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1. 发明授权

US4482496A Stilbene compounds 失效
标题翻译：二苯乙烯化合物
公开(公告)号：US4482496A
公开(公告)日：1984-11-13
申请号：US383853
申请日：1982-06-01
申请人： Kurt Weber
发明人： Kurt Weber
IPC分类号： C09B57/00 , C07D235/18 , C07D237/14 , C07D249/06 , C07D249/20 , C07D249/24 , C07D261/08 , C07D263/56 , C07D263/57 , C07D271/10 , C07D271/107 , C07D271/113 , C07D471/04 , C07D498/04 , C07F9/40 , C07F9/653 , D06L3/12 , C07C121/78
CPC分类号： C07D263/57 , C07C255/00 , C07D237/14 , C07D249/06 , C07D249/20 , C07D249/24 , C07D261/08 , C07D271/107 , C07D271/113 , C07D471/04 , C07F9/4056 , C07F9/65324
摘要： The invention relates to stilbene compounds of the formula ##STR1## wherein Q is hydrogen; a monocyclic 5- or 6-membered aromatic heterocyclic ring which is unsubstituted or substituted by non-chromophoric groups and which contains no fused benzene rings or one or two fused benzene rings; a bicyclic 9-membered aromatic heterocyclic ring or the radical --CH.dbd.C(R.sub.1)(R.sub.2), in which R.sub.1 is hydrogen, C.sub.1 -C.sub.6 alkyl which is unsubstituted or substituted by non-chromophoric groups, and R.sub.2 is alkoxycarbonyl containing altogether 2 to 7 carbons atoms, cyano, carboxyl, carbamoyl, phosphonic acid dialkyl ester, C.sub.1 -C.sub.6 alkyl or arylsulfonyl; or Q may also be ##STR2## R.sub.o is hydrogen or C.sub.1 -C.sub.6 alkyl, R is C.sub.1 -C.sub.6 alkyl which is unsubstituted or substituted by non-chromophoric groups, C.sub.2 -C.sub.5 alkenyl, C.sub.2 -C.sub.5 alkynyl, di(C.sub.1 -C.sub.4)alkylamino(C.sub.1 -C.sub.4)alkyl, C.sub.1 -C.sub.4 hydroxyalkyl, C.sub.1 -C.sub.4 phenylalkyl or cycloalkyl containing 5 to 12 ring members, and each of m and n independently of the other is 1 or 2. These compounds may be used for whitening manmade, regenerated manmade and natural organic material of high molecular weight.
摘要翻译：本发明涉及下式的芪化合物：其中Q是氢; 未被取代或被非发色基团取代并且不含稠合苯环或一个或两个稠合苯环的单环5-或6-元芳族杂环; 双环9元芳族杂环或基团-CH = C（R 1）（R 2），其中R 1是氢，未被取代或被非发色基团取代的C 1 -C 6烷基，R 2是含有2至 7个碳原子，氰基，羧基，氨基甲酰基，膦酸二烷基酯，C 1 -C 6烷基或芳基磺酰基; 或者Q也可以是R a是氢或C 1 -C 6烷基，R是未被取代或被非发色基团取代的C 1 -C 6烷基，C 2 -C 5烯基，C 2 -C 5炔基，二（C 1 -C 4）烷基氨基（C 1 -C 4） C4）烷基，C1-C4羟烷基，C1-C4苯基烷基或含有5至12个环成员的环烷基，m和n各自独立地为1或2.这些化合物可用于增白人造，再生人造和天然有机材料的高分子量。

2. 发明授权

US3849163A Process for the optical brightening of organic materials 失效
标题翻译：有机材料的光学加工工艺
公开(公告)号：US3849163A
公开(公告)日：1974-11-19
申请号：US29540572
申请日：1972-10-05
申请人： CIBA GEIGY AG
发明人： MEYER H , WEBER K , MAEDER E , GUGLIELMETTI L , SIEGRIST A , LIECHTI P
IPC分类号： C07D213/16 , C07D215/04 , C07D231/12 , C07D233/56 , C07D235/18 , C07D239/26 , C07D241/42 , C07D249/06 , C07D249/08 , C07D249/20 , C07D249/22 , C07D249/24 , C07D251/24 , C07D253/065 , C07D263/00 , C07D263/56 , C07D263/57 , C07D271/06 , C07D271/10 , C07D271/107 , C07D277/66 , C07D285/12 , D06P5/00 , C09B23/00
CPC分类号： C07D213/16 , C07D215/04 , C07D235/18 , C07D239/26 , C07D241/42 , C07D249/06 , C07D249/08 , C07D249/20 , C07D249/22 , C07D249/24 , C07D251/24 , C07D253/065 , C07D263/00 , C07D263/57 , C07D271/06 , C07D271/107 , C07D277/66 , C07D285/12
摘要： The present invention relates to a process for the optical brightening of organic materials using compounds of the formula

