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1. 发明授权

US3732275A Separating phthalonitriles from reaction gases containing the same 失效
标题翻译：从含有它的反应气体中分离出苯并噻吩
公开(公告)号：US3732275A
公开(公告)日：1973-05-08
申请号：US3732275D
申请日：1970-12-30
申请人： BASF AG
发明人： PLATZ R , DECKER M , BUERGER G , STECHL H
IPC分类号： C07C255/51 , C07C121/56
CPC分类号： C07C255/00
摘要： AN IMPROVED PROCESS FOR THE RECOVERY OF PHTHALONITRILES FROM HOT REACTION GASES CONTAINING THE SAME BY CONTACTING THE HOT REACTION GASES WITH A COOLANT WHICH IS AT A TEMPERATURE OF FROM 40* TO 200*C. AND COOLING THEM DOWN AT A RATE OF MORE THAN 350*C. PER SECONDS, THE COOLANT BEING WATER, BENZONITRILE OR O-TOLUNITRILE WHICH FROM RRECYCLING CONTAINS 2 TO 40% PHTHALONITRILES. O-PHTHALONITRILE IS SUITABLE FOR THE PRODUCTION OF PHTHALOCYANINES WHICH ARE VALUABLE PIGMENTS, TEREPHTHALONITRILE AND ISOPHTHALONITRILES CAN BE REDUCED TO THE CORRESPONDING DIAMINES WHICH ARE STARTING MATERIALS FOR THE MANUFACTURE OF POLYAMIDES WHICH CAN BE USED FOR THE PRODUCTION OF FIBERS.

2. 发明授权

US4572806A Process for the continuous production of tetrachlorophthalo-nitrile in two reactors in series 失效
标题翻译：串联在两个反应器中连续生产四氯苯腈的方法
公开(公告)号：US4572806A
公开(公告)日：1986-02-25
申请号：US629948
申请日：1984-07-10
申请人： Giuseppe Ghielmetti , Liborio Casale , Giordano Donelli
发明人： Giuseppe Ghielmetti , Liborio Casale , Giordano Donelli
IPC分类号： C07C255/51 , C07B61/00 , C07C20060101 , C07C67/00 , C07C253/00 , C07C121/56
CPC分类号： C07C255/00
摘要： In an improved process for the continuous production of tetrachlorophthalonitrile, of the type with activated carbon fluidized bed reactor, under whose grid melted and atomized phthalonitrile, chlorine, hydrochloric acid and possibly nitrogen are simultaneously introduced the use of a second static bed reactor, also of activated carbon, in series with the first, is provided for, thereby greatly improving the life of the catalyzer, and, above all, the quality of the product.
摘要翻译：在连续生产四氯邻苯二甲腈的改进方法中，使用活性炭流化床反应器的类型，在其网格熔化和雾化邻苯二腈，氯，盐酸和可能的氮的同时引入了使用第二静态床反应器，也是提供了与第一种串联的活性炭，从而大大提高了催化剂的寿命，最重要的是提高了产品的质量。

3. 发明授权

US3776937A Process for the manufacture of aromatic nitriles 失效
标题翻译：制备硝基苯胺的方法
公开(公告)号：US3776937A
公开(公告)日：1973-12-04
申请号：US3776937D
申请日：1972-06-23
申请人： LUMMUS CO
发明人： GELBEIN A
IPC分类号： C07C255/51 , C07C121/12 , C07C121/56
CPC分类号： C07C253/20 , C07C255/51
摘要： IN THE PRODUCTION OF AROMATIC POLYNITRILES AHVING AT LEAST ONE PAIR OF NITRILE GROUPS IN THE ORTHO POSITION RELATIVE TO EACH OTHER BY THE REACTION OF AN ALKYL AROMATIC HYDROCARBON WITH AMMONIA, THE PROBLEM OF IMIDE FORMATION CAN BE AT LEAST PARTIALLY RESOLVED BY PASSING THE PRODUCT STREAM OF THE RECTION OVER A DEHYDRATION CATALYST TO CONVENT IMIDES PRESENT TO ADDITIONAL NITRILE TO PRODUCT. IF NECCESSARY, ADDITIONAL AMMONIA CAN BE ADDED.

