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1. 发明授权

US09796805B2 Aminoplast crosslinker resin compositions, process for their preparation, and method of use 有权
公开(公告)号：US09796805B2
公开(公告)日：2017-10-24
申请号：US14352459
申请日：2012-10-21
申请人： Allnex IP S.a.r.l. , Allnex Austria GmbH
发明人： Lon-Tang Wilson Lin , Kuang-Jong Wu , Katsumi Inagaki , Johann Billiani
IPC分类号： C08G12/42 , C08G12/30 , B05D3/02 , C08G12/32 , C08L61/00 , C08G16/02 , C08G16/04 , C09D161/34 , C08G12/00 , B05D7/06 , B05D7/12 , B05D7/14 , C09D161/28
CPC分类号： C08G12/32 , B05D3/0254 , B05D7/06 , B05D7/12 , B05D7/14 , C08G12/00 , C08G16/0225 , C08G16/0268 , C08G16/04 , C08L61/00 , C09D161/28 , C09D161/34 , C08L101/06 , C08L67/04
摘要： This invention relates to aminoplast crosslinker resins compositions based on at least partially alkylated reaction products A of melamine, formaldehyde and an alkanol with the following parameters: the ratio of the amount of substance n(CH2O) of combined formaldehyde to the amount of substance n(Mel) of melamine is in the range of from 5.6 mol/mol to 6.2 mol/mol, the ratio of the amount of substance n(RO) of alkyl ether groups in the crosslinker resin to the amount of substance n(Mel) of melamine is in the range of from 5.0 mol/mol to 5.6 mol/mol, the mass fraction of monomer in the resin, calculated as the ratio of the mass of monomer m(1) to the mass m(A) of the reaction products A is between 35% and 55%, to a process for their preparation, and to a method of use thereof as crosslinker in combination with hydroxy-functional polymers for coating of heat-sensitive substrates.

2. 发明授权

US09217053B2 Active ester resin, thermosetting resin composition, cured product of same, semiconductor encapsulation material, prepreg, circuit board, and build-up film 有权
标题翻译：活性酯树脂，热固性树脂组合物，其固化产物，半导体封装材料，预浸料，电路板和堆积膜
公开(公告)号：US09217053B2
公开(公告)日：2015-12-22
申请号：US14386476
申请日：2013-03-19
申请人： DIC Corporation
发明人： Etsuko Suzuki , Kazuo Arita
IPC分类号： B32B27/08 , H05K1/05 , C08L63/00 , C08G8/32 , C08J5/24 , H01L23/29 , H05K1/03 , C08G16/02 , C08L61/14 , H05K3/00 , C08G8/28 , C08G16/04
CPC分类号： C08G8/32 , C08G8/28 , C08G16/0243 , C08G16/04 , C08G2190/00 , C08J5/24 , C08L61/14 , C08L2201/02 , C08L2203/206 , H01L23/293 , H01L2924/0002 , H05K1/0353 , H05K1/056 , H05K3/0067 , H05K2201/012 , H05K2201/0145 , Y10T428/31529 , H01L2924/00
摘要： A cured product exhibits good heat resistance and flame retardancy as well as low dielectric constant and low loss tangent. A phosphorus-containing compound (i) obtained by a reaction between an aromatic aldehyde (a1) having an alkoxy group as a substituent on a nucleus and an organic phosphorus compound (a2) having a P—H group or a P—OH group in a molecular structure is reacted with a phenolic substance (a3) to obtain a phosphorus-containing phenolic substance (A1). Then the phosphorus-containing phenolic substance (A1) is reacted with an aromatic dicarboxylic acid or an anhydride or dihalide of an aromatic dicarboxylic acid or a C2-6 saturated dicarboxylic acid or an anhydride or dihalide of a C2-6 saturated dicarboxylic acid (A2) so that all or some of hydroxyl groups of the phenolic substance (A1) form ester bonds.
摘要翻译：固化产物具有良好的耐热性和阻燃性以及低介电常数和低损耗角正切。通过在核上具有烷氧基作为取代基的芳香醛（a1）与具有P-H基或P-OH基的有机磷化合物（a2）之间的反应获得的含磷化合物（i）使分子结构与酚类物质（a3）反应，得到含磷酚类物质（A1）。然后将含磷酚类物质（A1）与芳族二羧酸或芳族二羧酸或C2-6饱和二羧酸的酸酐或二卤化物或C2-6饱和二羧酸的二卤化物（A2 ）使得酚类物质（A1）的全部或部分羟基形成酯键。

