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1. 发明授权

US09403923B2 Process for preparing synthetic polyethylene waxes having a high crystallinity and low viscosity 有权
标题翻译：制备具有高结晶度和低粘度的合成聚乙烯蜡的方法
公开(公告)号：US09403923B2
公开(公告)日：2016-08-02
申请号：US12516152
申请日：2007-09-13
申请人： Volker Schrenk , Udo Spitzer , Hans-Dieter Zagefka
发明人： Volker Schrenk , Udo Spitzer , Hans-Dieter Zagefka
IPC分类号： C08F4/52 , C08F110/02 , C10L1/16 , C07C2/02 , C07C2/04 , C07C2/24 , C09D5/03 , C09D7/12 , C09J123/08 , C08L23/04 , C08L23/06
CPC分类号： C08F110/02 , C08L23/04 , C08L23/06 , C08L2314/02 , C08L2314/04 , C08L2666/02 , C09D5/037 , C09D7/65 , C09J123/0853 , C08F2/02 , C08F4/655 , C08F2500/23 , C08F2500/02 , C08F2500/18 , C08F2500/17 , C08F2500/20
摘要： A process for preparing a polyethylene wax by polymerization of ethylene in the presence of a Ziegler-Natta catalyst system composed of titanium tetrachloride and dialkylaluminium halide, wherein the polymerization temperature is in the range from 170 to 200° C., the polymerization is carried out essentially in the absence of solvents and the Al/Ti molar ratio is less than 1.6, gives a wax having the following property profile: dropping point of from 115 to 125° C.; penetration number of not more than 1 mm·10−1; viscosity at 150° C. of less than 60 mPas; density of from 0.945 to 0.960 g/cm3 at 23° C.; molar mass of less than 1500 g/mol and crystallinity of more than 70%.
摘要翻译：在由四氯化钛和二烷基卤化铝组成的齐格勒 - 纳塔催化剂体系存在下聚合乙烯制备聚乙烯蜡的方法，其中聚合温度为170-200℃，聚合反应进行基本上在不存在溶剂的情况下，Al / Ti摩尔比小于1.6，得到具有以下特性分布的蜡：滴点为115-125℃。穿透数不超过1毫米·10-1; 在150℃下的粘度小于60mPas; 在23℃下的密度为0.945〜0.960g / cm 3。摩尔质量小于1500g / mol，结晶度大于70％。

2. 发明授权

US09376557B2 Process for preparing polyethylene blend comprising metallocene produced resins and chromium produced resins 有权
标题翻译：包括茂金属生产的树脂和生产铬的树脂的聚乙烯混合物的制备方法
公开(公告)号：US09376557B2
公开(公告)日：2016-06-28
申请号：US14003164
申请日：2012-03-02
申请人： Daan Dewachter , Eric Damme
发明人： Daan Dewachter , Eric Damme
IPC分类号： C08L23/06 , C08L23/08 , C08L23/04 , C08F110/02
CPC分类号： C08L23/06 , C08F110/02 , C08L23/04 , C08L23/0815 , C08L2205/025 , C08L2314/04 , C08L2314/06 , C08F2500/12
摘要： A process for preparing a homogeneous polyethylene product can include producing a first polyethylene resin in the presence of a metallocene catalyst in a reactor. The first polyethylene resin can have a density of from 0.942 to 0.970 g/cm3 and an HLMI of from 0.5 to 150 g/10 min. The process can include separately producing a second polyethylene resin in the presence of a chromium catalyst in a reactor. The process can include physically blending together the first polyethylene resin and the second polyethylene resin to produce the homogeneous polyethylene product. The homogeneous polyethylene product can include at least 25% by weight of the first polyethylene resin.
摘要翻译：制备均匀的聚乙烯产品的方法可以包括在茂金属催化剂存在下在反应器中制备第一聚乙烯树脂。第一聚乙烯树脂的密度可以为0.942-0.970g / cm3，HLMI为0.5-150g / 10min。该方法可以包括在反应器中在铬催化剂存在下单独制备第二聚乙烯树脂。该方法可以包括将第一聚乙烯树脂和第二聚乙烯树脂物理混合在一起以产生均匀的聚乙烯产品。均匀的聚乙烯产品可以包含至少25重量％的第一聚乙烯树脂。

