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    • 4. 发明授权
    • Sample cooling apparatus for X-ray diffractometer and X-ray diffractometer
    • 用于X射线衍射仪和X射线衍射仪的样品冷却装置
    • US09008270B2
    • 2015-04-14
    • US13454393
    • 2012-04-24
    • Tomokazu HasegawaKazuaki Aburaya
    • Tomokazu HasegawaKazuaki Aburaya
    • G01N23/207H05G1/02G01N1/42
    • G01N23/207G01N1/42G01N2223/307
    • The sample cooling apparatus is used in an X-ray diffractometer for rotating a sample supported by a sample rod about an ω axis, directing X-rays thereto, and detecting X-rays deflected from the sample using an X-ray detector. The apparatus has a nozzle for blowing a cooling gas on the sample; and a gas-suctioning device for suctioning, via an aperture, gas that has passed over the sample. The sample rod moves when rotated about the ω axis forming a conical surface having the sample as a vertex. The nozzle is provided so that the extension direction of the sample rod and the direction of the blown gas form an acute angle of 90° or less. The gas-suctioning device suctions the gas so the path of gas having contacted the sample rod bends when the extension direction of the sample rod and the blown direction of the gas form an acute angle.
    • 样品冷却装置用于X射线衍射仪,用于将由样品杆支撑的样品围绕ω轴旋转,将X射线引导到其上,并使用X射线检测器检测从样品偏转的X射线。 该装置具有用于在样品上吹送冷却气体的喷嘴; 以及用于经由孔径抽吸已经通过样品的气体的吸气装置。 当围绕ω轴旋转时,样品棒移动,形成具有样品作为顶点的锥形表面。 喷嘴被设置成使得样品棒的延伸方向和吹入气体的方向形成90°或更小的锐角。 气体吸引装置吸入气体,当样品棒的延伸方向和气体的吹出方向形成锐角时,接触样品棒的气体的路径弯曲。