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1. 发明授权

US09925500B2 Membrane derived from polyfunctional amine and combination of different polyfunctional amine-reactive monomers 有权
公开(公告)号：US09925500B2
公开(公告)日：2018-03-27
申请号：US14407013
申请日：2013-07-03
申请人： Dow Global Technologies LLC
发明人： Mou Paul , Tina L. Arrowood , Robert C. Cieslinski , Steven D. Jons , Steven Rosenberg , Abhishek Roy , Ian A. Tomlinson
IPC分类号： B01D67/00 , B01D69/12 , B01D71/56 , B01D61/02 , B01D69/10
CPC分类号： B01D67/0006 , B01D61/025 , B01D67/0002 , B01D69/10 , B01D69/12 , B01D69/125 , B01D71/56 , B01D2323/00 , B01D2323/38 , B01D2323/40 , B01D2325/20
摘要： A method for making a composite polyamide membrane including a porous support and a thin film polyamide layer including the steps of applying a polyfunctional amine monomer and a combination amine-reactive compounds to a surface of the porous support and reacting the constituents to form a thin film polyamide layer, wherein the amine-reactive compounds include: i) a polyfunctional amine-reactive monomer including two to three amine-reactive moieties selected from acyl halide, sulfonyl halide and anhydride, ii) a polyfunctional amine-reactive monomer including at least four amine-reactive moieties selected from acyl halide, sulfonyl halide and anhydride, and iii) an acid compound including at least on carboxylic acid moiety or salt thereof and at least one amine-reactive moiety selected from acyl halide and sulfonyl halide.

2. 发明授权

US09701766B2 Hydrophilic vinylidene fluoride polymers 有权
公开(公告)号：US09701766B2
公开(公告)日：2017-07-11
申请号：US13995454
申请日：2011-12-13
申请人： Julio A. Abusleme , Roberto Biancardi , Fabien Roblot , Anna Maria Bertasa , Giulio Brinati
发明人： Julio A. Abusleme , Roberto Biancardi , Fabien Roblot , Anna Maria Bertasa , Giulio Brinati
IPC分类号： C08F14/22 , B01D71/32 , B01D71/78 , C08F214/22 , C08F251/02 , C08F290/02 , C08F290/10 , C08F8/00
CPC分类号： C08F14/22 , B01D71/32 , B01D71/78 , B01D2323/38 , C08F8/00 , C08F214/225 , C08F251/02 , C08F290/02 , C08F290/10 , C08F214/22
摘要： The present invention pertains to a process for the manufacture of a grafted fluorinated polymer comprising at least one grafted side chain comprising one or more glycosidic recurring units [polymer (F)], said process comprising polymerizing: vinylidene fluoride (VDF), optionally, one or more other fluorinated monomers [monomers (F)], and optionally, one or more (meth)acrylic monomers [monomers (MA)], in the presence of at least one polysaccharide derivative [derivative (P)], said polysaccharide derivative having a dynamic viscosity of less than 15 mPa×s, as measured according to ASTM D445 at 20° C. in an aqueous solution at a concentration of 2% by weight, and by further providing novel polymers (F) as defined above.

3. 发明授权

US09643128B2 Thin film composite membrane derived from tetra-functional acyl halide monomer 有权
公开(公告)号：US09643128B2
公开(公告)日：2017-05-09
申请号：US14405697
申请日：2013-07-03
申请人： Dow Global Technologies LLC
发明人： Tina L. Arrowood , Aman A. Desai , Steven D. Jons , Mou Paul , Abhishek Roy
IPC分类号： B01D67/00 , B01D69/12 , B01D71/56 , B01D61/02 , B01D69/10
CPC分类号： B01D67/0006 , B01D61/025 , B01D67/0002 , B01D69/10 , B01D69/12 , B01D69/125 , B01D71/56 , B01D2323/00 , B01D2323/38 , B01D2323/40 , B01D2325/20
摘要： A method for making a composite polyamide membrane including a porous support and a thin film polyamide layer, wherein the method includes the step of applying a polyfunctional amine monomer and a tetraacyl acyl halide monomer represented by Formula (I) to a surface of the porous support and interfacially polymerizing the monomers to form a thin film polyamide layer; wherein A is selected from: oxygen (—O—); carbon (—C—); silicon (—Si—); each of which may be unsubstituted or substituted, e.g. with alkyl groups of 1-4 carbon atoms; or a carbonyl group (—C(O)—), X is the same or different and is selected from a halogen, and Y is selected from halogen and hydroxide.

