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1. 发明授权

US5552508A Difunctional bitricyclodecatriene monomers 失效
标题翻译：双功能双环癸烯单体
公开(公告)号：US5552508A
公开(公告)日：1996-09-03
申请号：US448637
申请日：1995-05-23
申请人： David C. Martin , Jeffrey S. Moore , Larry J. Mar koski , Kenneth A. Walker , Gary E. Spilman
发明人： David C. Martin , Jeffrey S. Moore , Larry J. Mar koski , Kenneth A. Walker , Gary E. Spilman
IPC分类号： C07C37/055 , C07C39/17 , C07C63/38 , C07C63/49 , C07C63/72 , C07C211/61 , C07C233/65 , C07C265/14 , C08G65/40 , C08G69/26 , C08G69/32 , C08G63/00
CPC分类号： C08G69/32 , C07C211/61 , C07C233/65 , C07C265/14 , C07C29/147 , C07C37/00 , C07C63/38 , C07C63/49 , C07C63/72 , C08G65/4012 , C08G69/26 , C07C2102/06 , C07C2103/08
摘要： Novel difunctionalized cyclobutabenzene monomers of the general formula: ##STR1## wherein Z can be hydrogens or a cyclobutane ring; and X and Y are carboxyl, amino, alcohol, isocyanate, acid halide, or bis-acyl halide groups. Exemplary difunctional bitricyclodecatriene monomers are [2,2'-bidicyclo[2.4.0]octa-1,3,5-triene]-5,5'-dicarboxylic acid (BXTA) and [2,2'-bitricyclo[6.2.0.0]deca-1,3,(6),7-triene]-7,7'-dicarboxylic acid (QXTA). The difunctionalized bitricyclodecatriene monomers can form part of a polymer backbone chain in which the multiple butane ring functionalities can be easily opened to produce strong, three-dimensional covalent bond crosslinking between polymer chains. The crosslinking can be induced simply by heating the polymer to a temperature in excess of 250.degree. C.
摘要翻译：新的具有以下通式的二官能化环丁苯类单体：其中Z可以是氢或环丁烷环; X和Y是羧基，氨基，醇，异氰酸酯，酰卤或双酰卤基。示例性双官能双环癸三烯单体是[2,2'-双环[2.4.0]八氢-1,3,5-三烯] -5,5'-二羧酸（BXTA）和[2,2'-二环[6.2.0.0 ]癸-1,3，（6），7-三烯] -7,7'-二羧酸（QXTA）。双官能化的双环癸三烯单体可以形成聚合物主链的一部分，其中多个丁烷环官能团可以容易地打开以在聚合物链之间产生强烈的三维共价键交联。可以简单地通过将聚合物加热到超过250℃的温度来诱导交联。

2. 发明授权

US5770763A Difunctional bitricyclodecatriene monomers 失效
公开(公告)号：US5770763A
公开(公告)日：1998-06-23
申请号：US705630
申请日：1996-08-30
申请人： David C. Martin , Jeffrey S. Moore , Larry J. Markoski , Kenneth A. Walker , Gary E. Spilman
发明人： David C. Martin , Jeffrey S. Moore , Larry J. Markoski , Kenneth A. Walker , Gary E. Spilman
IPC分类号： C07C37/055 , C07C39/17 , C07C63/38 , C07C63/49 , C07C63/72 , C07C211/61 , C07C233/65 , C07C265/14 , C08G65/40 , C08G69/26 , C08G69/32 , C07C205/12
CPC分类号： C08G69/32 , C07C211/61 , C07C233/65 , C07C265/14 , C07C29/147 , C07C37/00 , C07C63/38 , C07C63/49 , C07C63/72 , C08G65/4012 , C08G69/26 , C07C2102/06 , C07C2103/08
摘要： Novel difunctionalized cyclobutabenzene monomers of the general formula: ##STR1## wherein Z can be hydrogens or a cyclobutane ring; and X and Y are carboxyl, amino, alcohol, isocyanate, acid halide, or bis-acyl halide groups. Exemplary difunctional bitricyclodecatriene monomers are �2,2'-bidicyclo�2.4.0!octa-1,3,5-triene!-5,5'-dicarboxylic acid (BXTA) and �2,2'-bitricyclo�6.2.0.0!deca-1,3,(6),7-triene!-7,7'-dicarboxylic acid (QXTA). The difunctionalized bitricyclodecatriene monomers can form part of a polymer backbone chain in which the multiple butane ring functionalities can be easily opened to produce strong, three-dimensional covalent bond crosslinking between polymer chains. The crosslinking can be induced simply by heating the polymer to a temperature in excess of 250.degree. C.