3. 发明申请

US20040192864A1 Utility conduit resin 审中-公开
标题翻译：实用导管树脂
公开(公告)号：US20040192864A1
公开(公告)日：2004-09-30
申请号：US10784460
申请日：2004-02-23
发明人： Thomas W. Towles
IPC分类号： C08F004/06
CPC分类号： C08F210/16 , C08F110/02 , C08L23/06 , C08L2314/02 , C08L2314/04 , C08F2/34 , C08F4/24 , C08F2500/07 , C08F2500/12 , C08F2500/13 , C08F210/14
摘要： This invention is related to conduit resins comprising ethylene made using an activated chromium and titanium-based catalyst.
摘要翻译：本发明涉及包含使用活化的铬和钛基催化剂制备的乙烯的导管树脂。

4. 发明授权

US06479589B2 Production of multimodal polyethylene 失效
标题翻译：生产多峰聚乙烯
公开(公告)号：US06479589B2
公开(公告)日：2002-11-12
申请号：US10037504
申请日：2002-01-04
申请人： Guy Debras , Abbas Razavi , Jacques Michel
发明人： Guy Debras , Abbas Razavi , Jacques Michel
IPC分类号： C08L2300
CPC分类号： C08F210/16 , C08F4/65916 , C08F110/02 , C08L23/06 , C08L23/0815 , C08L2205/02 , C08L2205/025 , C08L2308/00 , C08L2314/02 , C08L2314/04 , C08L2314/06 , C08F4/65925 , C08F4/65927 , C08F2/001 , C08L2666/04 , C08F210/14 , C08F2500/01 , C08F2500/02 , C08F2500/13 , C08F2500/07 , C08F2500/12 , C08F2500/05 , C08F2500/08 , C08F4/24
摘要： A process for preparing polyethylene, including contacting ethylene monomer and an alpha-olefin comonomer to produce a first polyethylene (HLMI of ≦0.5 g/10 min, density ≦0.925 g/ml). The a catalyst system is a bis tetrahydroindenyl formula (IndH4)2R″MQ2 wherein each Ind is the same or different and is indenyl or substituted indenyl, R″ is a bridge which comprises a C1-C20 alkylene radical, a dialkyl germanium or silicon or siloxane, or an alkyl phosphine or amine radical, which bridge is substituted or unsubstituted, M is a Group IVB transition metal or vanadium and each Q is hydrocarbyl having 1 to 20 carbon atoms or halogen. The polyethylene resin having multimodal molecular weight distribution is formed by mixing the first polyethylene with a second polyethylene (produced with a different catalyst and with a lower molecular weight and higher density than the first polyethylene).
摘要翻译：一种制备聚乙烯的方法，包括使乙烯单体和α-烯烃共聚单体接触以制备第一种聚乙烯（HLMI <= 0.5g / 10min，密度<= 0.925g / ml）。该催化剂体系是双四氢茚基配基（IndH4）2R''MQ2，其中每个Ind相同或不同，并且是茚基或取代的茚基，R“是包含C 1 -C 20亚烷基，二烷基锗或硅或硅氧烷，或烷基膦或胺基，该桥是取代或未取代的，M为ⅣB族过渡金属或钒，Q为具有1至20个碳原子的烃基或卤素。具有多峰分子量分布的聚乙烯树脂通过将第一聚乙烯与第二聚乙烯（用不同的催化剂制得，分子量低于第一聚乙烯的密度较低）混合形成。

