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1. 发明申请

US20190126231A1 A METHANOL SYNTHESIS PROCESS LAYOUT FOR LARGE PRODUCTION CAPACITY 审中-公开
公开(公告)号：US20190126231A1
公开(公告)日：2019-05-02
申请号：US16083549
申请日：2017-03-23
申请人： Haldor Topsøe A/S
发明人： Hassan Modarresi
IPC分类号： B01J19/24 , B01J8/06
CPC分类号： B01J19/242 , B01J8/0257 , B01J8/0278 , B01J8/06 , B01J2208/00176 , B01J2208/00274 , B01J2208/0053 , B01J2219/00006 , B01J2219/00018 , B01J2219/00051 , C07C29/152 , C07C31/04
摘要： A process layout for large scale methanol synthesis comprises one or more boiling water reactors and one or more radial flow reactors in series, the boiling water reactor(s) being fed with approximately fresh make-up syngas. The methanol synthesis loop comprises a make-up gas compressor K1, a recycle gas compressor K2, two or more boiling water converters for methanol synthesis (A1, A2, . . . ), a radial flow converter (B) for methanol synthesis, a steam drum (V1), a high pressure separator (V2), a low pressure separator (V3), feed effluent heat exchangers (E1 and E2), a wash column (C), an air cooler (E3) and a water cooler (E4).

2. 发明申请

US20190092886A1 METHODS OF MONITORING AND CONTROLLING THE MELT INDEX OF A POLYOLEFIN PRODUCT DURING PRODUCTION 审中-公开
公开(公告)号：US20190092886A1
公开(公告)日：2019-03-28
申请号：US15527035
申请日：2015-11-24
申请人： Univation Technologies, LLC
发明人： Bruce J. Savatsky , Daniel N. Thomas, JR. , Timothy R. Lynn
IPC分类号： C08F210/16 , B01J8/18
CPC分类号： C08F210/16 , B01J8/1809 , B01J8/1827 , B01J8/1836 , B01J2208/00061 , B01J2208/00274 , B01J2208/00539 , B01J2208/00548 , B01J2208/00628 , B01J2208/00663 , B01J2208/00725 , B01J2208/00991 , C08F2400/02 , G05B17/00 , C08F4/65904 , C08F2/001 , C08F210/14 , C08F2500/12 , C08F2500/05 , C08F2/34 , C08F4/65925
摘要： Methods for producing polyolefin polymers may use a predictive melt index regression to estimate the melt index of the polyolefin during production based on the composition of the gas phase and, optionally, the concentration of catalyst in the reactor or reactor operating conditions. Such predictive melt index regression may include multiple terms to account for concentration of ICA in the reactor, optionally concentration of hydrogen in the reactor, optionally concentration of comonomer in the reactor, optionally the catalyst composition, and optionally reactor operating conditions. One or more terms may independently be represented by a smoothing function that incorporates a time constant.

3. 发明申请

US20180056263A1 CONTINUOUS GAS FLUIDIZED BED POLYMERIZATION PROCESS 审中-公开
公开(公告)号：US20180056263A1
公开(公告)日：2018-03-01
申请号：US15560238
申请日：2016-03-24
申请人： SABIC Global Technologies B.V.
发明人： Mohammed Althukair , Abdulrahman Ashri
IPC分类号： B01J8/00 , B01J8/18 , C08F10/02
CPC分类号： B01J8/0015 , B01J8/1827 , B01J8/1836 , B01J8/20 , B01J19/18 , B01J2208/00274 , B01J2208/003 , B01J2219/00006 , C08F2/01 , C08F2/34 , C08F10/02 , C08F10/00 , C08F210/16 , C08F210/08 , C08F2500/12
摘要： The invention relates to a process for the preparation of a polyolefin in a reaction system from one or more α-olefin monomers of which at least one is ethylene or propylene, 5 wherein the reaction system comprises a reactor, a product purge bin, a granular feed bin, wherein the granular feed bin is located downstream of the product purge bin, a recovery unit and an extrusion unit directly coupled to the granular fed bin, wherein the reactor comprises a fluidized bed, an expanded section located at or near the top of the reactor, a distribution plate located at the lower part of the reactor and an 10 inlet for a recycle stream located under the distribution plate, wherein the process comprises a) feeding a polymerization catalyst to the fluidized bed in the area above the distribution plate, b) feeding the one or more α-olefin monomers to the reactor, 15 c) circulating fluids from the top of the reactor to the bottom of the reactor, wherein the circulating fluids are cooled using a heat exchanger, resulting in a cooled recycle stream comprising liquid, and wherein the cooled recycle stream is introduced into the reactor using the inlet for the recycle stream, d) withdrawing a stream comprising the polyolefin and fluids from the reactor and 20 passing said stream into the product purge bin, e) purging the product purge bin with a purge stream comprising a first inert gas, preferably nitrogen and steam such that a stream comprising a purged polyolefin and a stream comprising fluids, wherein the stream comprising the fluids is substantially free of steam, is obtained, 25 f) introducing at least part of the stream comprising the fluids back into the reactor via the recovery unit, g) introducing the stream comprising the purged polyolefin into the granular feed bin and h) contacting a deactivating stream comprising steam with the purged polyolefin in the 30 granular feed bin to obtain a polyolefin that is substantially free of active polymerization catalyst.

