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1. 再颁专利

USRE40728E1 Acid functional polymers based on benzocyclobutene 有权
公开(公告)号：USRE40728E1
公开(公告)日：2009-06-09
申请号：US10808270
申请日：2004-03-24
申请人： Ying H. So , Robert A. DeVries , Mitchell G. Dibbs , Robert L. McGee , Edward O. Shaffer, II , Michael J. Radler , Richard P. DeCaire
发明人： Ying H. So , Robert A. DeVries , Mitchell G. Dibbs , Robert L. McGee , Edward O. Shaffer, II , Michael J. Radler , Richard P. DeCaire
IPC分类号： G03F7/038 , G03F7/039 , G03F7/021 , G03F7/023
CPC分类号： C08G61/06 , C08G77/04 , G03F7/0045 , G03F7/027 , G03F7/0755 , G03F7/0757 , G03F7/095
摘要： The invention is a curable cyclobutarene based polymer comprising acid functional pendant groups. The cured polymer displays excellent qualities of toughness, adhesion, dielectric constant, and low stress. The preferred system is soluble in an aqueous base and can be used to generate patterned films with excellent resolution without the need to handle organic developer solvents.

2. 发明授权

US5567835A Preparation of a vinylsiloxane-benzocylobutene from a hydrolyzable vinylsilane-benzocylobutene 失效
标题翻译：由可水解的乙烯基硅烷 - 苯并环丁烯制备乙烯基硅氧烷 - 苯并二烯
公开(公告)号：US5567835A
公开(公告)日：1996-10-22
申请号：US549136
申请日：1995-10-27
申请人： Robert A. DeVries , Edmund J. Stark
发明人： Robert A. DeVries , Edmund J. Stark
IPC分类号： C07F7/08 , C07F7/14 , C08G77/20
CPC分类号： C07F7/0874 , C07F7/14 , C08G77/20
摘要： This invention relates to a novel process for preparing vinylsiloxane-BCBs (vinylsiloxane-benzocyclobutenes) comprising reacting a hydrolyzable hydrosilating reagent with an acetylene-BCB in the presence of a catalyst, then hydrolyzing the hydrolyzable vinylsilane-BCB to form a vinylsiloxane-BCB.
摘要翻译：本发明涉及制备乙烯基硅氧烷-BCBs（乙烯基硅氧烷 - 苯并环丁烯）的新方法，其包括在催化剂存在下使可水解氢化硅烷化试剂与乙炔-BCB反应，然后水解可水解的乙烯基硅烷-BCB以形成乙烯基硅氧烷-BCB。

3. 发明授权

US5532817A Method of optical inspection 失效
标题翻译：光学检查方法
公开(公告)号：US5532817A
公开(公告)日：1996-07-02
申请号：US317089
申请日：1994-10-03
申请人： Robert A. DeVries , Reed A. Shick , G. Thomas Wells , Joseph N. Carr
发明人： Robert A. DeVries , Reed A. Shick , G. Thomas Wells , Joseph N. Carr
IPC分类号： C09K11/06 , G01N21/64 , G01B11/02 , G01B15/02
CPC分类号： G01N21/64 , C09K11/06 , G01N2021/646 , G01N21/8422
摘要： A method for determining the configuration of a resin portion of an article comprising exposing the article to a light source at a first wavelength and measuring emission of light at a second, different wavelength; wherein the resin contains a moiety containing a structure of the formula: ##STR1## or a moiety which is a reaction product of said moiety in a quantity sufficient to impart fluorescent properties to said resin.
摘要翻译：一种用于确定制品的树脂部分的构造的方法，包括将制品暴露于第一波长的光源并测量第二不同波长的光的发射; 其中所述树脂包含含有下式结构的部分：其中所述部分的反应产物的量足以赋予所述树脂荧光性质。