3. 发明申请

US20140302241A1 AMINOPLAST CROSSLINKER RESIN COMPOSITIONS, PROCESS FOR THEIR PREPARATION, AND METHOD OF USE 有权
标题翻译：氨基酸交联树脂组合物，其制备方法和使用方法
公开(公告)号：US20140302241A1
公开(公告)日：2014-10-09
申请号：US14352459
申请日：2012-10-21
申请人： Allnex USA , Allnex Austria GmbH
发明人： Lon-Tang Wilson Lin , Kuang-Jong Wu , Katsumi Inagaki , Johann Billiani
IPC分类号： C08G12/32 , B05D7/12 , B05D7/14 , B05D7/06 , C09D161/28 , B05D3/02
CPC分类号： C08G12/32 , B05D3/0254 , B05D7/06 , B05D7/12 , B05D7/14 , C08G12/00 , C08G16/0225 , C08G16/0268 , C08G16/04 , C08L61/00 , C09D161/28 , C09D161/34 , C08L101/06 , C08L67/04
摘要： This invention relates to aminoplast crosslinker resins compositions based on at least partially alkylated reaction products A of melamine, formaldehyde and an alkanol with the following parameters: the ratio of the amount of substance n(CH2O) of combined formaldehyde to the amount of substance n(Mel) of melamine is in the range of from 5.6 mol/mol to 6.2 mol/mol, the ratio of the amount of substance n(RO) of alkyl ether groups in the crosslinker resin to the amount of substance n(Mel) of melamine is in the range of from 5.0 mol/mol to 5.6 mol/mol, the mass fraction of monomer in the resin, calculated as the ratio of the mass of monomer m(1) to the mass m(A) of the reaction products A is between 35% and 55%, to a process for their preparation, and to a method of use thereof as crosslinker in combination with hydroxy-functional polymers for coating of heat-sensitive substrates.
摘要翻译：本发明涉及基于三聚氰胺，甲醛和链烷醇的至少部分烷基化反应产物A的氨基塑料交联剂树脂组合物，其具有以下参数：甲醛组合物的物质n（CH 2 O）的量与物质n（蜜胺的摩尔比在5.6摩尔/摩尔至6.2摩尔/摩尔的范围内，交联剂树脂中的烷基醚基团的物质n（RO）与三聚氰胺的物质n（Mel）的量的比例在5.0mol / mol至5.6mol / mol的范围内，树脂中单体的质量分数以单体m（1）的质量与反应产物A的质量m（A）的比计算相对于其制备方法为35％至55％，以及作为交联剂与用于涂覆热敏性基材的羟基官能聚合物结合使用的方法。

4. 发明授权

US4548738A Electrically conducting complexes of poly (3,6-N-alkylcarbazolyl alkenes) and method of making 失效
标题翻译：聚（3,6-N-烷基咔唑烯烃）的导电络合物及其制备方法
公开(公告)号：US4548738A
公开(公告)日：1985-10-22
申请号：US626565
申请日：1984-06-29
申请人： Samson A. Jenekhe , Barbara J. Fure
发明人： Samson A. Jenekhe , Barbara J. Fure
IPC分类号： C08G16/02 , C08G16/04 , C08G73/06 , H01B1/12 , H01B1/00
CPC分类号： C08G16/04 , C08G16/0268 , C08G73/0672 , H01B1/127 , H01B1/128
摘要： Environmentally stable polymer complexes of processible poly (3,6-N-alkylcarbazolyl alkenes) are disclosed with can be doped to a high electrical conductivity with charge transfer acceptors such as iodine together with a method of making the complexes.
摘要翻译：公开了可加工的聚（3,6-N-烷基咔唑烯烃）的环境稳定的聚合物复合物，其可以与电荷转移受体如碘一起掺杂到高导电性以及制备络合物的方法。

5. 发明授权

US4539377A Alkenylphenylglycidyl ether capped hydroxystyryl pyridines (pyrazines) and polymers thereof 失效
标题翻译：烯基苯基缩水甘油醚封端的羟基苯乙烯基吡啶（吡嗪）及其聚合物
公开(公告)号：US4539377A
公开(公告)日：1985-09-03
申请号：US632346
申请日：1984-07-19
申请人： Robert E. Hefner, Jr.
发明人： Robert E. Hefner, Jr.
IPC分类号： C08F299/02 , C08G16/02 , C08G16/04 , C08G73/12 , C08J5/24 , C08L61/00 , C08F283/06
CPC分类号： C08F299/026 , C08G16/0268 , C08G16/04 , C08G73/128 , C08J5/24 , C08L61/00
摘要： Alkenylphenylglycidyl ether capped styryl pyridines and styryl pyrazines are prepared by etherifying with an alkenylphenylglycidyl ether the reaction product of (A) a substituted pyridine and/or pyrazine with (B) a substituted aromatic aldehyde with the proviso that at least one of the components (A) or (B) contains a hydroxyl group which is susceptible to etherification by an alkenylphenylglycidyl ether. These alkenylphenylglycidyl ether capped styryl pyridines and pyrazines can be homopolymerized or copolymerized with other materials to produce polymers having excellent high temperature resistance, good mechanical strength and excellent processability and are used to make cured composites with heat resistant fibers that have applications in high temperature environments such as engine compartments and/or fire walls.
摘要翻译：烯基苯基缩水甘油醚封端的苯乙烯基吡啶和苯乙烯基吡嗪通过烯基苯基缩水甘油醚与（A）取代的吡啶和/或吡嗪与（B）取代的芳族醛的反应产物醚化而制备，条件是至少一种组分（A ）或（B）含有通过烯基苯基缩水甘油醚易于醚化的羟基。这些烯基苯基缩水甘油醚封端的苯乙烯基吡啶和吡嗪可以与其它材料均聚或共聚以制备具有优异的耐高温性，良好机械强度和优异加工性能的聚合物，并用于制备具有耐高温纤维的固化复合材料，作为发动机舱和/或防火墙。