3. 发明授权

US5418312A Difunctional cyclobutabenzene monomers 失效
标题翻译：二官能环丁苯类单体
公开(公告)号：US5418312A
公开(公告)日：1995-05-23
申请号：US284006
申请日：1994-08-01
申请人： David C. Martin , Jeffrey S. Moore , Larry J. Markoski , Kenneth A. Walker
发明人： David C. Martin , Jeffrey S. Moore , Larry J. Markoski , Kenneth A. Walker
IPC分类号： C07C37/055 , C07C39/17 , C07C63/38 , C07C63/49 , C07C63/72 , C07C211/61 , C07C233/65 , C07C265/14 , C08G65/40 , C08G69/26 , C08G69/32 , C08G63/00
CPC分类号： C07C265/14 , C07C211/61 , C07C233/65 , C07C37/00 , C07C63/38 , C07C63/49 , C07C63/72 , C08G65/4012 , C08G69/26 , C08G69/32 , C07C2102/06 , C07C2103/08
摘要： Novel difucntionalized cyclobutabenzene monomers of the general formula: ##STR1## wherein Z can be hydrogens or a cyclobutane ring; and X and Y are carboxyl, amino, alcohol, isocyanate, acid halide, or bis-acyl fluoride groups. In a particularly preferred embodiment, the cyclobutabenzene derivative is 1,2-dihydrocyclobutabenzene-3,6-carboxylic acid. The difunctionalized cyclobutabenzene monomer can form part of a polymer backbone chain, but has an additional functionality, the butane ring, which can be easily opened to produce strong, covalent bond crosslinking between polymer chains. The crosslinking can be induced simply by heating the polymer to a temperature in excess of 300.degree. C.
摘要翻译：新颖的通式为：其中Z可以是氢或环丁烷环的通式为：并且X和Y是羧基，氨基，醇，异氰酸酯，酰卤或双酰基氟基团。在一个特别优选的实施方案中，环丁苯衍生物是1,2-二氢环丁碱-3,6 - 羧酸。二官能化环丁苯单体可以形成聚合物主链的一部分，但具有额外的官能度丁烷环，其可容易地打开以在聚合物链之间产生强烈的共价键交联。可以简单地通过将聚合物加热到超过300℃的温度来诱导交联。