4. 发明授权

US5248829A Production of acetylated aromatic compounds 失效
标题翻译：乙酰化芳族化合物的生产
公开(公告)号：US5248829A
公开(公告)日：1993-09-28
申请号：US911230
申请日：1992-07-09
申请人： Robert A. DeVries
发明人： Robert A. DeVries
IPC分类号： C07C45/51 , C07C205/45
CPC分类号： C07C201/12 , C07C45/513 , C07C2101/04
摘要： This invention is a process for the production of acetylated aromatic products, including acetyl benzoeyclobutenes, in one step and in high yield. The process comprises contacting an aryl halide with an alkyl vinyl ether in the presence of a zerovalent palladium catalyst complex and a hydrogen halide acceptor in a aqueous solvent mixture containing at least about one molar equivalent of water based on moles of the aryl halide.
摘要翻译：本发明是一步法生产乙酰化芳香族产物，包括乙酰基苯并环丁烯的方法，高产率。该方法包括在零价钯催化剂配合物和卤化氢受体存在下，将芳基卤与烷基乙烯基醚在含有基于芳基卤的摩尔数的至少约1摩尔当量水的含水溶剂混合物中接触。

5. 发明授权

US5138081A Process for purifying vinylically-unsaturated organosilicon compounds 失效
标题翻译：乙烯基不饱和有机硅化合物的纯化方法
公开(公告)号：US5138081A
公开(公告)日：1992-08-11
申请号：US694521
申请日：1991-04-30
申请人： Robert A. DeVries , Mary L. Ash , Hughie R. Frick, deceased
发明人： Robert A. DeVries , Mary L. Ash , Hughie R. Frick, deceased
IPC分类号： C07F7/08 , C07F7/18 , C07F7/20
CPC分类号： C07F7/1896 , C07F7/0889 , C07F7/089 , C07F7/1892 , C07F7/20
摘要： A process for purifying an impure vinylically-unsaturated organosilicon product compound prepared by reaction between a vinylically-unsaturated organosilicon precursor and a halogenated organic compound in the presence of a homogeneous zerovalent palladium catalyst complex, the catalyst complex including an organophosphine or organoarsine ligand, in the presence of a hydrogen halide acceptor in an essentially anhydrous diluent, comprising treating a mixture containing the impure vinylically-unsaturated organosilicon product compound with a peroxide for a time sufficient to oxidize organophosphine or organoarsine impurities present in a mixture being treated. The peroxide can be selected from aqueous hydrogen peroxide or organic peroxides. The thus-treated mixture can be further treated by chromatography over silica gel or alumina. In optional embodiments, chromatography over silica gel or alumina can precede treatment with the peroxide.
摘要翻译：一种在均相的零价钯催化剂络合物（包括有机膦或有机砷配体）的催化剂络合物的存在下，通过在乙烯基不饱和有机硅前体和卤代有机化合物之间的反应制备的不纯的乙烯基不饱和有机硅产物化合物的方法，在基本上无水的稀释剂中存在卤化氢受体，包括用过氧化物处理含有不纯的乙烯基不饱和有机硅产物化合物的混合物足以氧化存在于待处理的混合物中的有机膦或有机砷杂质。过氧化物可以选自过氧化氢水溶液或有机过氧化物。这样处理的混合物可以通过硅胶或氧化铝上的色谱进一步处理。在任选的实施方案中，硅胶或氧化铝上的色谱可以在用过氧化物处理之前进行。

