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1. 发明授权

US5352246A Dye composition containing a mixture of water-soluble fiber-reactive dyes and method of dyeing with said dye composition 失效
标题翻译：含有水溶性纤维活性染料的混合物的染料组合物和用所述染料组合物染色的方法
公开(公告)号：US5352246A
公开(公告)日：1994-10-04
申请号：US944050
申请日：1992-09-10
申请人： Manfred Hahnke , Marcos Segal , Werner H. Russ , Uwe Mrotzeck , Jutta Reiter , Christine Feuchtner
发明人： Manfred Hahnke , Marcos Segal , Werner H. Russ , Uwe Mrotzeck , Jutta Reiter , Christine Feuchtner
IPC分类号： C09B67/02 , C09B62/503 , C09B67/22 , D06P3/24 , D06P3/60 , D06P1/38 , C09B62/002 , C09B62/006
CPC分类号： C09B67/0041 , C09B62/503 , C09B67/0042 , Y10S8/918
摘要： The invention relates to dye compositions for obtaining level dyeings on carboxamido-containing and hydroxyl-containing fiber materials, which dyeings have comparably good light and wetlightfastness properties, the dye compositions containing dioxazine dyes (I) and disazo dyes (II) (one or more than one from IIa to IIf) in a weight ratio of 90:10 to 10:90, preferably 60:40 to 10:90, in particular 40:60 to 15:85.
摘要翻译：本发明涉及用于在含羧酰氨基和含羟基的纤维材料上获得水平染色的染料组合物，其染色具有相当好的耐光牢度和耐光固性，染料组合物含有二恶嗪染料（I）和二偶氮染料（II）（一种或多种比IIa至IIf的重量比）重量比为90:10至10:90，优选为60:40至10:90，特别是40:60至15:85。

2. 发明授权

US5167668A Process for level exhaust of cellulose fibers with reactive dyes: addition of fixing alkali according to a parabolic time function 失效
标题翻译：具有活性染料的纤维素纤维的排气过程：根据抛物线时间功能添加固定碱
公开(公告)号：US5167668A
公开(公告)日：1992-12-01
申请号：US617944
申请日：1990-11-26
申请人： Manfred Hahnke , Pablo Canora
发明人： Manfred Hahnke , Pablo Canora
IPC分类号： D06P1/00 , D06P3/66 , D06P3/86
CPC分类号： D06P3/66 , D06P1/0004 , Y10S8/918
摘要： In an existing isothermal dyeing process, the alkali required for dye fixation is added to the neutral dyebath under linear or progressive program control. In this process, the amount of alkali added per unit time is small at the beginning and is increased progressively and in accordance with a program. This process passes through a certain (non-controlable) initial phase until the start of dye fixation on the cellulose. As a consequence the rate of fixation passes through a maximum before gradually decreasing when the final state of the dyeing is reached. To shorten the initial phase (waiting time) of dye fixation and to slow down dye fixation during the steepest part, it has proved advantageous according to the invention to add the alkali in accordance with a parabolic program.
摘要翻译：在现有的等温染色工艺中，在线性或逐步程序控制下，将染料固定所需的碱加入到中性染浴中。在这个过程中，单位时间内添加的碱的量在开始时很小，并且按照程序逐渐增加。该过程通过一定的（不可控制的）初始阶段，直到染料固定在纤维素上。因此，当达到染色的最终状态时，定影速率在逐渐降低之前经过最大值。为了缩短染色剂固定的初始阶段（等待时间）和减缓最陡部分的染色剂固定，根据本发明，根据抛物线程序添加碱是有利的。