4. 发明授权

US5334752A Cyclobutabenzene monomers 失效
标题翻译：环丁苯类单体
公开(公告)号：US5334752A
公开(公告)日：1994-08-02
申请号：US907430
申请日：1992-07-01
申请人： David C. Martin , Jeffrey S. Moore , Larry J. Markoski , Kenneth A. Walker
发明人： David C. Martin , Jeffrey S. Moore , Larry J. Markoski , Kenneth A. Walker
IPC分类号： C07C37/055 , C07C39/17 , C07C63/38 , C07C63/49 , C07C63/72 , C07C211/61 , C07C233/65 , C07C265/14 , C08G65/40 , C08G69/26 , C08G69/32 , C07C205/12
CPC分类号： C07C265/14 , C07C211/61 , C07C233/65 , C07C37/00 , C07C63/38 , C07C63/49 , C07C63/72 , C08G65/4012 , C08G69/26 , C08G69/32 , C07C2102/06 , C07C2103/08
摘要： Novel difunctionalized cyclobutabenzene monomers of the general formula: ##STR1## wherein Z can be hydrogens or a cyclobutane ting; and X and Y are carbox amino, alcohol, isocyanate, acid halide, or bis-acyl fluoride groups. In a particularly preferred embodiment, the cyclobutabenzene derivative is 1,2-dihydrocyclobutabenzene-3,6-carboxylic acid. The difunctionalized cyclobutabenzene monomer can form part of a polymer backbone chain, but has an additional functionality, the butane ring, which can be easily opened to produce strong, covalent bond crosslinking between polymer chains. The crosslinking can be induced simply by heating the polymer to a temperature in excess of 300.degree. C.
摘要翻译：新的具有以下通式的双官能化环丁苯类单体：其中Z可以是氢或环丁烷; 并且X和Y是羧基，氨基，醇，异氰酸酯，酰卤或双酰基氟基团。在一个特别优选的实施方案中，环丁苯衍生物是1,2-二氢环丁碱-3,6 - 羧酸。二官能化环丁苯单体可以形成聚合物主链的一部分，但具有额外的官能度丁烷环，其可容易地打开以在聚合物链之间产生强烈的共价键交联。可以简单地通过将聚合物加热到超过300℃的温度来诱导交联。

5. 发明授权

US08846404B2 System for visual indication of mechanical damage 有权
标题翻译：机械损伤视觉指示系统
公开(公告)号：US08846404B2
公开(公告)日：2014-09-30
申请号：US13168166
申请日：2011-06-24
申请人： Susan A. Odom , Mary M. Caruso , Aaron D. Finke , Aaron C. Jackson , Jeffrey S. Moore , Nancy R. Sottos , Scott R. White
发明人： Susan A. Odom , Mary M. Caruso , Aaron D. Finke , Aaron C. Jackson , Jeffrey S. Moore , Nancy R. Sottos , Scott R. White
IPC分类号： G01N31/22 , G01N21/78 , B29C73/22
CPC分类号： G01N21/78
摘要： A self-indicating material system may include a solid polymer matrix having a first color, a first plurality of capsules in the matrix, and a plurality of particles in the matrix. The first plurality of capsules includes a first reactant, and the plurality of particles includes a second reactant, which forms a product when in contact with the first reactant. When a crack forms in the polymer matrix, at least a portion of the first plurality of capsules is ruptured, the first and second reactants form the product in the matrix, and the portion of the polymer matrix containing the product has a second color different from the first color. A self-indicating material system may include a solid polymer matrix, a plurality of capsules in the matrix, and an activator in the matrix, where the polymer matrix includes a first polymer and has a first color, the plurality of capsules includes a polymerizer, and the activator is an activator for the polymerizer. When a crack forms in the polymer matrix, at least a portion of the plurality of capsules is ruptured, the polymerizer and the activator form a second polymer in the crack, and the second polymer has a second color different from the first color.
摘要翻译：自指示材料系统可以包括具有第一颜色的固体聚合物基质，基质中的第一多个胶囊和基质中的多个颗粒。第一多个胶囊包括第一反应物，并且多个颗粒包括第二反应物，其在与第一反应物接触时形成产物。当在聚合物基体中形成裂纹时，第一多个胶囊的至少一部分破裂，第一和第二反应物在基质中形成产物，并且含有产物的聚合物基质的部分具有不同于第一种颜色。自指示材料系统可以包括固体聚合物基质，基质中的多个胶囊和基质中的活化剂，其中聚合物基质包括第一聚合物并且具有第一颜色，所述多个胶囊包括聚合反应器，并且活化剂是聚合反应器的活化剂。当在聚合物基质中形成裂纹时，多个胶囊的至少一部分破裂，聚合器和活化剂在裂纹中形成第二聚合物，并且第二聚合物具有与第一颜色不同的第二颜色。