4. 发明授权

US4637897A Nematic compounds 失效
标题翻译：向列化合物
公开(公告)号：US4637897A
公开(公告)日：1987-01-20
申请号：US638089
申请日：1984-08-06
申请人： Stephen M. Kelly
发明人： Stephen M. Kelly
IPC分类号： C07C17/00 , C07C25/18 , C07C39/42 , C07C41/00 , C07C43/225 , C07C45/46 , C07C49/84 , C07C53/44 , C07C67/00 , C07C69/75 , C07C69/757 , C07C69/76 , C07C69/78 , C07C253/00 , C07C255/50 , C07C255/54 , C07C255/55 , C07C255/57 , C09K19/30 , G02F1/13 , C07C25/13 , C07C121/52 , C07C121/56
CPC分类号： C07C255/00 , C07C25/18 , C07C43/225 , C07C45/46 , C07C49/84 , C07C53/44 , C09K19/3028 , C09K19/3066 , C09K19/3068
摘要： Nematic compounds with a negative DC antisotropy, characterized by the formula I ##STR1## in which m=1 or 2, r is zero or 1 and m+r=1 or 2, and R.sup.1 and R.sup.2 are identical or different and are selected from alkyl and alkoxy groups each having 1-12 carbon atoms in a straight or branched chain, which may be chiral, Z is a bridge member selected from a single bond and the groups of the formulae --CH.sub.2 CH.sub.2 --, --OCH.sub.2 --, --O--CO-- or --CO--O--, one of the groups X and Y is selected from fluorine, chlorine, bromine and cyano and the other of the groups X and Y is selected from hydrogen, fluorine, chlorine, bromine and cyano, with the proviso that m=r=1 if X and Y are both cyano, are suitable as components for liquid crystal mixtures having an overall negative DC anisotropy, such as are required in particular for electro-optical displays of the type of guest/host displays or homotropic-nematic displays.
摘要翻译：具有负直流消偏性的向列化合物，其特征在于其中m = 1或2，r为0或1，m + r = 1或2，并且R 1和R 2相同或不同并且被选择的式I 在直链或支链上各自具有1-12个碳原子的烷基和烷氧基，其可以是手性的，Z是选自单键的桥连体，式-CH 2 CH 2 - ， - OCH 2 - ，-O -CO-或-CO-O-，基团X和Y之一选自氟，氯，溴和氰基，X和Y中的另一个选自氢，氟，氯，溴和氰基，与条件是如果X和Y都是氰基，则m = r = 1，适合作为具有总的负DC各向异性的液晶混合物的组分，例如特别对客体/主机显示器类型的电光显示器或同向向列型显示器。

5. 发明授权

US4485050A Process for the continuous production of tetrachlorophthalonitrile in a fluidized bed reactor 失效
标题翻译：在流化床反应器中连续生产四氯邻苯二甲腈的方法
公开(公告)号：US4485050A
公开(公告)日：1984-11-27
申请号：US494285
申请日：1983-05-13
申请人： Liborio Casale , Giordano Donelli
发明人： Liborio Casale , Giordano Donelli
IPC分类号： C07C255/51 , C07C20060101 , C07C67/00 , C07C253/00 , C07C121/56
CPC分类号： C07C255/00
摘要： In an improved process of the continuous production of tetrachlorophthalonitrile, molten atomized phthalonitrile, chlorine, hydrochloric acid and possibly nitrogen are fed simultaneously below the grid of a reactor with a fluidized bed of activated carbon, and the tetrachlorophthalonitrile is separated and recovered continuously by simple cooling.
摘要翻译：在连续生产四氯邻苯二甲腈的改进方法中，熔融雾化的邻苯二甲腈，氯，盐酸和可能的氮气同时在具有活性炭流化床的反应器的格栅下同时进料，并且四氯邻苯二甲腈通过简单冷却连续分离和回收。

6. 发明授权

US4298545A Process for producing phthalonitrile 失效
标题翻译：邻苯二甲腈生产方法
公开(公告)号：US4298545A
公开(公告)日：1981-11-03
申请号：US136989
申请日：1980-04-03
申请人： Masao Saito , Motoyuki Hosokawa , Takamasa Kawakami , Yuko Murayama
发明人： Masao Saito , Motoyuki Hosokawa , Takamasa Kawakami , Yuko Murayama
IPC分类号： C07B61/00 , B01J21/00 , B01J21/02 , B01J21/06 , B01J23/00 , B01J23/16 , B01J23/70 , B01J27/00 , B01J27/02 , B01J27/16 , C07C67/00 , C07C253/00 , C07C255/51 , C07C121/56
CPC分类号： C07C255/00
摘要： Phthalonitrile is produced in a good yield by contacting a xylylenediamine condensate with an oxide catalyst of silica or alumina system in the presence of a molecular oxygen-containing gas or a mixture of a molecular oxygen-containing gas and ammonia.
摘要翻译：通过在含分子氧的气体或含分子氧的气体和氨的混合物的存在下使苯二甲胺缩合物与二氧化硅或氧化铝体系的氧化物催化剂接触，生产邻苯二腈。

