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1. 发明授权

US09012690B2 Method for producing alcohol and/or amine from amide compound 有权
标题翻译：从酰胺化合物制备醇和/或胺的方法
公开(公告)号：US09012690B2
公开(公告)日：2015-04-21
申请号：US13825449
申请日：2011-09-01
申请人： Osamu Ogata , Wataru Kuriyama , Takaji Matsumoto
发明人： Osamu Ogata , Wataru Kuriyama , Takaji Matsumoto
IPC分类号： C07C209/00 , C07C209/50 , C07B41/02 , C07B43/04 , C07C29/149 , C07C209/62 , C07D295/18 , C07C29/36 , C07D295/02
CPC分类号： C07C209/50 , B01J31/1805 , B01J31/189 , B01J31/20 , B01J31/24 , B01J2231/643 , B01J2531/821 , C07B41/02 , C07B43/04 , C07C29/149 , C07C29/36 , C07C209/62 , C07D295/02 , C07D295/18 , C07C211/04 , C07C211/46 , C07C211/48 , C07C211/55 , C07C31/125 , C07C33/22
摘要： Disclosed herein is a method for producing an alcohol and an amine from an amide under an atmosphere of hydrogen with the use of, as a catalyst, a ruthenium complex that is easily prepared, easy to handle, and relatively cheaply obtained. Specifically, the method is a method for producing an alcohol and/or an amine from an amide compound under an atmosphere of hydrogen with the use of as a catalyst, a ruthenium carbonyl complex represented by the following general formula (1): RuXY(CO)(L) (1) wherein X and Y may be the same or different from each other and each represents an anionic ligand and L represents a tridentate aminodiphosphine ligand containing two phosphino groups and a —NH— group.
摘要翻译：本文公开了一种在氢气氛下由酰胺制备醇和胺的方法，其中使用易于制备，易于处理和相对便宜地获得的钌络合物作为催化剂。具体地说，该方法是使用作为催化剂的氢气气氛下的酰胺化合物制备醇和/或胺的方法，由以下通式（1）表示的羰基钌络合物：RuXY（CO ）（L）（1）其中X和Y可以相同或不同，各自表示阴离子配体，L表示含有两个膦基和-NH-基团的三齿氨基二膦配体。

2. 发明申请

US20130172619A1 METHOD FOR PRODUCING ALCOHOL AND/OR AMINE FROM AMIDE COMPOUND 有权
标题翻译：从酰胺化合物生产醇和/或胺的方法
公开(公告)号：US20130172619A1
公开(公告)日：2013-07-04
申请号：US13825449
申请日：2011-09-01
申请人： Osamu Ogata , Wataru Kuriyama , Takaji Matsumoto
发明人： Osamu Ogata , Wataru Kuriyama , Takaji Matsumoto
IPC分类号： C07C209/50 , C07C29/36
CPC分类号： C07C209/50 , B01J31/1805 , B01J31/189 , B01J31/20 , B01J31/24 , B01J2231/643 , B01J2531/821 , C07B41/02 , C07B43/04 , C07C29/149 , C07C29/36 , C07C209/62 , C07D295/02 , C07D295/18 , C07C211/04 , C07C211/46 , C07C211/48 , C07C211/55 , C07C31/125 , C07C33/22
摘要： Disclosed herein is a method for producing an alcohol and an amine from an amide under an atmosphere of hydrogen with the use of, as a catalyst, a ruthenium complex that is easily prepared, easy to handle, and relatively cheaply obtained. Specifically, the method is a method for producing an alcohol and/or an amine from an amide compound under an atmosphere of hydrogen with the use of as a catalyst, a ruthenium carbonyl complex represented by the following general formula (1): RuXY(CO)(L) (1) wherein X and Y may be the same or different from each other and each represents an anionic ligand and L represents a tridentate aminodiphosphine ligand containing two phosphino groups and a —NH— group.
摘要翻译：本文公开了一种在氢气氛下由酰胺制备醇和胺的方法，其中使用易于制备，易于处理和相对便宜地获得的钌络合物作为催化剂。具体地说，该方法是使用作为催化剂的氢气气氛下的酰胺化合物制备醇和/或胺的方法，由以下通式（1）表示的羰基钌络合物：RuXY（CO ）（L）（1）其中X和Y可以相同或不同，各自表示阴离子配体，L表示含有两个膦基和-NH-基团的三齿氨基二膦配体。