6. 发明授权

US07566747B2 Wax particles for protection of activators, and multifunctional autonomically healing composite materials 有权
标题翻译：用于保护活化剂的蜡颗粒和多功能自动愈合复合材料
公开(公告)号：US07566747B2
公开(公告)日：2009-07-28
申请号：US10840937
申请日：2004-05-07
申请人： Jeffrey S. Moore , Joseph D. Rule , Scott R. White , Nancy R. Sottos , Eric N. Brown
发明人： Jeffrey S. Moore , Joseph D. Rule , Scott R. White , Nancy R. Sottos , Eric N. Brown
IPC分类号： C08K9/10
CPC分类号： B29C73/22 , C08F291/00 , C08K9/10
摘要： A composite material comprises (i) a polymer, (ii) a polymerizer, (iii) a protected corresponding activator for the polymerizer, and (iv) a plurality of capsules. The polymerizer is in the capsules, and the corresponding activator is protected with a corresponding encapsulant for the polymer and the polymerizer.
摘要翻译：复合材料包括（i）聚合物，（ii）聚合反应器，（iii）用于聚合反应器的受保护的相应的活化剂，和（iv）多个胶囊。聚合器在胶囊中，相应的活化剂用聚合物和聚合反应器的相应密封剂保护。

7. 发明申请

US20080305343A1 SELF-HEALING MATERIALS WITH MICROFLUIDIC NETWORKS 有权
标题翻译：具有微流控网络的自愈材料
公开(公告)号：US20080305343A1
公开(公告)日：2008-12-11
申请号：US11760517
申请日：2007-06-08
申请人： Kathleen S. Toohey , Nancy R. Sottos , Jennifer A. Lewis , Jeffrey S. Moore , Scott R. White
发明人： Kathleen S. Toohey , Nancy R. Sottos , Jennifer A. Lewis , Jeffrey S. Moore , Scott R. White
IPC分类号： B32B9/04
CPC分类号： B29C73/22 , B29C73/163 , Y10T428/31663
摘要： A composite material includes a polymeric layer and a substrate, in contact with the polymeric layer. The substrate includes a substrate matrix, a first microfluidic network in the substrate matrix and in fluid communication with the polymeric layer, and a polymerizer in the first microfluidic network. The composite material may further include an activator, and may be a self-healing composite.
摘要翻译：复合材料包括与聚合物层接触的聚合物层和基底。衬底包括衬底基质，衬底基质中的第一微流体网络和与聚合物层流体连通，以及第一微流体网络中的聚合反应器。复合材料还可以包括活化剂，并且可以是自修复复合物。

8. 发明授权

US06821485B2 Method and structure for microfluidic flow guiding 有权
标题翻译：微流体导流的方法和结构
公开(公告)号：US06821485B2
公开(公告)日：2004-11-23
申请号：US10071846
申请日：2002-02-08
申请人： David J. Beebe , Jeffrey S. Moore , Bin Zhao
发明人： David J. Beebe , Jeffrey S. Moore , Bin Zhao
IPC分类号： B01L302
CPC分类号： B82Y30/00 , B01L3/5027 , B01L3/502707 , B01L2300/089 , B01L2400/0672 , Y10T436/11 , Y10T436/117497 , Y10T436/118339 , Y10T436/2575
摘要： A flow of liquids is carried out on a microscale utilizing surface effects to guide the liquid on flow paths to maintain laminar flow. No sidewall confining structure is required, minimizing resistance to flow and allowing laminar flow to be maintained at high flow rates. The guiding structure has flow guiding stripes formed on one or both of facing base and cover surfaces which are wettable by a selected liquid to direct the liquid from a source location to a destination location. The regions adjacent to the guiding stripes on the base and cover surfaces are non-wettable. The smooth interface between the gas and liquid along the flowing stream allows gas-liquid reactions to take place as a function of diffusion across the interface without mixing of the gas and liquid. Liquid-liquid flows may also be guided with such structures.
摘要翻译：使用表面效应在微尺度上进行液体流动以将液体引导到流动路径上以保持层流。不需要侧壁约束结构，使流动阻力最小化，并允许层流维持在高流速。引导结构具有形成在一个或两个相对的基底和盖表面上的流动引导条纹，其可被选定的液体润湿以将液体从源位置引导到目的地位置。在基部和盖表面上与引导条相邻的区域是不可润湿的。沿着流动流动的气体和液体之间的平滑界面允许气 - 液反应作为扩散跨越界面而发生，而不会混合气体和液体。液 - 液流也可以用这种结构引导。