4. 发明授权

US09610542B2 Composite polyamide membrane with increased carboxylic acid functionality 有权
公开(公告)号：US09610542B2
公开(公告)日：2017-04-04
申请号：US14406994
申请日：2013-07-03
申请人： Dow Global Technologies LLC
发明人： Abhishek Roy , Tina L. Arrowood , Robert C. Cieslinski , David D. Hawn , Steven D. Jons , Mou Paul , Martin H. Peery , XiaoHua Qiu , Steven Rosenberg , Ian A. Tomlinson , Chengli Zu
IPC分类号： B01D39/00 , B01D39/14 , B01D71/56 , B05D5/00 , B01D67/00 , B01D69/12 , B01D61/02 , B01D69/10
CPC分类号： B01D67/0006 , B01D61/025 , B01D67/0002 , B01D69/10 , B01D69/12 , B01D69/125 , B01D71/56 , B01D2323/00 , B01D2323/38 , B01D2323/40 , B01D2325/20
摘要： A thin film composite membrane including a porous support and a thin film polyamide layer characterized by having a dissociated carboxylate content of at least 0.45 moles/kg at pH 9.5 and a method for making a composite polyamide applying a polar solution comprising a polyfunctional amine monomer and a non-polar solution comprising a polyfunctional amine-reactive monomer to a surface of the porous support and interfacially polymerizing the monomers to form a thin film polyamide layer, wherein the method is characterized by the non-polar solution comprising at least 0.025 wt % of an acid compound including at least one carboxylic acid moiety and at least one amine-reactive moiety selected from acyl halide and anhydride.

5. 发明授权

US09393528B2 Filtration membrane 有权
标题翻译：过滤膜
公开(公告)号：US09393528B2
公开(公告)日：2016-07-19
申请号：US14115242
申请日：2012-04-27
申请人： Allan Hjarbæk Holm
发明人： Allan Hjarbæk Holm
IPC分类号： B01D39/00 , B01D39/14 , B01D61/00 , B01D29/46 , B01D65/02 , B01D65/08 , B01D67/00 , B01D71/02
CPC分类号： B01D65/08 , B01D65/02 , B01D67/0093 , B01D71/022 , B01D2321/04 , B01D2321/22 , B01D2321/223 , B01D2323/38 , B01D2323/42
摘要： A filtration membrane (4) including a porous base layer (8) arranged adjacent to a filtration layer (6) having pores (10) extending through the filtration layer (6) is provided. The filtration layer is electrically conductive and at least one compound (24, 26) is attached on the filtration layer (6), thereby providing a protective surface layer (40). The at least one compound (24, 26) is configured to be at least partially cleaved off of the filtration layer (6) by a predefined cleave-off process.
摘要翻译：提供了一种过滤膜（4），其包括邻近具有延伸穿过过滤层（6）的孔（10）的过滤层（6）布置的多孔基层（8）。过滤层是导电的，并且至少一种化合物（24,26）附着在过滤层（6）上，从而提供保护表面层（40）。至少一种化合物（24,26）构造成通过预定义的切割过程至少部分地从过滤层（6）上分离。

6. 发明授权

US09272245B2 Filtration method 有权
标题翻译：过滤方法
公开(公告)号：US09272245B2
公开(公告)日：2016-03-01
申请号：US12993512
申请日：2009-04-30
申请人： Koichiro Yanagida
发明人： Koichiro Yanagida
IPC分类号： B01D69/08 , B01D69/12 , B01D71/34 , B01D71/68 , B01D71/82 , C07K1/00 , B01D61/14 , A61L2/00 , B01D61/22 , B01D67/00 , B01D69/02 , C07K1/34
CPC分类号： B01D61/145 , A61L2/0017 , B01D61/22 , B01D67/0093 , B01D69/02 , B01D69/08 , B01D69/12 , B01D71/34 , B01D71/68 , B01D2323/02 , B01D2323/38 , B01D2325/04 , B01D2325/20 , B01D2325/36 , C07K1/34
摘要： Provided is a filtration method for the step of removing viruses in a process of producing a protein preparation during which an intermediate protein preparation with a high protein concentration flows at high pressure to a virus removal filter. The filtration method employs a virus removal filter which has a close fitting nozzle of which the inlet at least has a pressure resistance of 600 kPa or more, and an effective area of the virus removal membrane of at least 0.0001 m2 and no more than 0.03 m2. An intermediate protein preparation with the protein concentration raised to at least 20 mg/ml and no more than 100 mg/ml by means of a purification process flows down to said virus removal filter under conditions in which the inlet pressure of the intermediate protein preparation is at least 150 kPa and no more than 600 kPa, the average protein filtration speed is at least 1.0 kg/m2/hr, and the filtration time is at least 1 hour and no more than 5 hours, to give an intermediate protein preparation filtrate with a viral removal rate (LRV) of ≧3.
摘要翻译：本发明提供一种过滤方法，用于在制备蛋白质制剂的过程中除去病毒的步骤，其中具有高蛋白质浓度的中间蛋白质制剂在高压下流向病毒去除过滤器。过滤方法采用病毒去除过滤器，其具有紧密喷嘴，入口至少具有600kPa以上的耐压性，病毒去除膜的有效面积为至少0.0001m 2且不大于0.03m 2 。通过纯化过程将蛋白质浓度升至至少20mg / ml且不超过100mg / ml的中间体蛋白质制剂在中间体蛋白质制剂的入口压力为至少150kPa且不超过600kPa，平均蛋白质过滤速度为至少1.0kg / m 2 / hr，并且过滤时间为至少1小时且不超过5小时，得到具有病毒清除率（LRV）≥3。