6. 发明授权

US5310809A Arylcyclobutene grafted polyolefins 失效
标题翻译：芳基环丁烯接枝聚烯烃
公开(公告)号：US5310809A
公开(公告)日：1994-05-10
申请号：US64533
申请日：1993-05-20
申请人： Raul A. Pabon, Jr. , Robert A. DeVries
发明人： Raul A. Pabon, Jr. , Robert A. DeVries
IPC分类号： C08F255/02 , C08L51/06
CPC分类号： C08F255/02
摘要： An olefinic polymer is grafted with a vinyl arylcyclobutene such as 4-vinylbenzocyclobutene. The arylcyclobutene grafted olefinic polymers are useful in a number of industrial applications including electronics, and as coatings, membranes, fibers, structural composites, adhesives, and wrapping and packaging films.
摘要翻译：烯烃聚合物用乙烯基芳基环丁烯如4-乙烯基苯并环丁烯接枝。芳基环丁烯接枝的烯属聚合物可用于许多工业应用，包括电子器件，以及作为涂层，膜，纤维，结构复合材料，粘合剂和包装和包装膜。

7. 发明授权

US5264646A Process for preparing vinylically-unsaturated compounds 失效
标题翻译：制备乙烯基不饱和化合物的方法
公开(公告)号：US5264646A
公开(公告)日：1993-11-23
申请号：US677023
申请日：1991-03-28
申请人： Robert A. DeVries , Gregory F. Schmidt , Hughie R.* Frick , Bonnie Frick
发明人： Robert A. DeVries , Gregory F. Schmidt , Hughie R.* Frick , Bonnie Frick
IPC分类号： C07B37/04 , C07B63/02 , C07F7/08 , C07F7/18 , C07F7/20 , C07C1/30
CPC分类号： C07F7/0889 , C07B37/04 , C07B63/02 , C07F7/0849 , C07F7/1892 , C07F7/1896 , C07F7/20
摘要： A process for preparing a vinylically-unsaturated product compound comprises reacting a halogenated organic compound with a hydrolytically-stable, vinylically-unsaturated precursor compound in the presence of (a) a homogeneous zerovalent palladium catalyst complex, (b) an organic hydrogen halide acceptor and (c) a diluent, wherein the diluent is water or an aqueous solution containing up to 95% by volume of an organic solvent. The halogenated organic compound is selected from aryl halides, benzyl halides or vinylic halides. The hydrolytically-stable, vinylically-unsaturated precursor compound is selected from organosilicon compounds, hydrocarbon compounds or compounds containing at least one of an oxygen atom, a nitrogen atom, a sulfur atom, a phosphorus atom or a combination thereof.
摘要翻译：制备乙烯基不饱和产物化合物的方法包括在（a）均相的零价钯催化剂络合物，（b）有机卤化氢受体和（b）有机卤化氢受体的存在下使卤代有机化合物与水解稳定的乙烯基不饱和前体化合物反应，（c）稀释剂，其中稀释剂是水或含有至多95％（体积）有机溶剂的水溶液。卤代有机化合物选自芳基卤化物，苄基卤化物或乙烯基卤化物。水解稳定的乙烯基不饱和前体化合物选自有机硅化合物，烃化合物或含有氧原子，氮原子，硫原子，磷原子或其组合中的至少一个的化合物。

8. 发明授权

US5243068A Process for preparing vinylically-unsaturated compounds (II) 失效
标题翻译：制备乙烯基不饱和化合物（II）的方法
公开(公告)号：US5243068A
公开(公告)日：1993-09-07
申请号：US877580
申请日：1992-05-01
申请人： Robert A. DeVries , Hughie R. Frick, deceased
发明人： Robert A. DeVries , Hughie R. Frick, deceased
IPC分类号： C07F7/08 , C07F7/20
CPC分类号： C07F7/20 , C07F7/0849 , C07F7/0889
摘要： A process for preparing a vinylically-unsaturated product compound comprises reacting a halogenated organic compound with a hydrolytically-stable, vinylically-unsaturated precursor compound in the presence of (a) a homogeneous zerovalent palladium catalyst complex, (b) an inorganic hydrogen halide acceptor and (c) a diluent, wherein the diluent is water or an aqueous solution containing up to 95% by volume of an organic solvent. The halogenated organic compound is selected from aryl halides, benzyl halides or vinylic halides. The hydrolytically-stable, vinylically-unsaturated precursor compound is selected from hydrocarbon compounds or compounds containing at least one of an oxygen atom, a nitrogen atom, a sulfur atom, a phosphorus atom or a combination thereof.
摘要翻译：一种制备乙烯基不饱和产物化合物的方法包括在（a）均匀的零价钯催化剂络合物，（b）无机卤化氢受体和（b）无机卤化氢受体的存在下使卤代有机化合物与水解稳定的乙烯基不饱和前体化合物反应，（c）稀释剂，其中稀释剂是水或含有至多95％（体积）有机溶剂的水溶液。卤代有机化合物选自芳基卤化物，苄基卤化物或乙烯基卤化物。水解稳定的乙烯基不饱和前体化合物选自烃化合物或含有氧原子，氮原子，硫原子，磷原子或其组合中的至少一种的化合物。