4. 发明授权

US09895676B2 Processes and catalysts for converting alkanes to alkenes 有权
公开(公告)号：US09895676B2
公开(公告)日：2018-02-20
申请号：US14398891
申请日：2013-05-06
申请人： Sajet Development LLC
发明人： Jorge Miller , Luisa Kling Miller , Barry L. Stucky
IPC分类号： B01J21/16 , B01J8/08 , B01J8/12 , B01J8/18 , C07C1/26 , B01J37/04 , B01J23/02 , B01J29/08 , B01J35/00 , B01J35/02 , B01J35/10 , B01J37/00 , B01J37/14 , C07C1/30 , B01J37/06 , B01J37/08 , B01J38/30 , B01J23/06 , B01J23/92 , B01J29/90 , B01J35/08
CPC分类号： B01J21/16 , B01J8/085 , B01J8/125 , B01J8/1809 , B01J23/02 , B01J23/06 , B01J23/92 , B01J29/082 , B01J29/90 , B01J35/0006 , B01J35/002 , B01J35/0093 , B01J35/023 , B01J35/026 , B01J35/08 , B01J35/1061 , B01J35/1066 , B01J37/0009 , B01J37/0018 , B01J37/0063 , B01J37/0072 , B01J37/04 , B01J37/06 , B01J37/086 , B01J37/088 , B01J37/14 , B01J38/30 , B01J2208/00274 , C07C1/26 , C07C1/30 , C07C2521/10 , C07C2521/16 , C07C2527/232 , Y02P20/584 , C07C11/02 , C07C11/08
摘要： Generally, regenerable, encapsulated metal oxide catalysts comprising a ceramic matrix and metal catalysts may be used to convert alkanes to alkenes. The encapsulated metal oxide catalyst may be tailored to produce a variety of alkenes including ethylene, butylene, and propylene. Further, the encapsulated metal oxide catalysts advantageously allow for regeneration and reactant recovery for cost effective and environmentally friendly processes.

5. 发明授权

US09844763B2 Method of preheating dehydrogenation reactor feed 有权
公开(公告)号：US09844763B2
公开(公告)日：2017-12-19
申请号：US14674433
申请日：2015-03-31
申请人： Technip Process Technology, Inc.
发明人： Slawomir A. Oleksy
IPC分类号： C07C5/327 , C07C5/367 , B01J19/00 , F28D15/00 , B01J8/04
CPC分类号： B01J19/0013 , B01J8/0403 , B01J8/0446 , B01J8/0492 , B01J8/0496 , B01J2208/00176 , B01J2208/00256 , B01J2208/00274 , B01J2208/00309 , B01J2208/00371 , B01J2208/00504 , B01J2208/0053 , B01J2219/00103 , B01J2219/00121 , C07C5/327 , F28D15/00
摘要： Methods and systems for heating a reactor feed in a multi reactor hydrocarbon dehydrogenation process. The methods and systems are advantageously employed for the production of styrene by the catalytic dehydrogenation of ethylbenzene. The catalytic dehydrogenation process employs heating steam operating at a steam to oil ratio of about 1.0 or less and relatively low steam superheater furnace temperature, such that all components exposed to steam in the process (outside of the fired heaters) can be constructed with standard metallurgy.