5. 发明授权

US5834557A Graft modified ethylene/.alpha.-olefin copolymer composition 失效
标题翻译：接枝改性乙烯/α-烯烃共聚物组合物
公开(公告)号：US5834557A
公开(公告)日：1998-11-10
申请号：US872937
申请日：1997-06-11
申请人： Toshiyuki Tsutsui , Ken Yoshitsugu , Mamoru Takahashi , Akira Todo , Seiji Ohta , Hajime Inagaki
发明人： Toshiyuki Tsutsui , Ken Yoshitsugu , Mamoru Takahashi , Akira Todo , Seiji Ohta , Hajime Inagaki
IPC分类号： C08F4/659 , C08F4/6592 , C08F10/00 , C08F210/16 , C08F255/02 , C08F255/04 , C08F255/08 , C08F287/00 , C08F297/08 , C08L23/04 , C08L23/08 , C08L51/06
CPC分类号： C08F10/00 , C08F210/16 , C08F255/02 , C08F255/04 , C08F255/08 , C08F287/00 , C08F297/08 , C08L23/04 , C08L23/0815 , C08L51/06 , C08F4/65904 , C08F4/65912 , C08F4/65916 , C08F4/65922 , C08L2205/02 , C08L2314/04 , C08L2314/06
摘要： An ethylene/.alpha.-olefin copolymer composition including (I) a graft-modified ethylene/.alpha.-olefin copolymer composition and (II) a polyolefin. The graft-modified composition is prepared by graft copolymerizing an ethylene/.alpha.-olefin copolymer with a polar monomer. The ethylene/.alpha.-olefin copolymer composition includes first and second ethylene/.alpha.-olefin copolymers. The copolymers are each prepared in the presence of a polymerization catalyst containing (a) an organoaluminum oxy compound and (b) for the first ethylene/.alpha.-olefin copolymer at least two kinds, and for the second ethylene/.alpha.-olefin copolymer one kind, of compounds of Group IV transition metals of the periodic table containing a ligand having a cyclopentadienyl skeleton. The graft-modified ethylene/.alpha.-olefin copolymer composition is blended with a polyolefin, such as by mechanical or solution blending, at a weight ratio (I) to (II) of 1:99 to 99:1. The copolymer compositions have excellent moldability and heat stability properties and form films having high transparency and mechanical strength and good adhesion to polar materials.
摘要翻译：包含（I）接枝改性的乙烯/α-烯烃共聚物组合物和（II）聚烯烃的乙烯/α-烯烃共聚物组合物。通过将乙烯/α-烯烃共聚物与极性单体接枝共聚来制备接枝改性组合物。乙烯/α-烯烃共聚物组合物包括第一和第二乙烯/α-烯烃共聚物。共聚物各自在含有（a）有机铝氧化合物和（b）第一乙烯/α-烯烃共聚物至少两种的聚合催化剂存在下制备，并且对于第二种乙烯/α-烯烃共聚物为一种的含有具有环戊二烯基骨架的配体的周期表的IV族过渡金属的化合物。将接枝改性的乙烯/α-烯烃共聚物组合物与聚烯烃例如通过机械或溶液共混以1:99至99:1的重量比（I）至（II）共混。共聚物组合物具有优异的成型性和热稳定性，并且形成具有高透明度和机械强度以及对极性材料的良好粘附性的膜。

6. 发明申请

US20090311453A1 Molding compostion comprsing polyethlene for preparing films and process for preparing the molding composition in the presence of a mixed catalyst 审中-公开
标题翻译：用于制备膜的聚乙烯的成型组合物和在混合催化剂存在下制备模塑组合物的方法
公开(公告)号：US20090311453A1
公开(公告)日：2009-12-17
申请号：US11919166
申请日：2006-04-15
申请人： Shahram Mihan , Dieter Lilge , Heinz Vogt , Jennifer Kipke , Rainer Karer
发明人： Shahram Mihan , Dieter Lilge , Heinz Vogt , Jennifer Kipke , Rainer Karer
IPC分类号： B32B1/02 , C08F110/02 , C08L23/06 , C08F2/00 , C07F17/00 , B01J31/12 , B29C47/00
CPC分类号： C08J5/18 , C08F4/65912 , C08F4/65925 , C08F10/00 , C08F10/02 , C08F110/02 , C08F210/16 , C08J2323/08 , C08L23/06 , C08L23/0815 , C08L2205/02 , C08L2314/04 , C08L2314/06 , Y02P20/52 , Y10T428/1352 , C08F4/69 , C08F4/025 , C08F4/65916 , C08L2666/06 , C08F2500/17 , C08F2500/12 , C08F2500/04 , C08F2500/26 , C08F2500/09 , C08F2500/18 , C08F210/14 , C08F4/6292 , C08F4/63904
摘要： Molding composition comprising polyethylene and having a density in the range from 0.915 to 0.955 g/cm, an MI in the range from 0 to 3.5 g/10 min, an MFR in the range from 5 to 50, a polydispersity Mw/Mn in the range from 5 to 20, and a z-average moiar mass Mz of less than 1 million g/mol, a process for preparing such a composition, a catalyst suitable for the preparation of the same, as well as films comprising this molding composition.
摘要翻译：包含聚乙烯并且密度在0.915至0.955g / cm 3，MI在0至3.5g / 10min范围内的MFR，5至50范围内的MFR，5分钟内的多分散性Mw / Mn 范围为5至20，z平均摩尔质量Mz小于100万g / mol，制备这种组合物的方法，适用于其制备的催化剂以及包含该模塑组合物的薄膜。