9. 发明授权

US5136069A Process for preparing vinylically-unsaturated compounds (II) 失效
标题翻译：制备乙烯基不饱和化合物（II）的方法
公开(公告)号：US5136069A
公开(公告)日：1992-08-04
申请号：US676622
申请日：1991-03-28
申请人： Robert A. DeVries , Hughie R. Frick, deceased
发明人： Robert A. DeVries , Hughie R. Frick, deceased
IPC分类号： C07F7/08 , C07F7/20
CPC分类号： C07F7/0889 , C07F7/0849 , C07F7/20
摘要： A process for preparing a vinylically-unsaturated product compound comprises reacting a halogenated organic compound with a hydrolytically-stable, vinylically-unsaturated precursor compound in the presence of (a) a homogeneous zerovalent palladium catalyst complex, (b) an inorganic hydrogen halide acceptor and (c) diluent, wherein the diluent is water or an aqueous solution containing up to 95% by volume of an organic solvent. The halogenated organic compound is selected from aryl halides, benzyl halides or vinylic halides. The hydrolytically-stable, vinylically-unsaturated precursor compound is selected from hydrocarbon compounds or compounds containing at least one of an oxygen atom, a nitrogen atom, a sulfur atom, a phosphorus atom, silicon atom or a combination thereof.
摘要翻译：一种制备乙烯基不饱和产物化合物的方法包括在（a）均匀的零价钯催化剂络合物，（b）无机卤化氢受体和（b）无机卤化氢受体的存在下使卤代有机化合物与水解稳定的乙烯基不饱和前体化合物反应，（c）稀释剂，其中稀释剂是水或含有至多95％（体积）有机溶剂的水溶液。卤代有机化合物选自芳基卤化物，苄基卤化物或乙烯基卤化物。水解稳定的乙烯基不饱和前体化合物选自含有氧原子，氮原子，硫原子，磷原子，硅原子或其组合中的至少一种的烃化合物或化合物。

10. 发明授权

US5077367A Crystalline syndiotactic copolymers from arylcyclobutene functional monomers and vinyl aromatic monomers 失效
标题翻译：来自芳香族官能单体和乙烯芳族单体的结晶聚合共聚物
公开(公告)号：US5077367A
公开(公告)日：1991-12-31
申请号：US541455
申请日：1990-06-22
申请人： Richard E. Campbell, Jr. , Robert A. DeVries
发明人： Richard E. Campbell, Jr. , Robert A. DeVries
IPC分类号： C08F12/12 , C08F4/645 , C08F12/00 , C08F12/32 , C08F212/00 , C08F212/08 , C08F212/32 , C08J3/24
CPC分类号： C08F12/32 , C08J3/24 , Y10S526/902 , Y10S526/943
摘要： Syndiotactic homopolymers of an arylcyclobutene functional monomer and syndiotactic copolymers of an arylcyclobutene functional monomer and a vinylaromatic monomer are prepared by conducting the polymerization in the presence of a catalytic amount of a suitable coordination catalyst such as the reaction product of polymethylaluminoxane and a transition metal compound.

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