6. 发明授权

US09840445B2 Method and apparatus for recycling methane 有权
公开(公告)号：US09840445B2
公开(公告)日：2017-12-12
申请号：US14210774
申请日：2014-03-14
申请人： John Winter , Takahiro Obase
发明人： John Winter , Takahiro Obase
IPC分类号： C07C1/00 , C07C7/12 , C10J3/48 , B01J8/18
CPC分类号： C07C1/00 , B01J8/1809 , B01J2208/00274 , C07C7/12 , C10J3/48 , C10J2200/152 , C07C9/04
摘要： The present invention relates to a method and gasification system for recycling methane-rich gas from syngas stream emanating from fluidized bed reactor and then returning the methane to the fluidized bed reactor. The method comprises recovering methane-rich gas from the synthesis gas and delivering at least a portion of the recovered methane-rich gas to the fluidized bed reactor. Methods to recover methane-rich gas from syngas at different steps in the gasification system are also provided herein.

7. 发明授权

US09617478B2 Process and apparatus for converting greenhouse gases into synthetic fuels 有权
公开(公告)号：US09617478B2
公开(公告)日：2017-04-11
申请号：US14995147
申请日：2016-01-13
申请人： ECOKAP Technologies LLC
发明人： Ben Zion Livneh
IPC分类号： C10G2/00 , B01J8/42 , B01J8/02 , B01J19/12
CPC分类号： C10G2/332 , B01J8/025 , B01J8/0278 , B01J8/0285 , B01J8/42 , B01J19/126 , B01J2208/00274 , B01J2208/00442 , B01J2219/0871 , B01J2219/0875 , B01J2219/0884 , B01J2219/0892 , B01J2219/1215 , B01J2219/1221 , B01J2219/1296 , C10G2/00 , Y02P20/133 , Y02P20/134 , Y02P20/582 , Y02P30/10
摘要： Embodiments of the present invention are directed to apparatus and methods for converting carbon dioxide and/or methane into higher alkanes and hydrogen gas in a single reaction chamber using a catalyst and microwave radiation.

8. 发明授权

US09587074B2 Multi-stage process for forming polyarylene sulfides 有权
标题翻译：形成聚亚芳基硫化物的多阶段工艺
公开(公告)号：US09587074B2
公开(公告)日：2017-03-07
申请号：US14481257
申请日：2014-09-09
申请人： Ticona LLC
发明人： Hendrich Chiong , Michael Haubs , Damian Feord , Stanley Leonard , Jacob Grayson , Venkata Nekkanti
IPC分类号： C08G75/14 , B01J19/00 , B01J19/18 , C08G75/00
CPC分类号： C08G75/14 , B01J19/0046 , B01J19/1862 , B01J2208/00176 , B01J2208/00274 , B01J2208/00283 , B01J2208/00539 , B01J2219/0013
摘要： A multi-stage process and system for formation of a polyarylene sulfide is described. The multi-stage process can include at least three separate formation stages that can take place in three different reactors. The first stage of the formation process can include reaction of an alkali metal sulfide with an organic amide solvent to form a complex including a hydrolysis product of the solvent and an alkali metal hydrogen sulfide. The second stage of the formation process can include reaction of the complex formed in the first stage with a dihaloaromatic monomer to form a prepolymer, and the third stage can include further polymerization of the prepolymer with additional monomers to form the final product.
摘要翻译：描述了用于形成聚芳硫醚的多阶段方法和系统。多级方法可以包括可以在三个不同的反应器中进行的至少三个分开的形成阶段。形成方法的第一阶段可以包括碱金属硫化物与有机酰胺溶剂的反应以形成包括溶剂和碱金属硫化氢的水解产物的络合物。形成方法的第二阶段可以包括在第一阶段中形成的络合物与二卤代芳族单体的反应以形成预聚物，第三阶段可包括预聚物与另外的单体的进一步聚合以形成最终产物。