3. 发明授权

US4769449A Red mono-azo water-soluble dye containing cyano, amide and amino substituents 失效
标题翻译：含有氰基，酰胺和氨基取代基的红色偶氮水溶性染料
公开(公告)号：US4769449A
公开(公告)日：1988-09-06
申请号：US11103
申请日：1987-02-05
申请人： Ulrich Buhler , Manfred Hahnke , Michael Kunze , Albert Bode
发明人： Ulrich Buhler , Manfred Hahnke , Michael Kunze , Albert Bode
IPC分类号： C09B29/085 , C09B29/01 , C09B29/08 , C09B67/22 , D06P1/18
CPC分类号： C09B67/0051 , C09B29/0003 , C09B29/0813 , D06P1/18 , Y10S534/01
摘要： Azo dyes of the formula ##STR1## wherein R.sup.1 is alkyl having 1 to 4 carbon atoms; R.sup.2 is alkyl having 1 to 3 carbon atoms; R.sup.3 is alkylcarbonyloxyethyl having 1 to 3 carbon atoms in the alkyl moiety, alkoxycarbonyloxyethyl having 1 to 4 carbon atoms in the alkoxy moiety, methoxyethoxycarbonyloxyethyl or ethoxyethoxycarbonyloxyethyl; and R.sup.4 is one of the definitions of R.sup.3 or cyanoethyl; or mixtures of at least two species of said formula are used for dyeing and printing hydrophobic fiber materials.
摘要翻译：其中R 1是具有1至4个碳原子的烷基的式“IMAGE”的偶氮染料; R2是具有1至3个碳原子的烷基; R3是在烷基部分具有1至3个碳原子的烷基羰氧基乙基，在烷氧基部分具有1至4个碳原子的烷氧基羰氧基乙基，甲氧基乙氧基羰基氧基乙基或乙氧基乙氧基羰基氧基乙基; R4是R3或氰乙基的定义之一; 或至少两种所述配方的混合物用于染色和印刷疏水纤维材料。

4. 发明授权

US4765797A Storable formulations of cationic dyes with oxidizing agent as stabilizer 失效
标题翻译：阳离子染料与氧化剂作为稳定剂的可储存配方
公开(公告)号：US4765797A
公开(公告)日：1988-08-23
申请号：US58983
申请日：1987-06-08
申请人： Manfred Hahnke , Sierling Ong , Kurt Hohmann
发明人： Manfred Hahnke , Sierling Ong , Kurt Hohmann
IPC分类号： C09B67/22 , C09B67/32 , C09B67/34
CPC分类号： C09B67/0033 , C09B67/0075 , C09B67/0076
摘要： Liquid formulations of mixtures of cationic dyes frequently have a very short storage life. As a consequence, these formulations give rise to customer complaints concerning incorrect dyeing strengths and hues and concerning isoluble constituents. It has now been found according to the invention that powder formulations and in particular liquid formulations of cationic dyes or of mixtures of these dyes can be stabilized by adding selected oxidizing agents.
摘要翻译：阳离子染料混合物的液体配方通常具有非常短的储存寿命。因此，这些配方引起客户对不正确的染色强度和色调以及涉及可分离成分的投诉。现在已经发现，根据本发明，可以通过加入选择的氧化剂来稳定粉末制剂，特别是阳离子染料的液体制剂或这些染料的混合物。

5. 发明授权

US5234465A Pad-dyeing of cellulose fibers with sulfur black dyes: mixture of dithionite and glucose reducing sugar as reducing agent in aqueous alkaline dye bath 失效
标题翻译：纤维素纤维与硫化黑色染色体的染色：脱水和葡萄糖降低糖的混合作为还原剂在水性碱性染色浴中
公开(公告)号：US5234465A
公开(公告)日：1993-08-10
申请号：US827290
申请日：1992-01-29
申请人： Manfred Hahnke , Ullrich Saalfrank , Claus Schuster , Joachim Steinbach , Gerd Krauzpaul
发明人： Manfred Hahnke , Ullrich Saalfrank , Claus Schuster , Joachim Steinbach , Gerd Krauzpaul
IPC分类号： D06P1/30 , D06P3/60
CPC分类号： D06P1/30 , D06P3/6025 , Y10S8/918
摘要： Cellulose fibers are dyed ecologically soundly with sulfur black dyes by the pad-dyeing process by avoiding sulfides as reducing agent by replacing them by a dithionite-based mixture with at least one reducing sugar. A high color yield, a deep black shade and good reproducibility are ensured. The preferred reducing sugar is glucose.
摘要翻译：纤维素纤维用硫化黑染料通过垫染染方法生态地染色，通过用至少一种还原糖的连二亚硫酸盐基混合物代替硫化物作为还原剂。确保了高产率，深黑色和良好的再现性。优选的还原糖是葡萄糖。