6. 发明授权

US4115365A Process for preparing aminomethyl diaryl compound resins 失效
标题翻译：制备氨基甲基二芳基化合物树脂的方法
公开(公告)号：US4115365A
公开(公告)日：1978-09-19
申请号：US856443
申请日：1977-12-01
申请人： Harry A. Smith
发明人： Harry A. Smith
IPC分类号： C08G16/02 , C08G16/04 , C08L63/00 , C08G12/42 , C08G14/06
CPC分类号： C08G16/04 , C08G16/02 , C08L63/00
摘要： A method for the preparation of soluble, fusible, aminomethyl diaryl compound resins in the absence of halomethylation or halomethylated materials, which method comprises (a) refluxing a mixture of diaryl compound, an aldehyde, a saturated monocarboxylic acid, and a small amount of a strong acid catalyst to form an aldehyde-diaryl resin, (b) stripping off excess monocarboxylic acid under vacuum, and then (c) adding at least about 1 mole of a primary or secondary amine containing at least one additional nontertiary amino group per reactive group on the aldehyde-diaryl resin.
摘要翻译：一种在不存在卤代甲基化或卤代甲基化物质的情况下制备可溶的易熔氨基甲基二芳基化合物树脂的方法，该方法包括：（a）回流二芳基化合物，醛，饱和一元羧酸和少量的强酸催化剂以形成醛 - 二芳基树脂，（b）在真空下剥离过量的单羧酸，然后（c）每反应性基团加入至少约1摩尔含有至少一个另外的非氨基的伯或仲胺在醛 - 二芳基树脂上。

7. 发明授权

US4110279A High temperature polymers from methoxy functional ether aromatic monomers 失效
标题翻译：来自甲氧基官能团的芳族单体的高温聚合物
公开(公告)号：US4110279A
公开(公告)日：1978-08-29
申请号：US765143
申请日：1977-02-03
申请人： Donald L. Nelson , Norman T. Herbert
发明人： Donald L. Nelson , Norman T. Herbert
IPC分类号： C08G14/04 , C08G14/12 , C08G16/02 , C08G16/04 , C08L61/34 , C08L91/00
CPC分类号： C08G16/04 , C08G14/04 , C08G14/12 , C08G16/0218 , C08L61/34
摘要： A polymer derived by heating in the presence of an acid catalyst at between about 65.degree. C. and 260.degree. C.I. a reaction product, a cogeneric mixture of alkoxy functional compounds, having average equivalent weights in the range from about 220 to about 1200, obtained by heating in the presence of a strong acid at about 50.degree. C. to about 250.degree. C.(a) a diaryl compound selected from naphthalene, diphenyl oxide, diphenyl sulfide, their alkylated or halogenated derivatives or mixtures thereof,(B) formaldehyde or formaldehyde-yielding derivative,(C) water, and(D) a hydroxy aliphatic hydrocarbon compound having at least one free hydroxyl group and from 1 to 4 carbon atoms, which mixture contains up to 50 percent by weight unreacted (A); withIi. at least one monomeric phenolic reactant selected from the group ##STR1## WHEREIN R is selected from the group consisting of ##STR2## HYDROGEN, ALKYL RADICAL OF 1-20 CARBON ATOMS, ARYL RADICAL OF 6-20 CARBON ATOMS, WHEREIN R.sub.1 represents hydrogen, alkyl or aryl, m represents an integer from 1 to 3; o represents an integer from 1 to 5; p represents an integer from 0 to 3; X represents oxygen, sulfur or alkylidene; and q represents an integer from 0 to 1; and,Iii. optionally an aldehyde or an aldehyde-yielding derivative or a ketone,For from several minutes to several hours.These polymeric materials are liquids or low melting solids which are capable of further modification to thermoset resins. These polymers are capable of being thermoset by heating at a temperature of from about 130.degree. C. to about 260.degree. C. for from several minutes to several hours in the presence of a formaldehyde-yielding compound. These polymers are also capable of further modification by reacting under basic conditions with formaldehyde with or without a phenolic compound. The polymers, both base catalyzed resoles and acid catalyzed novolacs are useful as laminating, molding, film-forming and adhesive materials. The polymers, both resoles and novolacs, can be epoxidized as well as reacted with a drying oil to produce a varnish resin.
摘要翻译：在酸催化剂存在下，在约65℃和260℃之间加热得到的聚合物