7. 发明申请

US20150314243A1 COMPOSITE POLYAMIDE MEMBRANE INCLUDING TRI-HYDROCARBYL PHOSPHATE 审中-公开
标题翻译：复合聚酰胺膜包括三氯磷酸盐
公开(公告)号：US20150314243A1
公开(公告)日：2015-11-05
申请号：US14650197
申请日：2014-01-03
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： Abhishek ROY , Yasushi MAEDA , Mou PAUL , Steven ROSENBERG , Ian A. TOMLINSON
IPC分类号： B01D71/56 , B01D69/10 , B01D69/12 , C08J5/18 , B01D67/00
CPC分类号： B01D69/125 , B01D67/0006 , B01D67/0093 , B01D69/10 , B01D71/56 , B01D2323/38 , C08J5/18 , C08J2377/00
摘要： A method for making a composite polyamide membrane comprising a porous support and a thin film polyamide layer, wherein the method includes:i) applying a polar solution including a polyfunctional amine monomer and a non-polar solution including a polyfunctional acylhalide monomer to a surface of a porous support and interfacially polymerizing the monomers to form a thin film polyamide layer, and wherein at least one or both of the solutions further includes a tri-hydrocarbyl phosphate compound and ii) exposing the thin film polyamide layer to nitrous acid.
摘要翻译：一种制造复合聚酰胺膜的方法，其包括多孔载体和薄膜聚酰胺层，其中所述方法包括：i）将包含多官能胺单体和包含多官能酰卤化物单体的非极性溶液的极性溶液施加到多孔载体和界面聚合单体以形成薄膜聚酰胺层，并且其中至少一种或两种溶液还包括三烃基磷酸酯化合物，和ii）将薄膜聚酰胺层暴露于亚硝酸。

8. 发明授权

US09028740B2 Permselective membrane and process for manufacturing thereof 有权
标题翻译：选择性渗透膜及其制造方法
公开(公告)号：US09028740B2
公开(公告)日：2015-05-12
申请号：US13926045
申请日：2013-06-25
申请人： Gambro Lundia AB
发明人： Hermann Gohl , Reinhold Buck
IPC分类号： B29D99/00 , B01D67/00 , B01D69/02 , B01D69/08 , D01D5/24 , A61M1/16 , A61M1/34
CPC分类号： B29D99/005 , A61M1/16 , A61M1/34 , A61M1/3403 , A61M2205/3368 , B01D67/0009 , B01D67/0011 , B01D67/0013 , B01D69/02 , B01D69/08 , B01D71/68 , B01D2323/08 , B01D2323/12 , B01D2323/36 , B01D2323/38 , B01D2325/022 , D01D5/24 , Y10T428/2975 , Y10T442/3106 , Y10T442/3325 , Y10T442/612 , Y10T442/647
摘要： A method for preparing by solvent phase inversion spinning a hollow fiber membrane suitable for dialysis. The membrane includes at least one hydrophobic polymer and at least one hydrophilic polymer. An outer surface of the membrane is characterized by pores having sizes in the range of 0.5-3 μm, with the density of the pores on the outer surface of the membrane being in the range of 10,000 to 150,000 pores per mm2. The method includes dissolving the at least one hydrophobic polymer and the at least one hydrophilic polymer in at least one solvent to form a polymer solution, extruding the thus-formed polymer solution through an outer ring slit of a nozzle with two concentric openings, extruding a center fluid through the inner opening of the nozzle, and wishing said membrane. The polymer solution coming out through the outer slit opening on the outside of the precipitating fiber is exposed to a humid steam/air mixture including a solvent content of between 0.5 and 10% by weight related to the water content.
摘要翻译：通过溶剂相转化制备适合于透析的中空纤维膜的方法。膜包括至少一种疏水性聚合物和至少一种亲水性聚合物。膜的外表面的特征在于具有0.5-3μm范围内的尺寸的孔，膜的外表面上的孔的密度在每平方毫米10,000至150,000个孔的范围内。该方法包括将至少一种疏水性聚合物和至少一种亲水性聚合物溶解在至少一种溶剂中以形成聚合物溶液，将由此形成的聚合物溶液通过具有两个同心开口的喷嘴的外环狭缝挤出，挤出中心流体通过喷嘴的内部开口，并希望所述膜。通过沉淀纤维外部的外部狭缝开口出来的聚合物溶液暴露于包含与含水量相关的0.5至10重量％的溶剂含量的湿蒸汽/空气混合物。