6. 发明授权

US4985043A Mixtures of monoazo dyes containing halogen and cyano substituents 失效
标题翻译：含有卤素和氰基取代基的单偶氮染料的混合物
公开(公告)号：US4985043A
公开(公告)日：1991-01-15
申请号：US323876
申请日：1989-03-15
申请人： Ulrich Buhler , Manfred Hahnke , Reinhard Kuhn , Margarete Boos
发明人： Ulrich Buhler , Manfred Hahnke , Reinhard Kuhn , Margarete Boos
IPC分类号： C09B67/22
CPC分类号： C09B67/0051 , Y10S534/01
摘要： Mixtures of monoazo dyes suitable for dyeing and printing hydrophobic fiber materials and mixtures thereof with natural fibers contain one or more dyes of the formula I ##STR1## and one or more dyes of the formula II ##STR2## in which Hal denotes bromo or chloro; R.sup.1 and R.sup.2, independently of one another, denote methyl or ethyl; R.sup.3, R.sup.4, R.sup.5 and R.sup.6, independently of one another, denote linear alkyl having 1 to 4 carbon atoms or alkenyl having 3 or 4 carbon atoms; and R denotes methyl, acetylamino, propionylamino, i-butyrylamino, or n-butyrylamino.
摘要翻译：适用于染色和印刷疏水纤维材料及其与天然纤维的混合物的单偶氮染料的混合物含有一种或多种式I（I）的染料和一种或多种式II（II）的染料，其中 Hal表示溴或氯; R1和R2彼此独立地表示甲基或乙基; R3，R4，R5和R6彼此独立地表示具有1至4个碳原子的直链烷基或具有3或4个碳原子的烯基; R表示甲基，乙酰氨基，丙酰氨基，异丁酰氨基或正丁酰氨基。