7. 发明授权

US4246417A Treatment of waste water from nitrile production 失效
标题翻译：处理腈水生产废水
公开(公告)号：US4246417A
公开(公告)日：1981-01-20
申请号：US905958
申请日：1978-05-15
申请人： Utah Tsao
发明人： Utah Tsao
IPC分类号： B01D3/38 , C02F1/20 , C02F1/58 , C02F9/00 , C07D213/57 , C07C121/30 , C07C121/54 , C07C121/56
CPC分类号： C02F1/586 , B01D3/38 , C02F1/20 , C02F2103/38 , Y10S203/03
摘要： Waste water recovered from a nitrile production effluent, containing ammonia, hydrogen cyanide, carbon dioxide and water soluble polymers is stripped of ammonia, carbon dioxide and hydrogen cyanide to produce an aqueous stream containing the water soluble polymer. At least a portion of this stream is introduced into a steam scrubber to generate steam therefrom, with scrubber bottoms and any remaining water from the stripping operation being introduced into a reboiler to provide steam for the stripping and an aqueous concentrate of the water soluble polymer. Heat for the reboiler can be provided by indirect heat transfer with steam from the scrubber which produces a condensate suitable as feed water for steam generation.
摘要翻译：从腈生产流出物中回收的含氨，氰化氢，二氧化碳和水溶性聚合物的废水被除去氨，二氧化碳和氰化氢，以产生含有水溶性聚合物的水流。将该流的至少一部分引入蒸汽洗涤器以从其中产生蒸汽，其中洗涤塔底部和来自汽提操作的任何剩余的水被引入再沸器以提供用于汽提的蒸汽和水溶性聚合物的含水浓缩物。用于再沸器的热可以通过间接传热与来自洗涤器的蒸汽提供，其产生适于作为用于蒸汽产生的给水的冷凝物。

8. 发明授权

US3901935A Cyanophenyl sulfoxides and sulfones 失效
标题翻译： CYANOPHENYL SULFOXIDES和SULFONES
公开(公告)号：US3901935A
公开(公告)日：1975-08-26
申请号：US44359374
申请日：1974-02-19
申请人： DOW CHEMICAL CO
发明人： DOMENICO PENELOPE B
IPC分类号： C09K15/28 , A01N20060101 , A01N41/10 , C07C20060101 , C07C67/00 , C07C313/00 , C07C315/02 , C07C317/00 , C07C317/14 , C07C317/44 , C09D20060101 , C09D7/00 , C09D7/12 , C07C121/52 , C07C121/56
CPC分类号： C07C317/00
摘要： Fungicidal cyanophenyl sulfoxides and sulfones having the formula:

WHEREIN M IS 1 OR 2; N IS 1 OR 2; P IS 2, 3 OR 4; R is an alkyl or alkenyl group having 1 to 4 carbons and substituted with zero to two -Br, -Cl or F radicals; and X is -Br or -Cl, independently in each occurrence. The dicyano compounds are more active and are accordingly preferred. The disclosed compounds are of particular utility as paint film preservatives and microbicides.

9. 发明授权

US3544617A Process for the manufacture of aromatic nitriles 失效
标题翻译：制备硝基苯胺的方法
公开(公告)号：US3544617A
公开(公告)日：1970-12-01
申请号：US3544617D
申请日：1967-12-27
申请人： SHOWA DENKO KK
发明人： OGA TAIJIRO , ICHINOKAWA HIDEO , ITO MASATOMO
IPC分类号： B01J21/16 , C07C255/49 , C07D213/84 , C07C121/04 , C07C121/52 , C07C121/56
CPC分类号： C07D213/84 , B01J21/16 , C07C253/28 , C07C255/50 , C07C255/51

10. 发明授权

US4351776A Preparation of iodophthalonitrile 失效
标题翻译：碘邻苯二腈的制备
公开(公告)号：US4351776A
公开(公告)日：1982-09-28
申请号：US195999
申请日：1980-10-08
申请人： Teddy M. Keller , James R. Griffith
发明人： Teddy M. Keller , James R. Griffith
IPC分类号： C07C255/51 , C07D487/22 , C07C121/56
CPC分类号： C07D487/22 , C07C255/00
摘要： Iodophthalonitrile is prepared by mixing aminophthalonitrile with sulfuric acid at a temperature below 25.degree. C., reacting that product with sodium nitrite at a temperature below 15.degree. C., and reacting that product with potassium iodide at a temperature below 20.degree. C. A fluoroalkyl phthalonitrile is prepared by mixing fluoroalkyl iodide, activated copper, iodophthalonitrile, and a solvent under an inert atmosphere at a temperature from 110.degree. C. to 125.degree. C. at least until the solution turns green. Both compounds are useful in synthesizing phthalocyanines and polyphthalocyanines.
摘要翻译：通过在低于25℃的温度下将氨基邻苯二甲腈与硫酸混合，将该产物与低于15℃的亚硝酸钠反应，并在低于20℃的温度下使该产物与碘化钾反应制备碘代邻苯二甲腈。邻苯二腈通过在惰性气氛下在110℃至125℃的温度下混合氟代烷基碘，活化的铜，碘代邻苯二甲腈和溶剂来制备，至少直到溶液变绿。这两种化合物都可用于合成酞菁和多酞菁。

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