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1. 发明授权

US08715415B2 Vitreous silica crucible for pulling silicon single crystal 有权
标题翻译：硅玻璃坩埚用于拉硅单晶
公开(公告)号：US08715415B2
公开(公告)日：2014-05-06
申请号：US12752374
申请日：2010-04-01
申请人： Makiko Kodama , Hiroshi Kishi , Minoru Kanda
发明人： Makiko Kodama , Hiroshi Kishi , Minoru Kanda
IPC分类号： C30B15/10
CPC分类号： C30B15/10 , C30B29/06 , C30B35/002
摘要： Provided is a vitreous silica crucible for pulling silicon single crystals, which can melt a silicon raw material in a short time and improve production yield of silicon single crystals by temporal change of an opaque vitreous silica layer. The vitreous silica crucible includes an opaque vitreous silica layer(11) provided on an outer surface thereof and containing plural bubbles, and a transparent vitreous silica layer(12) provided on an inner surface and not containing bubbles substantially. The opaque vitreous silica layer(11) has a bubble diameter distribution in which the content of bubbles having a diameter of less than 40 μm is 10% or more and less than 30%, the content of bubbles having a diameter of 40 μm or more and less than 90 μm is 40% or more and less than 80%, and the content of bubbles having a diameter equal to or more than 90 μm is 10% or more and less than 30%. Relatively small bubbles contained in the opaque vitreous silica layer(11) contribute to the thermal conductivity of a crucible at an initial pulling stage, and relatively large bubbles contained in the opaque vitreous silica layer are expanded through a long-term pulling process to thereby largely contribute to the warmth retaining property of the crucible at a later pulling stage.
摘要翻译：本发明提供一种用于拉伸硅单晶的石英玻璃坩埚，其可以在短时间内熔化硅原料，并且通过不透明氧化硅玻璃层的时间变化提高硅单晶的产率。石英玻璃坩埚包括设置在其外表面并且包含多个气泡的不透明玻璃状石英层（11），以及设置在内表面上且基本上不含有气泡的透明玻璃状石英层（12）。不透明玻璃状石英层（11）具有气泡直径分布，其中直径小于40μm的气泡的含量为10％以上且小于30％，气泡的直径为40μm以上小于90μm的是40％以上且小于80％，直径等于或大于90μm的气泡的含量为10％以上且小于30％。包含在不透明玻璃状二氧化硅层（11）中的相对小的气泡有助于在初始拉伸阶段的坩埚的导热性，并且通过长期拉伸工艺使包含在不透明玻璃状二氧化硅层中的相对大的气泡膨胀，从而大大地扩大有助于在稍后的拉动阶段坩埚的保温性能。

2. 发明申请

US20120160155A1 COMPOSITE CRUCIBLE, METHOD OF MANUFACTURING THE SAME, AND METHOD OF MANUFACTURING SILICON CRYSTAL 有权
标题翻译：复合硬质合金，其制造方法和制造硅晶体的方法
公开(公告)号：US20120160155A1
公开(公告)日：2012-06-28
申请号：US13394268
申请日：2010-08-20
申请人： Toshiaki Sudo , Takuma Yoshioka , Hiroshi Kishi , Takeshi Fujita , Minoru Kanda , Koichi Suzuki , Ken Kitahara
发明人： Toshiaki Sudo , Takuma Yoshioka , Hiroshi Kishi , Takeshi Fujita , Minoru Kanda , Koichi Suzuki , Ken Kitahara
IPC分类号： C30B15/10 , C03B19/02 , C03B20/00
CPC分类号： C04B41/5022 , C03B5/025 , C03B19/02 , C03B19/09 , C03B19/095 , C03C17/004 , C03C17/02 , C03C2217/213 , C03C2218/13 , C03C2218/17 , C04B35/185 , C04B41/009 , C04B41/86 , C04B2235/6027 , C30B15/10 , C30B29/06 , C30B35/002 , Y02P40/57 , Y10T117/1032 , C04B41/4527
摘要： The purpose of the present invention is to provide a crucible which has high viscosity at high temperature, and can be used for a long time, and can be manufactured at low cost, and a method of manufacturing the same. The composite crucible 10 is characterized in the use of mullite (3Al2O3.2SiO2) as the basic material of the crucible. The composite crucible 10 has the crucible body 11 made of mullite material whose main component is alumina and silica, and a transparent vitreous silica layer 12 formed on the inner surface of the crucible body 11. The thickness of the transparent vitreous silica layer 12 is smaller than that of the crucible body 11. The crucible body 11 can be formed by the slip casting method, and the transparent vitreous silica layer 12 can be formed by the thermal spraying method.
摘要翻译：本发明的目的是提供一种在高温下具有高粘度且长时间使用并且可以低成本制造的坩埚及其制造方法。复合坩埚10的特征在于使用莫来石（3Al2O3.2SiO2）作为坩埚的基本材料。复合坩埚10具有由主成分为氧化铝和二氧化硅的莫来石材料制成的坩埚体11和形成在坩埚体11的内表面上的透明玻璃状石英层12.透明玻璃状石英层12的厚度较小坩埚主体11可以通过流延法形成，透明玻璃状二氧化硅层12可以通过热喷涂法形成。