7. 发明授权

US4705524A Mixtures of water-soluble fiber-reactive dyes and use thereof for dyeing: dioxazine and disazo dyes 失效
标题翻译：水溶性纤维活性染料的混合物及其用于染色的用途：二恶嗪和二偶氮染料
公开(公告)号：US4705524A
公开(公告)日：1987-11-10
申请号：US934688
申请日：1986-11-25
申请人： Manfred Hahnke , Marcos Segal
发明人： Manfred Hahnke , Marcos Segal
IPC分类号： C09B67/22 , C09B67/24 , D06P1/38 , D06P3/66 , C09B67/00
CPC分类号： C09B67/0042 , C09B67/004 , C09B67/0041 , Y10S8/917 , Y10S8/918 , Y10S8/924
摘要： The invention relates to dye compositions for preparing level dyeings on carboxamide- or hydroxyl-containing fiber materials of comparatively good light fastness properties, which contain dioxazine dyes I (Ia and/or Ib) and II (one or more of IIa to IId) in a weight ratio of 90:10 to 10:90 ##STR1## where in each case independently of one another Z denotes vinyl or .beta.-sulfatoethyl,Z' denotes vinyl-SO.sub.2 or .beta.-sulfatoethyl-SO.sub.2 --,R denotes sulfo or --SO.sub.2 --NR.sup.8 R.sup.9, wherein R.sup.8 is H or substituted or unsubstituted C.sub.1 -C.sub.4 -alkyl and R.sup.9 is H, C.sub.1 -C.sub.4 -alkyl which can be substituted by sulfato, sulfo, carboxyl or phosphato, or is an arylated C.sub.1 -C.sub.4 -alkyl group which can be substituted in the aryl radical by sulfo or carboxyl,R.sup.1 denotes H or substituted or unsubstituted C.sub.1 -C.sub.4 -alkyl,R.sup.2 denotes C.sub.1 -C.sub.4 -alkyl which can be substituted by sulfato, suflo, carboxyl or phosphato, or optionally sulfo- or carboxyl-substituted aryl or alkylaryl having 1 to 4 carbon atoms in the alkyl radical,R.sup.3 C.sub.1 -C.sub.4 -alkyl which can be substituted by sulfato, sulfo, carboxyl or phosphato, or denotes phenyl which is substituted by sulfo or carboxyl,R.sup.4 and R.sup.5 denote H, sulfo, carboxyl, C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy or Br,R.sup.6 denotes C.sub.1 -C.sub.4 -alkyl, --OH, sulfo, carboxyl or Cl,R.sup.7 denotes sulfo, carboxyl or --SO.sub.2 --NR.sup.8 R.sup.9, where R.sup.8 and R.sup.9 have the abovementioned meaning,n denotes 1, 2 or 3 andM denotes H or an alkali metal.
摘要翻译：本发明涉及用于制备具有相对良好的耐光性的含羧基酰胺或含羟基纤维材料的染色组合物，其含有二恶嗪染料I（Ia和/或Ib）和II（IIa至IId中的一种或多种）在重量比为90:10至10:90（I）Ia：A = NR1R2; II = D1 = IID：D1 = II图像D1 = IIc：D1 = Z表示乙烯基或β-磺基乙基，Z'表示乙烯基-SO 2或β-磺基乙基-SO 2 - ，R表示磺基或-SO 2 -NR 8 R 9，其中R 8为H或取代或未取代的C 1 -C 4 - 烷基，R 9为 H，可被硫酸根，磺基，羧基或磷酸取代的C 1 -C 4烷基，或者是可被磺基或羧基在芳基中被取代的芳基化C1-C4-烷基，R1表示H或取代或未取代的 C 1 -C 4 - 烷基，R 2表示可被硫酸根，磺酰基，羧基或磷酸酯取代的C 1 -C 4 - 烷基，或任选地在烷基中具有1至4个碳原子的磺基或羧基取代的芳基或烷基芳基，R 3 C1 可被硫酸根，磺基，羧基或磷酸取代的C 4-烷基，或表示被磺基或羧基取代的苯基，R 4和R 5表示H，磺基，羧基，C 1 -C 4 - 烷基，C 1 -C 4 - 烷基氧基或Br，R6表示C1-C4-烷基，-OH，磺基，羧基或C1，R7表示磺基，羧基或-SO2-NR8R9，其中R8和R9具有上述含义，n表示1,2或3，M 表示H或碱金属。

8. 发明授权

US4620853A Dyestuff mixtures, process for their preparation and process for dyeing and printing hydrophobic fiber materials 失效
标题翻译：染料混合物，其制备方法和染色和印刷疏水纤维材料的方法
公开(公告)号：US4620853A
公开(公告)日：1986-11-04
申请号：US806448
申请日：1985-12-09
申请人： Horst Tappe , Klaus Hofmann , Manfred Hahnke , Albert Bode
发明人： Horst Tappe , Klaus Hofmann , Manfred Hahnke , Albert Bode
IPC分类号： C09B67/22 , D06P1/18 , D06P3/54 , D06P3/87 , C09B29/15
CPC分类号： C09B67/0051 , D06P1/18 , Y10S534/01
摘要： Dyestuff mixtures which contain dyestuffs (A) of the formula ##STR1## and dyestuff (B) of the formula ##STR2## in an (A):(B) weight ratio of (80 to 60):(20 to 40) useful for dyeing and printing hydrophobic fiber materials.
摘要翻译：和（A）:( B）重量比为（80〜60）：（20〜40）的式（IMA）的染料（A）和式（IMAGE）的染料（B）染色和印花疏水纤维材料。