3. 发明授权

US08471048B2 Ruthenium carbonyl complex having tridentate ligand, its production method and use 有权
标题翻译：具有三齿配体的钌羰基络合物，其制备方法和用途
公开(公告)号：US08471048B2
公开(公告)日：2013-06-25
申请号：US13121990
申请日：2010-06-30
申请人： Wataru Kuriyama , Takaji Matsumoto , Yasunori Ino , Osamu Ogata
发明人： Wataru Kuriyama , Takaji Matsumoto , Yasunori Ino , Osamu Ogata
IPC分类号： C07F5/02 , C07F15/00 , C07C209/00 , C07C29/00
CPC分类号： C07B53/00 , C07B2200/07 , C07C29/145 , C07C29/149 , C07C29/177 , C07C41/26 , C07C213/08 , C07C269/06 , C07F9/5022 , C07F15/0046 , C07F15/0053 , C07C33/22 , C07C31/205 , C07C31/20 , C07C43/13 , C07C43/1782 , C07C271/16 , C07C215/16
摘要： The present invention relates to a ruthenium carbonyl complex that is represented by the following Formula (1): RuXY(CO)(L) (1) (in the Formula (1), X and Y, which may be the same or different from each other, represent an anionic ligand and L represents a tridentate aminodiphosphine ligand which has two phosphino groups and a —NH— group), its production method, and a method for production of alcohols by hydrogenation-reduction of ketones, esters, and lactones using the complex as a catalyst.The ruthenium carbonyl complex of the invention has a high catalytic activity and it can be easily prepared and handled.
摘要翻译：本发明涉及由下式（1）表示的羰基钌羰基络合物：RuXY（CO）（L）（1）（在式（1）中，X和Y可以相同或不同彼此表示阴离子配体，L表示具有两个膦基和-NH-基团的三齿氨基二膦配体），其制备方法和通过酮，酯和内酯的氢化还原来制备醇的方法，其使用该复合物作为催化剂。本发明的羰基钌络合物具有很高的催化活性，可以容易地制备和处理。

4. 发明申请

US20110237814A1 NOVEL RUTHENIUM CARBONYL COMPLEX HAVING TRIDENTATE LIGAND, ITS PRODUCTION METHOD AND USE 有权
标题翻译：具有三齿配子的新型亚麻烃复合物及其生产方法和用途
公开(公告)号：US20110237814A1
公开(公告)日：2011-09-29
申请号：US13121990
申请日：2010-06-30
申请人： Wataru Kuriyama , Takaji Matsumoto , Yasunori Ino , Osamu Ogata
发明人： Wataru Kuriyama , Takaji Matsumoto , Yasunori Ino , Osamu Ogata
IPC分类号： C07F19/00 , C07C29/149 , C07C269/06 , C07C41/18 , C07C209/68 , C07F7/18 , C07C29/145
CPC分类号： C07B53/00 , C07B2200/07 , C07C29/145 , C07C29/149 , C07C29/177 , C07C41/26 , C07C213/08 , C07C269/06 , C07F9/5022 , C07F15/0046 , C07F15/0053 , C07C33/22 , C07C31/205 , C07C31/20 , C07C43/13 , C07C43/1782 , C07C271/16 , C07C215/16
摘要： The present invention relates to a ruthenium carbonyl complex that is represented by the following Formula (1): RuXY(CO)(L) (1) (in the Formula (1), X and Y, which may be the same or different from each other, represent an anionic ligand and L represents a tridentate aminodiphosphine ligand which has two phosphino groups and a —NH— group), its production method, and a method for production of alcohols by hydrogenation-reduction of ketones, esters, and lactones using the complex as a catalyst. The ruthenium carbonyl complex of the invention has a high catalytic activity and it can be easily prepared and handled.
摘要翻译：本发明涉及由下式（1）表示的羰基钌羰基络合物：RuXY（CO）（L）（1）（在式（1）中，X和Y可以相同或不同彼此表示阴离子配体，L表示具有两个膦基和-NH-基团的三齿氨基二膦配体），其制备方法和通过酮，酯和内酯的氢化还原来制备醇的方法，其使用该复合物作为催化剂。本发明的羰基钌络合物具有很高的催化活性，可以容易地制备和处理。