9. 发明授权

US06523559B2 Self-regulating microfluidic device and method of using the same 有权
标题翻译：自调节微流体装置及其使用方法
公开(公告)号：US06523559B2
公开(公告)日：2003-02-25
申请号：US09917523
申请日：2001-07-27
申请人： David J. Beebe , Jeffrey S. Moore , Robin Liu , David T. Eddington
发明人： David J. Beebe , Jeffrey S. Moore , Robin Liu , David T. Eddington
IPC分类号： G05D1103
CPC分类号： G05D11/08 , G05D21/00 , Y10T137/0329 , Y10T137/2509
摘要： In accordance with the present invention, a microfluidic device and method of using the same is provided for self-regulating the flow of fluid therethrough. The microfluidic device includes a body defining first and second flow channels. The first flow channel has an input for receiving the fluid and an output. The second flow channel has an input for receiving a compensating fluid to modify the value of the property of the fluid and an output communicating with the first flow channel. A polymeric material is disposed in the first flow channel downstream of the output of the second flow channel. The polymeric material has a volume responsive to the value of the property of the fluid. A valve is disposed in the second flow channel and is movable in response to the volume of the material. The valve is movable between the first open position allowing the compensating fluid to flow past the valve into the first flow channel and a second closed position limiting the flow of compensating fluid therepast.
摘要翻译：根据本发明，提供了一种微流体装置及其使用方法，用于自我调节流体的流动。微流体装置包括限定第一和第二流动通道的主体。第一流道具有用于接收流体和输出的输入。第二流动通道具有用于接收补偿流体以修改流体性质的值的输入和与第一流动通道连通的输出。聚合材料设置在第二流动通道的第二流动通道的输出的下游。聚合物材料具有响应于流体性质的值的体积。阀设置在第二流动通道中并且可以响应于材料的体积而移动。所述阀可在所述第一打开位置和所述第一关闭位置之间移动，所述第一打开位置允许所述补偿流体流过所述阀进入所述第一流动通道，以及限制所述补偿流体的流动的第二关闭

10. 发明授权

US09108364B2 Solvent-promoted self-healing materials 有权
标题翻译：溶剂促进自愈材料
公开(公告)号：US09108364B2
公开(公告)日：2015-08-18
申请号：US12739537
申请日：2008-10-27
申请人： Mary M. Caruso , David A. Delafuente , Benjamin J. Blaiszik , Jason M. Kamphaus , Nancy R. Sottos , Scott R. White , Jeffrey S. Moore
发明人： Mary M. Caruso , David A. Delafuente , Benjamin J. Blaiszik , Jason M. Kamphaus , Nancy R. Sottos , Scott R. White , Jeffrey S. Moore
IPC分类号： B29C73/22 , B29C73/16
CPC分类号： B29C73/163 , B29C73/22
摘要： A composite material includes a solid polymer matrix, a plurality of capsules and a liquid, in the capsules. The liquid includes from 50 to 100 wt % of a solvent, and from 0 to 50 wt % of a polymerizer. There is no polymerizer outside of the capsules. The solid polymer matrix may include a native activating moiety for the polymerizer. The solvent may have a swelling ratio with the solid polymer matrix of at least 1.1 and/or may have a polarity ET of from 0.10 to 0.50.
摘要翻译：复合材料包括胶囊中的固体聚合物基质，多个胶囊和液体。液体包含50-100重量％的溶剂和0-50重量％的聚合反应器。胶囊外没有聚合反应器。固体聚合物基质可以包括用于聚合反应器的天然活化部分。溶剂可以具有至少1.1的固体聚合物基质的溶胀比和/或可以具有0.10-0.50的极性ET。

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