9. 发明授权

US09464014B2 Process for the preparation of methanol in parallel reactors 有权
标题翻译：在并联反应器中制备甲醇的方法
公开(公告)号：US09464014B2
公开(公告)日：2016-10-11
申请号：US14892124
申请日：2014-05-15
申请人： Haldor Topsøe A/S
发明人： Hassan Modarresi , Christian Wix
IPC分类号： C07C27/00 , C07C29/152 , B01J8/04 , B01J8/02 , B01J19/18
CPC分类号： C07C29/152 , B01J8/0292 , B01J8/0453 , B01J19/1856 , B01J2208/00274 , B01J2208/027 , C07C31/04
摘要： In a process for the preparation of methanolin parallel reactors, comprising the steps of (a) reacting carbon oxides and hydrogen in the presence of a methanol catalyst in a first methanol reactor to obtain a first methanol-containing effluent, (b) introducing and reacting unconverted synthesis gas in a second methanol reactor in the presence of a methanol catalyst to obtain a second methanol-containing effluent, the first methanol reactor and the second methanol reactor being connected in parallel, (c) combining the first and second effluent, and (d) cooling and separating the combined and cooled effluent into a methanol-containing liquid phase and unconverted synthesis gas, the methanol catalyst in the first methanol reactor is indirectly cooled by boiling water and the methanol catalyst in the second methanol reactor is either directly or indirectly cooled by the unconverted synthesis gas prior to conversion into the second effluent.
摘要翻译：在制备甲醇并行反应器的方法中，包括以下步骤：（a）在甲醇催化剂存在下，在第一甲醇反应器中使碳氧化物和氢气反应，得到第一含甲醇的流出物，（b）引入和反应未转化的合成气在第二甲醇反应器中在甲醇催化剂存在下得到第二含甲醇的流出物，第一甲醇反应器和第二甲醇反应器并联连接，（c）将第一和第二流出物与（ d）冷却并将合并后的流出物分离成含甲醇的液相和未转化的合成气，第一甲醇反应器中的甲醇催化剂由沸水间接冷却，第二甲醇反应器中的甲醇催化剂直接或间接地在转化成第二流出物之前由未转化的合成气冷却。

10. 发明授权

US09399688B2 Multistage process for the polymerization of olefins 有权
标题翻译：用于烯烃聚合的多步法
公开(公告)号：US09399688B2
公开(公告)日：2016-07-26
申请号：US14889794
申请日：2014-05-13
申请人： Basell Polyolefine GmbH
发明人： Giuseppe Penzo , Gabriele Mei , Gerhardus Meier , Ulf Schueller , Antonio Ciarrocchi
IPC分类号： C08F2/00 , B01J19/18 , C08F110/02 , B01J19/24
CPC分类号： C08F110/02 , B01J8/0025 , B01J8/1863 , B01J8/1872 , B01J8/26 , B01J19/245 , B01J2208/00274 , B01J2208/00292 , B01J2208/00557 , B01J2208/00752 , B01J2208/00761 , B01J2208/00769 , B01J2208/00991 , B01J2219/24 , C08F10/00 , C08F2/001 , C08F2/34 , C08F2/01 , C08F2500/12 , C08F2500/07 , C08F2500/24 , C08F2500/18
摘要： A process for polymerizing olefins at temperatures of from 30° C. to 140° C. and pressures of from 1.0 MPa to 10 MPa in the presence of a polymerization catalyst in a multistage polymerization of olefins in at least two serially connected gas-phase polymerization reactors, and apparatus for the multistage polymerization of olefins, comprising at least two serially connected gas-phase polymerization reactors and a device for transferring polyolefin particles from an up-stream gas-phase polymerization reactor to a downstream gas-phase polymerization reactor, the transferring device comprising—a gas/solid separation chamber placed downstream of the upstream gas-phase polymerization which gas/solid separation chamber is equipped at a lower part with an net for introducing a fluid, and—connected to the gas/solid separation chamber at least two lock hoppers, placed in a parallel arrangement, each connected to the downstream gas-phase polymerization reactor.
摘要翻译：在烯烃的多段聚合中在聚合催化剂存在下，在至少两个串联连接的气相聚合中，在30℃至140℃的温度和1.0MPa至10MPa的温度下使烯烃聚合的方法反应器和用于烯烃多段聚合的装置，包括至少两个串联连接的气相聚合反应器和用于将聚烯烃颗粒从上游气相聚合反应器转移到下游气相聚合反应器的装置，转移装置包括：在上游气相聚合的下游设置的气/固分离室，气/固分离室在下部配备有用于引入流体的网，并至少与气/固分离室连接两个锁定料斗，并排布置，每个连接到下游气相聚合反应器。

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