9. 发明授权

US08980096B2 Surface modified inorganic matrix and method for preparation thereof 有权
标题翻译：表面改性无机基体及其制备方法
公开(公告)号：US08980096B2
公开(公告)日：2015-03-17
申请号：US13257581
申请日：2010-03-19
申请人： Anita Buekenhoudt , Kenny Wyns , Vera Meynen , Bert Maes , Pegie Cool
发明人： Anita Buekenhoudt , Kenny Wyns , Vera Meynen , Bert Maes , Pegie Cool
IPC分类号： B01D61/00 , B01D39/00 , B01D39/14 , B01D67/00 , B01D69/12
CPC分类号： B01D67/0093 , B01D69/12 , B01D2323/04 , B01D2323/38
摘要： The present invention relates to a method for the modification of metal hydroxide and/or metal oxide surfaces of an inorganic matrix with an organometallic reagent for obtaining an organic functionalized matrix suitable for filtration processes. The method involves the direct covalent binding of organic functional groups by allowing a pre-treated matrix to react with organometallic reagents in the present of a suitable solvent. The present invention further relates to an organic functionalized matrix obtainable or obtained by carrying out a method according to the invention. The invention also provides various uses of a surface-modified matrices as described herein in various industrial applications, including for instance in filtration and/or adsorption and/or separation processes, or as support, e.g. for catalyst systems or for enzyme systems.
摘要翻译：本发明涉及一种用有机金属试剂改性无机基质的金属氢氧化物和/或金属氧化物表面的方法，用于获得适用于过滤工艺的有机官能化基质。该方法包括通过使预处理的基质与合适溶剂存在下的有机金属试剂反应来直接共价结合有机官能团。本发明还涉及通过实施根据本发明的方法可获得或获得的有机官能化基质。本发明还提供了各种工业应用中本文所述的表面改性基质的各种用途，包括例如在过滤和/或吸附和/或分离过程中，或作为载体，例如，用于催化剂体系或酶体系。

10. 发明授权

US08802273B2 Microporous polyethylene membrane, its production method, and battery separator 有权
标题翻译：微孔聚乙烯膜，其生产方法和电池隔膜
公开(公告)号：US08802273B2
公开(公告)日：2014-08-12
申请号：US12066965
申请日：2006-09-14
申请人： Kotaro Takita , Shintaro Kikuchi , Kazuhiro Yamada , Teiji Nakamura , Koichi Kono
发明人： Kotaro Takita , Shintaro Kikuchi , Kazuhiro Yamada , Teiji Nakamura , Koichi Kono
IPC分类号： H01M2/16
CPC分类号： H01M2/1653 , B01D67/0027 , B01D67/0083 , B01D67/009 , B01D67/0093 , B01D69/02 , B01D71/26 , B01D2323/30 , B01D2323/38 , B01D2325/022 , B01D2325/023 , B01D2325/24 , B01D2325/34 , H01M10/052 , Y10T428/249979
摘要： A microporous polyethylene membrane made of a polyethylene resin having a ratio (mass-average molecular weight/number-average molecular weight) of 5 to 300 and comprising 1% or more by mass of ultra-high-molecular-weight polyethylene having a mass-average molecular weight of 7×105 or more, the microporous polyethylene membrane comprising (a) a coarse-structure layer having an average pore diameter of more than 0.04 μm, which is formed on at least one surface, and (b) a dense-structure layer having an average pore diameter of 0.04 μm or less, an area ratio of the coarse-structure layer to the dense-structure layer in a membrane cross section being 0.1 to 0.8.
摘要翻译：一种由聚乙烯树脂制成的微孔聚乙烯膜，其具有5〜300的质量比（质量平均分子量/数均分子量），并且含有1质量％以上的超高分子量聚乙烯，平均分子量为7×10 5以上，所述微孔聚乙烯膜包含（a）在至少一个表面上形成的平均孔径大于0.04μm的粗结构层，和（b）平均孔径为0.04μm以下的结构层，在膜截面中粗构造层与致密结构层的面积比为0.1〜0.8。

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