9. 发明授权

US4061464A Process for the preparation of dyestuff compositions 失效
公开(公告)号：US4061464A
公开(公告)日：1977-12-06
申请号：US620385
申请日：1975-10-07
申请人： Manfred Hahnke , Kurt Hohmann , Theodor Papenfuhs
发明人： Manfred Hahnke , Kurt Hohmann , Theodor Papenfuhs
IPC分类号： C09B1/28 , C09B1/503 , C09B11/10 , C09B11/20 , C09B11/22 , C09B11/26 , C09B11/28 , C09B29/00 , C09B31/02 , C09B67/42 , C09B67/00
CPC分类号： C09B1/28 , C09B1/503 , C09B11/10 , C09B11/20 , C09B11/22 , C09B11/26 , C09B11/28 , C09B29/00 , C09B31/02 , C09B67/0071 , Y10S8/907
摘要： A process for the preparation of new dyestuff compositions which contain one or more basic dyestuffs in the form of dyestuff bases from the series of the triarylmethane, indoldiarylmethane, azine, oxazine, thiazine or xanthene dyestuffs or one or more basic dyestuffs of the series of the azo, anthraquinone, phthalocyanine, styryl, quinophthalone, benzoxanthene, naphthoylene-benzimidazole, naphthalimide or nitro series, carrying a primary, secondary or tertiary amino group or a guanidino or hydrazino group, as well as one or more non-ionic or slightly cationic surface-active agents and, optionally, water and/or an organic solvent miscible with water, which process comprises synthesizing the dyestuff in the surface-active agent optionally containing water and/or an organic solvent miscible with water, and then adding, if necessary, water and/or a solvent miscible with water and a further surface-active agent, this process of the invention having the advantage that an intermediate isolation, drying or grinding of the dyestuffs contained in the dyestuff compositions defined above is not necessary, so that the dyestuffs need not be introduced as substance into the surface-active agent and the solvent in a process wherein compositions of this type are prepared by a usual mixing, kneading or melting process; moreover, higher dyestuff yields are obtained in the dyestuff synthesis, and it allows to prepare dyestuff compositions from dyestuffs which are difficult to be isolated in substance after synthesis and often precipitate as oily or smeary products. The dyestuff compositions obtained according to the process of the invention, which are pastes or liquids, have a high stability upon storage. After being diluted with an aqueous solution of an amount at least equivalent to the dyestuff of an inorganic or organic acid, as well as, optionally, after the addition of dyeing and/or printing auxiliaries, the novel dyestuff compositions are suitable for dyeing or printing textile material containing acid groups.

10. 发明授权

US4985044A Multi-component mixtures of blue disperse azo dyes for the dyeing of synthetic fibers 失效
标题翻译：用于染色合成纤维的蓝色分散偶氮染料的多组分混合物
公开(公告)号：US4985044A
公开(公告)日：1991-01-15
申请号：US362845
申请日：1989-06-07
申请人： Manfred Hahnke , Reinhard Kuhn , Ulrich Buhler
发明人： Manfred Hahnke , Reinhard Kuhn , Ulrich Buhler
IPC分类号： C09B67/22 , D06P3/54 , D06P3/87
CPC分类号： C09B67/0051 , Y10S8/921 , Y10S8/922
摘要： Since anthraquinonoid disperse dyes of the dark blue and navy region give only a low color strength on synthetic fibers, there was an urgent need for their coloristically advantageous substitution by high performance blue azo dyes which are suitable for being used in the carrier dyeing process.According to the invention, the systematic development of multi-component mixtures based on selected blue azo dyes from the dicyano azo series makes it possible to avoid most of the disadvantages mentioned.
摘要翻译：由于深蓝色和海军区域的蒽醌类分散染料在合成纤维上仅具有低的着色强度，所以迫切需要通过适合用于载体染色过程的高性能蓝色偶氮染料进行色泽上有利的取代。根据本发明，基于来自二氰偶氮系列的选择的蓝色偶氮染料的多组分混合物的系统开发使得可以避免所提及的大多数缺点。

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