7. 发明申请

US20040242815A1 Multistep process for the (co) polymerization of olefins 失效
标题翻译：烯烃的（共）聚合的多步法
公开(公告)号：US20040242815A1
公开(公告)日：2004-12-02
申请号：US10482877
申请日：2004-01-06
发明人： Luigi Resconi , Giovanni Baruzzi
IPC分类号： C07F007/28 , C08F004/72
CPC分类号： C08F110/06 , C08F4/65912 , C08F4/6592 , C08F10/00 , C08F210/16 , C08F2410/05 , C08L23/12 , C08L23/142 , C08L2205/02 , C08L2207/14 , C08L2308/00 , C08L2314/02 , C08L2314/04 , C08L2314/06 , C08F2/001 , C08F2/00 , C08L2666/04 , C08F2500/04 , C08F2500/15 , C08F2500/17 , C08F2500/20 , C08F210/08
摘要： A multistep process for the polymerization of one or more olefins comprising a first step of polymerizing one or more of said olefins in the presence of a catalyst of the Ziegler-Natta type, a step wherein the polymer obtained in the first step is contacted with a catalyst system comprising an half-sandwich metallocene compound, followed by a second polymerization step. The amount of homo- or copolymer of olefins produced in the first polymerization step is between 10% to 90% by weight of the total amount of polymer produced.
摘要翻译：一种用于一种或多种烯烃的聚合的多步骤方法，包括在齐格勒 - 纳塔型催化剂存在下使一种或多种所述烯烃聚合的第一步骤，其中将第一步骤中获得的聚合物与催化剂体系，其包含半夹心金属茂化合物，随后进行第二聚合步骤。在第一聚合步骤中产生的烯烃的均聚物或共聚物的量为所生产的聚合物总量的10重量％至90重量％。

8. 发明授权

US06566450B2 Production of multimodal polyethylene 失效
标题翻译：生产多峰聚乙烯
公开(公告)号：US06566450B2
公开(公告)日：2003-05-20
申请号：US10037934
申请日：2002-01-04
申请人： Guy Debras , Abbas Razavi , Jacques Michel
发明人： Guy Debras , Abbas Razavi , Jacques Michel
IPC分类号： C08L2300
CPC分类号： C08F210/16 , C08F4/65916 , C08F110/02 , C08L23/06 , C08L23/0815 , C08L2205/02 , C08L2205/025 , C08L2308/00 , C08L2314/02 , C08L2314/04 , C08L2314/06 , C08F4/65925 , C08F4/65927 , C08F2/001 , C08L2666/04 , C08F210/14 , C08F2500/01 , C08F2500/02 , C08F2500/13 , C08F2500/07 , C08F2500/12 , C08F2500/05 , C08F2500/08 , C08F4/24
摘要： A process for the preparation of polyethylene resins having a multimodal molecular weight distribution which comprises: (i) contacting ethylene monomer and a comonomer comprising an alpha-olefin having from 3 to 10 carbon atoms with a first catalyst system in a first reactor under first polymerization conditions to produce a first polyethylene having a first molecular weight, an HLMI of not more than 0.5 g/10 min and a first density of not more than 0.925 g/ml and the first catalyst system comprising (a) a metallocene catalyst comprising a bis tetrahydroindenyl compound of the general formula (IndH4)2R″MQ2 in which each Ind is the same or different and is indenyl or substituted indenyl, R″ is a bridge which comprises a C1-C20 alkylene radical, a dialkyl germanium or silicon or siloxane, or an alkyl phosphine or amine radical, which bridge is substituted or unsubstituted, M is a Group IVB transition metal or vanadium and each Q is hydrocarbyl having 1 to 20 carbon atoms or halogen; and (b) a cocatalyst which activates the catalyst component; (ii) providing a second polyethylene having a second lower molecular weight and second higher density than the first polyethylene, the second polyethylene having been produced using a catalyst other than the bis tetrahydroindenyl compound; and (iii) mixing together the first and second polyethylenes to form a polyethylene resin having a multimodal molecular weight distribution.
摘要翻译：一种用于制备具有多峰分子量分布的聚乙烯树脂的方法，其包括：（i）在第一聚合反应器中，将第一催化剂体系中的乙烯单体和包含具有3-10个碳原子的α-烯烃的共聚单体与第一催化剂体系接触制备具有第一分子量，HLMI不大于0.5g / 10min和第一密度不大于0.925g / ml的第一聚乙烯的第一催化剂体系，所述第一催化剂体系包含（a）茂金属催化剂，其包含双四氢茚基化合物，其中每个Ind相同或不同，并且是茚基或取代的茚基，R“是包含C 1 -C 20亚烷基，二烷基锗或硅的桥，或硅烷或烷基膦或胺基，该桥是取代或未取代的，M为ⅣB族过渡金属或钒，Q为具有1至20个碳原子的烃基或卤素; 和（b）活化催化剂组分的助催化剂;（ii）提供具有比第一聚乙烯低的第二较低分子量和第二高密度的第二聚乙烯，所述第二聚乙烯使用不同于所述双四氢茚基化合物的催化剂制备; 和（iii）将第一和第二聚乙烯混合在一起以形成具有多峰分子量分布的聚乙烯树脂。