5. 发明授权

US08524953B2 Alcohol production method by reducing ester or lactone with hydrogen 有权
标题翻译：用氢还原酯或内酯的酒精生产方法
公开(公告)号：US08524953B2
公开(公告)日：2013-09-03
申请号：US13611381
申请日：2012-09-12
申请人： Wataru Kuriyama , Yasunori Ino , Osamu Ogata
发明人： Wataru Kuriyama , Yasunori Ino , Osamu Ogata
IPC分类号： C07C29/147 , C07F5/02 , B01J31/14
CPC分类号： C07C269/06 , B01J31/189 , B01J2231/643 , B01J2531/0255 , B01J2531/821 , C07B31/00 , C07B2200/07 , C07C29/149 , C07C213/08 , C07C2531/30 , C07D213/30 , C07D307/44 , C07C215/08 , C07C271/16 , C07C31/20 , C07C33/20 , C07C33/22 , C07C33/26
摘要： Provided is an alcohol production method comprising the step of reducing an ester or a lactone with hydrogen to produce a corresponding alcohol without addition of a base compound by using, as a catalyst, a ruthenium complex represented by the following general formula (1): RuH(X)(L1)(L2)n (1) wherein X represents a monovalent anionic ligand, L1 represents a tetradentate ligand having at least one coordinating phosphino group and at least one coordinating amino group or a bidentate aminophosphine ligand having one coordinating phosphino group and one coordinating amino group, and L2 represents a bidentate aminophosphine ligand having one coordinating phosphino group and one coordinating amino group, provided that n is 0 when L1 is the tetradentate ligand, and n is 1 when L1 is the bidentate aminophosphine ligand.
摘要翻译：提供了一种醇生产方法，其包括通过使用由以下通式（1）表示的钌络合物作为催化剂，用氢还原酯或内酯以产生相应的醇而不加入碱性化合物：RuH （X）（L）（L2）n（1）其中X表示一价阴离子配体，L1表示具有至少一个配位膦基的至少一个配位氨基或具有一个配位膦基的二齿氨基膦配体的四齿配位体和一个配位氨基，L2表示具有一个配位膦基和一个配位氨基的二齿氨基膦配体，条件是当L1为四齿配体时n为0，当L1为二齿氨基膦配体时，n为1。

6. 发明申请

US20100063294A1 ALCOHOL PRODUCTION METHOD BY REDUCING ESTER OF LACTONE WITH HYDROGEN 有权
标题翻译：酒精生产方法通过减少酯或酯与氢
公开(公告)号：US20100063294A1
公开(公告)日：2010-03-11
申请号：US12553544
申请日：2009-09-03
申请人： Wataru KURIYAMA , Yasunori Ino , Osamu Ogata
发明人： Wataru KURIYAMA , Yasunori Ino , Osamu Ogata
IPC分类号： C07D213/30 , C07C269/00 , C07C33/18 , C07C209/00 , C07C33/26 , C07D307/40 , C07C31/18
CPC分类号： C07C269/06 , B01J31/189 , B01J2231/643 , B01J2531/0255 , B01J2531/821 , C07B31/00 , C07B2200/07 , C07C29/149 , C07C213/08 , C07C2531/30 , C07D213/30 , C07D307/44 , C07C215/08 , C07C271/16 , C07C31/20 , C07C33/20 , C07C33/22 , C07C33/26
摘要： Provided is an alcohol production method comprising the step of reducing an ester or a lactone with hydrogen to produce a corresponding alcohol without addition of a base compound by using, as a catalyst, a ruthenium complex represented by the following general formula (1): RuH(X)(L1)(L2)n (1) wherein X represents a monovalent anionic ligand, L1 represents a tetradentate ligand having at least one coordinating phosphino group and at least one coordinating amino group or a bidentate aminophosphine ligand having one coordinating phosphino group and one coordinating amino group, and L2 represents a bidentate aminophosphine ligand having one coordinating phosphino group and one coordinating amino group, provided that n is 0 when L1 is the tetradentate ligand, and n is 1 when L1 is the bidentate aminophosphine ligand.
摘要翻译：提供了一种醇生产方法，其包括通过使用由以下通式（1）表示的钌络合物作为催化剂，用氢还原酯或内酯以产生相应的醇而不加入碱性化合物：RuH （X）（L）（L2）n（1）其中X表示一价阴离子配体，L1表示具有至少一个配位膦基的至少一个配位氨基或具有一个配位膦基的二齿氨基膦配体的四齿配位体和一个配位氨基，L2表示具有一个配位膦基和一个配位氨基的二齿氨基膦配体，条件是当L1为四齿配体时n为0，当L1为二齿氨基膦配体时，n为1。