IN WHICH A REPRESENTS HYDROGEN, HALOGEN, THE METHYL GROUP OR THE METHOXY GROUP, Z1 and/or Z2 denotes a ring member CH- or N- and Alpha represents a hydrogen atom, a phenyl residue or a residue of the series

IN WHICH (I) at least one residue Alpha differs from hydrogen or phenyl and has the significance of one of the other residues quoted for Alpha , and in which (II) terminal phenyl or naphthyl residues may contain alkyl, halogen or alkoxy groups. These new compounds represent valuable optical brightening agents.
摘要翻译：本发明涉及一种使用下式的化合物进行有机材料的光学增白的方法：其中氢，卤素，甲基或甲氧基，Z1和/或Z2表示环成员= CH-或= N - 和α表示氢原子，苯基残基或其中的（I）的残基，至少一个残基α与氢或苯基不同，并且具有引用为α的其它残基之一的含义，其中（ II）末端苯基或萘基残基可以含有烷基，卤素或烷氧基。这些新化合物代表有价值的荧光增白剂。

3. 发明授权

US3819615A Process for the manufacture of stilbene compounds 失效
标题翻译：苯乙烯化合物的制备方法
公开(公告)号：US3819615A
公开(公告)日：1974-06-25
申请号：US30428972
申请日：1972-11-06
申请人： CIBA GEIGY AG
发明人： SIEGRIST A
IPC分类号： C07D333/52 , C07C1/00 , C07C2/84 , C07C15/52 , C07C15/54 , C07C17/00 , C07C25/24 , C07C67/00 , C07D249/20 , C07D249/24 , C07D263/56 , C07D263/62 , C07D263/64 , C07D307/77 , C07D307/79 , C07D307/92 , C07D333/54 , C07D333/74 , C09B57/00 , C07D55/02
CPC分类号： C07D263/64 , C07C15/54 , C07D249/20 , C07D249/24 , C07D307/79 , C07D307/92 , C07D333/54 , C07D333/74
摘要： THE PRESENT INVENTION PROVIDES A PROCESS FOR THE MANUFACTURE OF STILBENE COMPOUNDS OF THE FORMULA

2,2''-DI(Y-),4,4''-DI(A-)STILBENE

WHEREIN A STANDS FOR A BENZO (B)FURNAL-2-YL, NAPHTHO(1,2-B)FURAN-2-YL, NAPHTHOL(2,1-B)FURAN-2-YL, BENZO (B) THIOPHEN-2-YL, NAPHTHOL(2,1-B)THIOPNEH-2-YL, BENZOXAZOL2-7L, NAPHTHOXAZOL-2-YL, BENZOTRIAZOL-2-YL, NAPHTHOL(1,2-D) TRIAZOL-2-YL, BENZO(1,2-D:3,4-D'')BIS-TRAZOL-2-YL OR PHENETHINYL RADICAL, WHICH ITSELF CAN AGAIN BE SUBSTITUTED BY CHLORINE OR ALKYL, CYCLOHEXYL PHENYL-(1-4C)-ALKYL, PHENYL, METHYLENEDIOXY, PHENOXY OR ALKOXY GROUPS OR WHICH CAN CONTAIN A 6-MEMBERED CARBOCYCLIC RING WHICH IS FUSED TO IT AND WHEREIN Y STANDS FOR A HYDROGEN ATOM, CHLORINE OR THE N,N-DIMETHYLCARBAMYL RADICAL, CHARACTERISED IN THAT A COMPOUND OF THE FORMULA

