a为2或3，a-m≥0。某些实施方案包括在有效产生式（I）化合物的条件下使氟化C 2烯烃如四氟乙烯与C1加成剂反应的步骤。

6. 发明授权

US08927791B2 Method for producing tetrafluoropropenes 有权
标题翻译：生产四氟丙烯的方法
公开(公告)号：US08927791B2
公开(公告)日：2015-01-06
申请号：US13073023
申请日：2011-03-28
申请人： Selma Bektesevic , Hsueh S. Tung , Haiyou Wang , Daniel C. Merkel , Robert C. Johnson
发明人： Selma Bektesevic , Hsueh S. Tung , Haiyou Wang , Daniel C. Merkel , Robert C. Johnson
IPC分类号： C07C17/00 , C07C17/25 , C07C19/08 , C07C21/18 , C07C17/21 , C07C17/087
CPC分类号： C07C17/21 , C07C17/087 , C07C17/25 , C07C19/10 , C07C19/08 , C07C21/18
摘要： The current invention relates to a process for making a tetrafluoropropene using a tetrafluorochloropropane and/or a pentafluoropropane as starting or intermediate reagents. More specifically, though not exclusively, the present invention relates to a novel method for preparing a tetrafluoropropene by dehydrohalogenating a starting or intermediate tetrafluorochloropropane and/or pentafluoropropane material in the presence of a caustic solution at a temperature range greater than 40° C. and less than or equal to 80° C.
摘要翻译：本发明涉及使用四氟氯丙烷和/或五氟丙烷作为起始剂或中间体试剂制备四氟丙烯的方法。更具体地说，本发明涉及一种通过在苛性碱溶液存在下，在大于40℃和更低的温度范围内将起始或中间四氟氯丙烷和/或五氟丙烷物质脱卤化氢来制备四氟丙烯的新方法超过或等于80℃

7. 发明授权

US08883767B2 Low ether compositions and delivery apparatus 有权
标题翻译：低醚组合物和输送装置
公开(公告)号：US08883767B2
公开(公告)日：2014-11-11
申请号：US12897476
申请日：2010-10-04
申请人： Gerald R. Dever , Eric Chen-nan Su , William Scott Rogersr , Robert C. Johnson
发明人： Gerald R. Dever , Eric Chen-nan Su , William Scott Rogersr , Robert C. Johnson
IPC分类号： A61K31/60 , A61K47/00 , A61M35/00 , B05C17/01 , B43K1/06 , B67D7/60 , A61K8/67 , A61K8/97 , A61K8/27 , A61K8/36 , A61K8/368 , A61K47/08 , A61K47/44 , A61K47/10 , A61K47/38 , A61K36/29 , A61K33/30 , A61K31/197 , A61K9/70 , A61K9/06 , A61K47/14 , A61K9/00 , A61K47/06 , A61K8/365 , A61K31/19 , A61K8/73 , A61K31/375
CPC分类号： A61K33/30 , A61K8/27 , A61K8/36 , A61K8/365 , A61K8/368 , A61K8/673 , A61K8/676 , A61K8/731 , A61K8/97 , A61K9/0014 , A61K9/06 , A61K9/7015 , A61K31/19 , A61K31/197 , A61K31/375 , A61K31/60 , A61K36/29 , A61K47/06 , A61K47/08 , A61K47/10 , A61K47/14 , A61K47/38 , A61K47/44 , Y10S514/944 , A61K2300/00
摘要： A low ether gel composition for application to skin comprising a keratolytic agent, in particular salicylic acid, and comprising a nitrocellulose and one or more volatile ingredients, which forms a film on contact with skin adequate to form a protective barrier for the keratolytic agent for a period of time necessary to provide treatment to the skin; methods of treating using such compositions, and dispensers containing such compositions.
摘要翻译：一种用于皮肤应用的低醚凝胶组合物，其包含角质分解剂，特别是水杨酸，并且包含硝化纤维素和一种或多种挥发性成分，其形成与皮肤接触足够的膜以形成角质分解剂的保护屏障为皮肤提供治疗所需的时间; 使用这种组合物的处理方法和含有这种组合物的分配器。

8. 发明申请

US20130245597A1 CLICK PEN APPLICATOR DEVICE AND METHOD OF USING SAME 审中-公开
标题翻译：点击笔应用器件及其使用方法
公开(公告)号：US20130245597A1
公开(公告)日：2013-09-19
申请号：US13988043
申请日：2011-11-18
申请人： Robert C. Johnson , James C. Wightman , Michael Furey , Jeff Hayet
发明人： Robert C. Johnson , James C. Wightman , Michael Furey , Jeff Hayet
IPC分类号： A61M5/315
摘要： A click pen applicator device that provides predetermined dosing of the formulation for precise application, and rapidly primes the formulation using the dosing click mechanism to prepare the applicator for use is disclosed.
摘要翻译：一种点击式笔式涂抹器装置，其提供用于精确应用的配方的预定剂量，并且公开了使用计量点击机构来准备施用器以使用的制剂。

9. 发明授权

US08392226B1 Controlling meta-data of information resources 有权
标题翻译：控制信息资源的元数据
公开(公告)号：US08392226B1
公开(公告)日：2013-03-05
申请号：US10700998
申请日：2003-11-04
申请人： Mark D. Hamm , James B. Greer , Robert C. Johnson
发明人： Mark D. Hamm , James B. Greer , Robert C. Johnson
IPC分类号： G06Q10/00 , G06Q20/00
CPC分类号： G06Q10/00
摘要： Controlling information resources involves accessing a control definition of a number of control definitions associated with a first party and a second party. The first party has a first information resource and the second party has a second information resource, where the first information resource is in communication with the second information resource. The control definitions define a practice for monitoring the second information resource, where each control definition has a condition and a consequence. Meta-data is received from a second monitor of the second information resource, where the meta-data describes operation of the second information resource. The condition is applied to the meta-data in order to monitor the second information resource.
摘要翻译：控制信息资源涉及访问与第一方和第二方相关联的多个控制定义的控制定义。第一方具有第一信息资源，第二方具有第二信息资源，其中第一信息资源与第二信息资源通信。控制定义定义了监视第二信息资源的做法，其中每个控制定义都有一个条件和后果。从第二信息资源的第二监视器接收元数据，其中元数据描述第二信息资源的操作。该条件被应用于元数据以便监视第二信息资源。

10. 发明申请

US20120291910A1 CLICK PEN APPLICATOR DEVICE AND METHOD OF USING SAME 有权
标题翻译：点击笔应用器件及其使用方法
公开(公告)号：US20120291910A1
公开(公告)日：2012-11-22
申请号：US13563269
申请日：2012-07-31
申请人： James C. Wightman , Michael Furey , Jeff Hayet , Robert C. Johnson
发明人： James C. Wightman , Michael Furey , Jeff Hayet , Robert C. Johnson
IPC分类号： B65B1/04
CPC分类号： A61M5/3156 , A45D34/042 , A45D2200/051 , A45D2200/055 , A46B11/0055 , A46B11/0058
摘要： A click pen applicator device that provides predetermined dosing of the formulation for precise application, and rapidly primes the formulation using the dosing click mechanism to prepare the applicator for use.
摘要翻译：一种点击式笔式涂抹器装置，其提供用于精确应用的配方的预定剂量，并使用计量点击机构快速注射制剂以制备使用的施用器。

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