7. 发明授权

US08288575B2 Alcohol production method by reducing ester of lactone with hydrogen 有权
标题翻译：用氢还原酯或内酯的酒精生产方法
公开(公告)号：US08288575B2
公开(公告)日：2012-10-16
申请号：US12553544
申请日：2009-09-03
申请人： Wataru Kuriyama , Yasunori Ino , Osamu Ogata
发明人： Wataru Kuriyama , Yasunori Ino , Osamu Ogata
IPC分类号： C07F5/02 , B01J31/14
CPC分类号： C07C269/06 , B01J31/189 , B01J2231/643 , B01J2531/0255 , B01J2531/821 , C07B31/00 , C07B2200/07 , C07C29/149 , C07C213/08 , C07C2531/30 , C07D213/30 , C07D307/44 , C07C215/08 , C07C271/16 , C07C31/20 , C07C33/20 , C07C33/22 , C07C33/26
摘要： Provided is an alcohol production method comprising the step of reducing an ester or a lactone with hydrogen to produce a corresponding alcohol without addition of a base compound by using, as a catalyst, a ruthenium complex represented by the following general formula (1): RuH(X)(L1)(L2)n (1) wherein X represents a monovalent anionic ligand, L1 represents a tetradentate ligand having at least one coordinating phosphino group and at least one coordinating amino group or a bidentate aminophosphine ligand having one coordinating phosphino group and one coordinating amino group, and L2 represents a bidentate aminophosphine ligand having one coordinating phosphino group and one coordinating amino group, provided that n is 0 when L1 is the tetradentate ligand, and n is 1 when L1 is the bidentate aminophosphine ligand.
摘要翻译：提供了一种醇生产方法，其包括通过使用由以下通式（1）表示的钌络合物作为催化剂，用氢还原酯或内酯以产生相应的醇而不加入碱性化合物：RuH （X）（L）（L2）n（1）其中X表示一价阴离子配体，L1表示具有至少一个配位膦基的至少一个配位氨基或具有一个配位膦基的二齿氨基膦配体的四齿配位体和一个配位氨基，L2表示具有一个配位膦基和一个配位氨基的二齿氨基膦配体，条件是当L1为四齿配体时n为0，当L1为二齿氨基膦配体时，n为1。

8. 发明授权

US09347617B2 Residual radioactive sludge liquid suction apparatus 有权
标题翻译：残留放射性污泥液体抽吸装置
公开(公告)号：US09347617B2
公开(公告)日：2016-05-24
申请号：US13807835
申请日：2011-06-29
申请人： Masahiro Aizawa , Osamu Ogata
发明人： Masahiro Aizawa , Osamu Ogata
IPC分类号： A47L5/00 , F17D1/14 , G21F9/04 , G21F9/22
CPC分类号： F17D1/14 , G21F9/04 , G21F9/22 , Y10T137/86083
摘要： There is provided a residual radioactive sludge liquid suction apparatus capable of safely and surely sucking radioactive sludge liquid remaining in a sludge storage tank with no fear of being exposed to radiation at a time when a small amount of sludge liquid remaining in the sludge storage tank is transferred to another tank. The suction apparatus is a residual radioactive sludge liquid suction apparatus used for sucking residual radioactive sludge liquid (L) at a time when the residual sludge liquid (L) remaining in a sludge storage tank T1 is transferred, and includes: a suction apparatus body 1; three hover skirts 2 mounted to the suction apparatus body 1; a suction head 8 mounted to the suction apparatus body 1 and configured to suck the residual sludge liquid (L); air jetting nozzles 13 mounted to the hover skirts 2, respectively; and an air supply source that supplies air to the hover skirts and the air jetting nozzles, wherein the suction apparatus body 1 floats on a surface of the residual sludge liquid (L) by supplying the air from the air supply source to the hover skirts, and moves on the surface of the residual sludge liquid (L) by jetting the air from the air supply source through the air jetting nozzles 13.
摘要翻译：提供了一种残留的放射性污泥液体抽吸装置，其能够安全地且可靠地吸入残留在污泥储罐中的放射性污泥液体，而不用担心在污泥储存罐中剩余的少量污泥液体不会暴露在辐射下转移到另一个坦克。吸入装置是在残留在污泥容纳槽T1中的残留污泥液体（L）被转移时用于吸附残留放射性污泥液体（L）的残留放射性污泥液体抽吸装置，具备：吸引装置主体1 ; 安装在吸引装置主体1上的三个悬停裙2; 吸入头8，安装在吸引装置本体1上，构成为吸收残留污泥液体（L）。分别安装在悬停裙2上的喷气喷嘴13; 以及将空气供给到悬浮裙部和空气喷射喷嘴的空气供给源，其中，通过将空气从空气供给源供给到悬停裙部，抽吸装置主体1浮动在残留污泥液体（L）的表面上，并且通过空气喷射喷嘴13从空气供给源喷射空气而在残留污泥液体（L）的表面上移动。