1-CH3,2-Y,4-A-BENZENE

WHEREIN A AND Y HAVE THE PREVIOUSLY INDICATED MEANING IS OXIDISED IN DIMETHYLFORMAMIDE, WHILST EXCLUDING AIR, IN THE PRESENCE OF A POTASSIUM COMPOUND OF THE FORMULA

KOC(X-1)H(2X-1)

WHEREIN X DENOTES AN INTEGER FROM 1 TO 6, WITH THE AZOBENZENE OF THE FORMULA

((Z1-PHENYL)-N=N-),Z2-BENZENE

WHEREIN Z1 AND Z2 STAND FOR HYDROGEN OR CHLORINE; THE PRESENT INVENTION FURTHER PROVIDES NEW STILBENE DERIVATIVE WHICH CAN BE MANUFACTURE ACCORDING TO THIS PROCESS AND WHICH CAN BE USED AS OPTICAL BRIGHTENERS.

4. 发明授权

US3758462A Tri aryl azines as fluorescent whitening agents 失效
标题翻译：三氰基腈作为荧光白剂
公开(公告)号：US3758462A
公开(公告)日：1973-09-11
申请号：US3758462D
申请日：1970-08-28
申请人： CIBA GEIGY AG
发明人： SIEGRIST A , GUGLIELMETTI L , MEYER H , LIECHTI P , MAEDER E , WEBER K
IPC分类号： C07D213/16 , C07D215/04 , C07D231/12 , C07D233/56 , C07D235/18 , C07D239/26 , C07D241/42 , C07D249/06 , C07D249/08 , C07D249/20 , C07D249/22 , C07D249/24 , C07D251/24 , C07D253/065 , C07D263/00 , C07D263/56 , C07D263/57 , C07D271/06 , C07D271/10 , C07D271/107 , C07D277/66 , C07D285/12 , C09B23/00
CPC分类号： C07D213/16 , C07D215/04 , C07D235/18 , C07D239/26 , C07D241/42 , C07D249/06 , C07D249/08 , C07D249/20 , C07D249/22 , C07D249/24 , C07D251/24 , C07D253/065 , C07D263/00 , C07D263/57 , C07D271/06 , C07D271/107 , C07D277/66 , C07D285/12
摘要： THE PRESENT INVENTION RELATES TO NEW COMPOUNDS OF THE FORMULA

2,4,6-TRI(4-ALPHA,A-PHENYL)-S-TRIAZINE WHERE N2 IS Z2

AND N1 IS Z1

IN WHICH A REPRESENTS HYDROGEN, HALOGEN, THE METHYL GROUP OR THE METHOXY GROUP, Z1 AND/OR Z2 DENOTES A RING MEMBER =CH- OR =N- AND A REPRESENTS A HYDROGEN ATOM, A PHENYL RESIDUE OR A RESIDUE OF THE SERIES

C6H5-CH=CH-, (NAPHTH-1-YL)-CH=CH-, (NAPHTH-2-YL)-CH=CH-,

AND (BIPHENYL-4-YL)-CH=CH-

IN WHICH (I) AT LEAST ONE RESIDUE A DIFFERS FROM HYDROGEN OR PHENYL AND HAS THE SIGNIFICANCE OF ONE OF THE OTHER RESIDUES QUOTED FOR A, AND IN WHICH (II) TERMINAL PHENYL OR NAPHTHYL RESIDUES MAY CONTAIN ALKYL, HALOGEN OR ALKOXY GROUPS. THE NEW COMPOUNDS REPRESENT VALUABLE OPTICAL BRIGHTENING AGENTS.