8. 发明授权

US4108808A Novel oxyalkylated polyol prepolymers, flame retardant interpolymers prepared therefrom, and processes for the preparation thereof 失效
标题翻译：新型烷氧基化多元醇预聚物，由其制备的阻燃互聚物及其制备方法
公开(公告)号：US4108808A
公开(公告)日：1978-08-22
申请号：US745049
申请日：1976-11-26
申请人： Thirumurti Narayan , Moses Cenker
发明人： Thirumurti Narayan , Moses Cenker
IPC分类号： C08G16/02 , C08G16/04 , C08G18/54 , C08J9/00
CPC分类号： C08G16/0262 , C08G16/04 , C08G18/546
摘要： Liquid oxyalkylated polyol prepolymers are prepared by oxyalkylating a prepolymer prepared from a hydroxy aromatic compound, an aldehyde and furfuryl alcohol with an alkylene oxide containing about 2-4 carbon atoms. The oxyalkylated polyol prepolymers have a viscosity of 1000-500,000 centipoises at 25.degree. C. and contain about 1.1-6 moles of interpolymerized aldehyde, about 3.1-15 moles of interpolymerized furfuryl alcohol, and about 1-10 moles of interpolymerized alkylene oxide for each mole of interpolymerized hydroxy aromatic compound. The resultant prepolymers are highly reactive and may be further polymerized with or without monomers such as polyisocyanate to produce flame retardant solid or cellular interpolymers. Flame retardant solid or cellular polyurethanes are prepared in one variant by interpolymerizing organic polyisocyanates with the oxyalkylated polyol prepolymers. In another variant, flame retardant closed cell cellular interpolymers are provided. Processes are provided for preparing the aforementioned novel oxyalkylated polyol prepolymers and solid or cellular interpolymers.
摘要翻译：液体烷氧基化多元醇预聚物通过使由羟基芳族化合物，醛和糠醇制备的预聚物与含约2-4个碳原子的烯化氧进行烷氧基化来制备。烷氧基化多元醇预聚物在25℃下的粘度为1000-500,000厘泊，并且含有约1.1-6摩尔的共聚醛，约3.1-15摩尔的共聚糠醇，以及每个约1-10摩尔的互聚环氧烷的共聚羟基芳族化合物。得到的预聚物是高度反应性的并且可以与单体如多异氰酸酯进一步聚合，以产生阻燃固体或细胞互聚物。通过使有机多异氰酸酯与烷氧基化多元醇预聚物共聚制备阻燃固体或细胞聚氨酯。在另一个变体中，提供阻燃闭孔细胞互聚物。提供了制备上述新型烷氧基化多元醇预聚物和固体或细胞互聚物的方法。

9. 发明授权

US3824214A Halovinylidene arylene polymers and process for making the same 失效
标题翻译：亚油酰亚胺聚合物及其制备方法
公开(公告)号：US3824214A
公开(公告)日：1974-07-16
申请号：US34313973
申请日：1973-03-20
申请人： GEN ELECTRIC
发明人： TAKAKOSHI T
IPC分类号： C08G10/00 , C08F16/02 , C08G16/00 , C08G16/02 , C08G16/04 , C08G61/00 , C08G61/12 , C08G5/00
CPC分类号： C08G16/04 , C08F16/02 , C08G16/02 , C08G61/00 , C08G61/12 , Y10T428/31627 , Y10T428/31652 , Y10T428/31688 , Y10T428/31942
摘要： HALOVINYLIDENE ARYLENE POLYMERS ARE PREPARED FROM THE DIHYDROHALOGENATION OF THE POLYMERIC REACTION PRODUCT OF AN AROMATIC COMPOUND CONTAINING NUCLEARLY-BONDED HYDROGEN AND EITHER CHLORAL OR BROMAL, IN THE PRESENCE OF A STRONG ACIDIC CATALYST.

10. 发明授权

US1677417A Resinous composition and process of making same 失效
标题翻译：树脂组合物及其制备方法
公开(公告)号：US1677417A
公开(公告)日：1928-07-17
申请号：US20414427
申请日：1927-07-07
申请人： BAKELITE CORP
发明人： TURKINGTON VICTOR H
IPC分类号： C08G8/28
CPC分类号： C08L61/14 , C08G8/12 , C08G8/34 , C08G16/0225 , C08G16/04 , C08L61/06 , C08L93/04 , C08L101/00

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