9. 发明申请

US20130291972A1 RADIOACTIVE SLUDGE TRANSFER APPARATUS 有权
公开(公告)号：US20130291972A1
公开(公告)日：2013-11-07
申请号：US13976522
申请日：2011-08-09
申请人： Masahiro Aizawa , Osamu Ogata
发明人： Masahiro Aizawa , Osamu Ogata
IPC分类号： F17D1/00
CPC分类号： G21F9/008 , B01F5/0206 , B01F5/0243 , F17D1/00 , F17D1/14 , G21F9/22 , G21F9/28 , G21F9/30 , Y10T137/86035 , Y10T137/86139
摘要： There is provided a radioactive sludge transfer apparatus for safely and surely transferring radioactive sludge contaminated by radioactive substance stored in a sludge storage tank to a transfer tank for the sake of tank inspection. A radioactive sludge transfer apparatus for transferring sludge stored in a sludge storage tank with supernatant solution to a transfer tank includes: a transfer apparatus body 1; a stirring apparatus 2 for blasting the supernatant solution to the sludge to thereby produce sludge solution in the one tank; sludge solution transfer means 8 for transferring the sludge solution to the transfer tank; an attitude control float 15; a floating force control ballast tank 16; and control means for remotely controlling the stirring apparatus 2, the sludge solution transfer means 8 and the floating force control ballast tank 16, wherein the stirring apparatus 2, the sludge solution transfer means 8, the attitude control float 15, and the floating force control ballast tank 16 are mounted respectively to the transfer apparatus body, the stirring apparatus 2 is provided with a supernatant solution suction pump 3 for sucking the supernatant solution and an injection nozzle 4 for jetting the supernatant solution to the sludge in the one tank to thereby form the sludge solution, the injection nozzle having freely controllable nozzle angle, the sludge solution transfer means 8 is provided with a sludge solution suction pump 9 for sucking the sludge solution and transfer the sucked sludge solution to the transfer tank, and the sludge solution suction pump 9 has suction ports 9A including bottom suction ports 10 and side suction ports 11 which are opened or closed by the open/close means 13, and when the sludge solution remaining inside the sludge storage tank is sucked out, the side suction ports 11 are closed by the open/close means 13.

10. 发明申请

US20130098483A1 RESIDUAL RADIOACTIVE SLUDGE LIQUID SUCTION APPARATUS 有权
标题翻译：残留放射性污泥液体吸收装置
公开(公告)号：US20130098483A1
公开(公告)日：2013-04-25
申请号：US13807835
申请日：2011-06-29
申请人： Masahiro Aizawa , Osamu Ogata
发明人： Masahiro Aizawa , Osamu Ogata
IPC分类号： F17D1/14
CPC分类号： F17D1/14 , G21F9/04 , G21F9/22 , Y10T137/86083
摘要： There is provided a residual radioactive sludge liquid suction apparatus capable of safely and surely sucking radioactive sludge liquid remaining in a sludge storage tank with no fear of being exposed to radiation at a time when a small amount of sludge liquid remaining in the sludge storage tank is transferred to another tank. The suction apparatus is a residual radioactive sludge liquid suction apparatus used for sucking residual radioactive sludge liquid (L) at a time when the residual sludge liquid (L) remaining in a sludge storage tank T1 is transferred, and includes: a suction apparatus body 1; three hover skirts 2 mounted to the suction apparatus body 1; a suction head 8 mounted to the suction apparatus body 1 and configured to suck the residual sludge liquid (L); air jetting nozzles 13 mounted to the hover skirts 2, respectively; and an air supply source that supplies air to the hover skirts and the air jetting nozzles, wherein the suction apparatus body 1 floats on a surface of the residual sludge liquid (L) by supplying the air from the air supply source to the hover skirts, and moves on the surface of the residual sludge liquid (L) by jetting the air from the air supply source through the air jetting nozzles 13.
摘要翻译：提供了一种残留的放射性污泥液体抽吸装置，其能够安全地且可靠地吸入残留在污泥储罐中的放射性污泥液体，而不用担心在污泥储存罐中剩余的少量污泥液体不会暴露在辐射下转移到另一个坦克。吸入装置是在残留在污泥容纳槽T1中的残留污泥液体（L）被转移时用于吸附残留放射性污泥液体（L）的残留放射性污泥液体抽吸装置，具备：吸引装置主体1 ; 安装在吸引装置主体1上的三个悬停裙2; 吸入头8，安装在吸引装置本体1上，构成为吸收残留污泥液体（L）。分别安装在悬停裙2上的喷气喷嘴13; 以及将空气供给到悬浮裙部和空气喷射喷嘴的空气供给源，其中，通过将空气从空气供给源供给到悬停裙部，抽吸装置主体1浮动在残留污泥液体（L）的表面上，并且通过空气喷射喷嘴13从空气供给源喷射空气而在残留污泥液体（L）的表面上移动。

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