5. 发明授权

US3732221A Heterocyclic compounds containing ethylene double bonds and process for their manufacture 失效
标题翻译：含有乙烯双酚的杂环化合物及其制造方法
公开(公告)号：US3732221A
公开(公告)日：1973-05-08
申请号：US3732221D
申请日：1971-05-11
申请人： CIBA GEIGY AG
发明人： SIEGRIST A , LIECHTI P , MAEDER E , GUGLIELMETTI L , MEYER H , WEBER K
IPC分类号： C07D213/16 , C07D215/04 , C07D231/12 , C07D233/56 , C07D235/18 , C07D239/26 , C07D241/42 , C07D249/06 , C07D249/08 , C07D249/20 , C07D249/22 , C07D249/24 , C07D251/24 , C07D253/065 , C07D263/00 , C07D263/56 , C07D263/57 , C07D271/06 , C07D271/10 , C07D271/107 , C07D277/66 , C07D285/12 , C09B23/00
CPC分类号： C07D213/16 , C07D215/04 , C07D235/18 , C07D239/26 , C07D241/42 , C07D249/06 , C07D249/08 , C07D249/20 , C07D249/22 , C07D249/24 , C07D251/24 , C07D253/065 , C07D263/00 , C07D263/57 , C07D271/06 , C07D271/107 , C07D277/66 , C07D285/12
摘要： IN WHICH R1 REPRESENTS A HETEROCYCLIC RING SYSTEM OF AROMATIC CHARACTER WHICH (A) CONTAINS AT LEAST ONE 5-MEMBERED OR 6-MEMBERED HETEROCYCLIC RING WITH AT LEAST ONE RING NITROGEN ATOM, (B) IS FREE OF HYDROGEN ATOMS WHICH (1) ARE BONDED TO RING NITROGEN ATOMS AND (2) WHICH ARE REPLACEABLE BY ALKALI METAL, AND (C) IS BONDED TO A RING MEMBER OF R2 BY MEANS OF A RING MEMBER OR HAS TWO ADJACENT RING MEMBERS IN COMMON WITH TWO ADJACENT RING MEMBERS OF R2, IN WHICH R2 DENOTES A CARBOCYCLIC OR HETEROCYCLIC RING SYSTEM OF AROMATIC CHARACTER WHICH CONTAINS 6 RING MEMBERS, AND WHICH OPTIONALLY IS CONDENSED WITH FURTHER AROMATIC OR HYDROAROMATIC RING SYSTEMS, AND IN WHICH (B) THE METHYL GROUP SHOWN IN THE FORMULA IS IN A P-POSITION TO THE BOND TO R1, IS REACTED WITH A SCHIFF BASE IN THE PRESENCE OF A STRONGLY BASIC ALKALI COMPOUND, WITH THE REACTION MEDIUM TO BE USED BEING A STRONGLY POLAR, NEUTRAL TO BASIC, ORGANIC SOLVENT WHICH (I) IS FREE OF ATOMS, ESPECIALLY HYDROGEN ATOMS, WHICH ARE REPLACEABLE BY ALKALI METAL AND (II) IS PRACTICALLY ANHYDROUS, EXCEPT IN THE CASE OF THE USE OF AN ALKALI HYDROXIDE AS THE STRONGLY BASIC ALKALI COMPOUND IN WHICH CASE THE ALKALI HYDROXIDE MAY HAVE A WATER CONTENT OF UP TO 25%.

R1-R2-CH3

THE PRESENT INVENTION COMPRISES A PROCESS FOR THE MANUFACTURE OF HETEROCYCLIC COMPOUNDS CONTAINING ETHYLENE DOUBLE BONDS. THIS PROCESS IS CHARACTERISED BY REACTING A COMPOUND OF FORMULA

6. 发明授权

US3679668A 1,2,4-triazolyl-(1)-derivatives of the stilbene and bis-styrylbenzene series,process for their manufacture and their use as optical brighteners 失效
标题翻译：苯乙烯和苯乙烯苯乙烯系列的1,2,4-三唑（1）衍生物及其制备方法及其作为光亮剂的使用
公开(公告)号：US3679668A
公开(公告)日：1972-07-25
申请号：US3679668D
申请日：1970-04-13
申请人： HOECHST AG
发明人： HORN ANTON , SCHINZEL ERICH , ROSCH GUNTER
IPC分类号： C07D249/16 , C07D249/20 , C07D249/24 , C07D521/00 , C07D99/02
CPC分类号： C07D249/16 , C07D231/12 , C07D233/56 , C07D249/08 , C07D249/20 , C07D249/24
摘要： 1,2,4-TRIAZOLYL-(1)-DERIVATIVES OF THE STILLBENE AND BISSTYRYLBENZENE SERIES ARE OBTAINED BY CONDENSATION OF THE CORRESPONDING PHENYLHYDRAZINES WITH FORMAMIDE. THE PRODUCTS ARE USEFUL AS OPTICAL BRIGHTENERS FOR VARIOUS SUBSTRATES.