9. 发明授权

US06455602B1 High-speed processable cellular insulation material with enhanced foamability 有权
标题翻译：高速可加工的泡沫隔热材料，具有增强的起泡性
公开(公告)号：US06455602B1
公开(公告)日：2002-09-24
申请号：US09694853
申请日：2000-10-24
申请人： Sandra Maki , Geoffrey David Brown , Scott Hanley Wasserman , David John Frankowski , Vicky Yafen He
发明人： Sandra Maki , Geoffrey David Brown , Scott Hanley Wasserman , David John Frankowski , Vicky Yafen He
IPC分类号： C08L4700
CPC分类号： C08J9/04 , C08J2201/03 , C08J2323/04 , C08L23/04 , C08L23/0815 , C08L23/10 , C08L51/06 , C08L2203/14 , C08L2203/202 , C08L2205/02 , C08L2314/02 , C08L2314/04 , C08L2314/06 , H01B3/441 , C08L2666/04 , C08L2666/02
摘要： An expandable composition comprising: (A) about 60 to about 98 percent by weight of a polyolefin or mixture of polyolefins wherein the polyolefin or mixture has an &eegr;0 of less than about 9.0 kilopascal.seconds (kPa.s), a Jr greater than about 50×10−5/pascals (Pa), and an Ea greater than about 6.7 kilocalories per mole (kcal/mol); and (B) about 2 to about 40 percent by weight of a polyolefin or mixture of polyolefins having an nRSI greater than about 4.5, and no greater than about 19; or (C) a polyolefin or mixture of polyolefins wherein the polymer or mixture has an &eegr;0 of less than about 9.0 kilopascal.seconds, a Jr greater than about 50×10−5/pascals, an Ea greater than about 6.7 kilocalories/mole, and an nRSI greater than about 9.
摘要翻译：一种可发泡组合物，其包含：（A）约60至约98重量％的聚烯烃或聚烯烃混合物，其中所述聚烯烃或混合物具有小于约9.0千帕斯卡/秒（kPa.s）的η，大于约 50×10 -5 /帕斯卡（Pa），Ea大于约6.7千卡每摩尔（kcal / mol）; 和（B）约2至约40重量％的具有nRSI大于约4.5且不大于约19的聚烯烃或聚烯烃的混合物; 或（C）聚烯烃或聚烯烃混合物，其中所述聚合物或混合物具有小于约9.0千帕斯卡的秒，大于约50×10-5 /帕斯卡的Δr，大于约6.7千卡/摩尔的Ea，以及 nRSI大于9。

10. 发明授权

US06448341B1 Ethylene interpolymer blend compositions 失效
标题翻译：乙烯互聚物共混组合物
公开(公告)号：US06448341B1
公开(公告)日：2002-09-10
申请号：US09645731
申请日：2000-08-24
申请人： Brian W. S. Kolthammer , Robert S. Cardwell , Ronald P. Markovich , Bharat I. Chaudhary , Adam E. Laubach , Jesus Nieto
发明人： Brian W. S. Kolthammer , Robert S. Cardwell , Ronald P. Markovich , Bharat I. Chaudhary , Adam E. Laubach , Jesus Nieto
IPC分类号： C08L2308
CPC分类号： C08F297/08 , C08F4/65908 , C08F4/65912 , C08F210/16 , C08L23/0815 , C08L2205/02 , C08L2314/02 , C08L2314/04 , C08L2314/06 , C08F4/6555 , C08F2/001 , C08L2666/04 , C08F210/14 , C08F2500/12 , C08F2500/06 , C08F2500/03 , C08F2500/08
摘要： Film, molded articles and fibers prepared from ethylene/&agr;-olefin interpolymer compositions are disclosed. The interpolymer compositions are blends prepared by combining specified amounts of a narrow molecular weight distribution, narrow composition distribution breadth index interpolymer, and a broad molecular weight distribution, broad composition distribution breadth index interpolymer, with each blend component having a specified density, melt index and degree of branching.
摘要翻译：公开了由乙烯/α-烯烃互聚物组合物制备的膜，模塑制品和纤维。互聚物组合物是通过组合规定量的窄分子量分布，窄组成分布宽度指数互聚物和宽分子量分布，广泛的组成分布宽度指数互聚物，每种共混组分具有指定的密度，熔体指数和分枝度。

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