7. 发明授权

US3417058A Brightened fine fabrics 失效
标题翻译：加亮的精细面料
公开(公告)号：US3417058A
公开(公告)日：1968-12-17
申请号：US53381366
申请日：1966-03-14
申请人： GAF CORP
发明人： STROBEL ALBERT F , CATINO SIGMUND C
IPC分类号： C07D249/24
CPC分类号： C07D249/24

8. 发明授权

US3759900A Optical brightening agents 失效
标题翻译：光学加工代理
公开(公告)号：US3759900A
公开(公告)日：1973-09-18
申请号：US3759900D
申请日：1970-06-04
申请人： BAYER AG
发明人： HORSTMANN W
IPC分类号： C07D231/12 , C07D249/04 , C07D249/24 , C07D55/22
CPC分类号： C07D231/12 , C07D249/04 , C07D249/24
摘要： OPTICAL BRIGHTENERS ON THE BASIS OF SALTS OF SULPHONIC ACIDS OF THE FORMULA

(4-X,2-(HO3S-)PHENYL)-CH=CH-(2-Z-1,4-PHENYLENE)-Y

IN WHICH X DENOTES A TRIAZINE, TRIAZOLE, NAPHTHOTRIAZOLE, PYRAZOLE, ACYLAMINO OR UREA RADICAL; Y REPRESNETS H, C1, CN OR X; Z DENOTES H OR-SO3H, WITH GUANIDINES OF THE GENERAL FORMULA

R1-N=C(-N(-R2)-R3)-N(-R4)-R1

IN WHICH R1 DENOTES H, NH2, ALKYL OR A CARBOCYCLIC RADICAL; R2, R3, R4 AND R5 REPRESNET H, ALKYL, A CARBOCYCLIC RADICAL; AND R2 TOGETHER WITH R3 OR R4 TOGETHER WITH R5 MAY ALSO DENOTE AN ALKYLENE RADICAL LINKED TO THE N-ATOM, COMPARED WITH THE FREE SULPHONIC ACID OR THE ALKALI METAL SALTS OF THE STILBENE-SULPHONIC ACIDS (I), THE SALTS WITH GUANIDINES (II) HAVE ADVANTAGES IN RESPECT OF THEIR SENSITIVITY TO HARDNESS, IN THE GRIGHTENING OF MIXED FABRICS AND IN SIMULTANEOUS HIGH QUALITY FINISHING AND OPTICAL BRIGHTENING.

9. 发明授权

US3743637A Phenanthrotriazolyl derivatives 失效
公开(公告)号：US3743637A
公开(公告)日：1973-07-03
申请号：US3743637D
申请日：1971-08-04
申请人： SANDOZ LTD
发明人： FLECK F , SCHMID H
IPC分类号： C07D249/24 , C09B43/06 , C07D55/02
CPC分类号： C09B43/06 , C07D249/24
摘要： PHENANTHRIOZOLYL DERIVATIVE OF FORMULA

2-((4-R3,R4-PHENYL)-C(-R2)=CH-(2-R1-1,4-PHENYLENE)-),

(HO3S)(M-1)-2H-PHENANTHRO(9,10-D)TRIAZOLE

WHERE R1 AND R4, INDEPENDENTLY OF EACH OTHER, STAND FOR H, F, CL, CN, COOH, SO3H, ALKYLSULPHONYL, ARYLSULPHONYL, AN AMIDE OR ESTER OF CARBOXYLIC ACID OR SULPHONIC ACID OR R1 JOINTLY WITH R2 FOR-O-CO, R2 FOR H OR -O-COR3 FOR R1, ALKYL WITH 1 TO 12 CARBON AROMS OR OPTIONALLY SUBSTITUTED PHENYL OR JOINTLY WITH R4 FOR

-CH=CH-CH=CH-

WHEN R4 IS VICINAL TO R3 AND M IS 1,2 OR 3.

10. 发明授权

US3441562A Process for preparing 2-(4-stilbyl) naphthotriazoles 失效
标题翻译：制备2-（4-苯基）萘甲酸酯的方法
公开(公告)号：US3441562A
公开(公告)日：1969-04-29
申请号：US3441562D
申请日：1967-09-01
申请人： GAF CORP
发明人： CATINO SIGMUND C , STROBEL ALBERT F
IPC分类号： C07D249/24 , C07D55/04 , D06L3/12
CPC分类号： C07D249/24

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