3. 发明授权

US08142565B2 Vitreous silica crucible for pulling single-crystal silicon 有权
标题翻译：用于拉拔单晶硅的玻璃状硅石坩埚
公开(公告)号：US08142565B2
公开(公告)日：2012-03-27
申请号：US12325033
申请日：2008-11-28
申请人： Hiroshi Kishi , Minoru Kanda
发明人： Hiroshi Kishi , Minoru Kanda
IPC分类号： C30B15/10 , C30B15/00
CPC分类号： C30B15/10 , C30B29/06 , Y10S117/90 , Y10T117/1024 , Y10T117/1032 , Y10T117/1052
摘要： A vitreous silica crucible for pulling single-crystal silicon, which is formed of vitreous silica and has a bottomed cylindrical shape, wherein, in a liquid-level movement range in the inner surface of the crucible, ranging from a position corresponding to the liquid surface level of a silicon melt at the time of stating the pulling of single-crystal silicon to a position corresponding to the liquid surface level of a silicon melt at the time of finishing the pulling of single-crystal silicon, the concentration of an OH group included in the vitreous silica is higher in an erosion thickness portion of the inner surface of the crucible than that in the range lower than the liquid surface level which is positioned below the liquid-level movement range.
摘要翻译：一种玻璃状石英玻璃坩埚，其用于拉拔由玻璃状二氧化硅形成的具有有底圆筒形状的单晶硅，其中，在坩埚内表面的液面移动范围内，从对应于液面的位置在完成拉伸单晶硅时，将单晶硅拉出到对应于硅熔体的液面的位置时的硅熔体的水平，包括OH基的浓度坩埚的内表面的侵蚀厚度部分的玻璃态二氧化硅的含量高于低于位于液面移动范围以下的液面的范围。

4. 发明授权

US09133063B2 Composite crucible, method of manufacturing the same, and method of manufacturing silicon crystal 有权
标题翻译：复合坩埚及其制造方法以及硅晶体的制造方法
公开(公告)号：US09133063B2
公开(公告)日：2015-09-15
申请号：US13394268
申请日：2010-08-20
申请人： Toshiaki Sudo , Takuma Yoshioka , Hiroshi Kishi , Takeshi Fujita , Minoru Kanda , Koichi Suzuki , Ken Kitahara
发明人： Toshiaki Sudo , Takuma Yoshioka , Hiroshi Kishi , Takeshi Fujita , Minoru Kanda , Koichi Suzuki , Ken Kitahara
IPC分类号： C30B15/10 , C03B19/02 , C03B20/00 , C04B41/50 , C03B19/09 , C04B35/185 , C04B41/00 , C04B41/86 , C30B29/06 , C30B35/00
CPC分类号： C04B41/5022 , C03B5/025 , C03B19/02 , C03B19/09 , C03B19/095 , C03C17/004 , C03C17/02 , C03C2217/213 , C03C2218/13 , C03C2218/17 , C04B35/185 , C04B41/009 , C04B41/86 , C04B2235/6027 , C30B15/10 , C30B29/06 , C30B35/002 , Y02P40/57 , Y10T117/1032 , C04B41/4527
摘要： The purpose of the present invention is to provide a crucible which has high viscosity at high temperature, and can be used for a long time, and can be manufactured at low cost, and a method of manufacturing the same. The composite crucible 10 is characterized in the use of mullite (3Al2O3.2SiO2) as the basic material of the crucible. The composite crucible 10 has the crucible body 11 made of mullite material whose main component is alumina and silica, and a transparent vitreous silica layer 12 formed on the inner surface of the crucible body 11. The thickness of the transparent vitreous silica layer 12 is smaller than that of the crucible body 11. The crucible body 11 can be formed by the slip casting method, and the transparent vitreous silica layer 12 can be formed by the thermal spraying method.
摘要翻译：本发明的目的是提供一种在高温下具有高粘度且长时间使用并且可以低成本制造的坩埚及其制造方法。复合坩埚10的特征在于使用莫来石（3Al2O3.2SiO2）作为坩埚的基本材料。复合坩埚10具有由主成分为氧化铝和二氧化硅的莫来石材料制成的坩埚体11和形成在坩埚体11的内表面上的透明玻璃状石英层12.透明玻璃状石英层12的厚度较小坩埚主体11可以通过流延法形成，透明玻璃状二氧化硅层12可以通过热喷涂法形成。

5. 发明申请

US20120160159A1 VITREOUS SILICA CRUCIBLE FOR PULLING SILICON SINGLE CRYSTAL AND METHOD OF MANUFACTURING THE SAME 有权
标题翻译：用于拉丝硅单晶的耐火二氧化硅巧克力及其制造方法
公开(公告)号：US20120160159A1
公开(公告)日：2012-06-28
申请号：US13394284
申请日：2010-08-10
申请人： Toshiaki Sudo , Makiko Kodama , Minoru Kanda , Hiroshi Kishi
发明人： Toshiaki Sudo , Makiko Kodama , Minoru Kanda , Hiroshi Kishi
IPC分类号： C30B15/10 , C03B20/00
CPC分类号： C03B19/095 , C30B15/10 , C30B29/06 , C30B29/18 , C30B35/002 , Y02P40/57 , Y10T117/1032
摘要： The present invention provides a vitreous silica crucible which can suppress the sidewall lowering of the crucible under high temperature during pulling a silicon single crystal, and a method of manufacturing such a vitreous silica crucible. The vitreous silica crucible 10 includes an opaque vitreous silica layer 11 provided on the outer surface side of the crucible and containing numerous bubbles, and a transparent vitreous silica layer 12 provided on the inner surface side. The opaque vitreous silica layer 11 includes a first opaque vitreous silica portion 11a provided on the crucible upper portion, and a second opaque vitreous silica portion 11b provided on the crucible lower portion. The specific gravity of the second opaque vitreous silica portion 11b is 1.7 to 2.1, and the specific gravity of the first opaque vitreous silica portion 11a is 1.4 to 1.8, and smaller than that of the second opaque vitreous silica portion. The particle size distribution of the material silica powder for the first opaque vitreous silica portion 11a is wider than that of the second opaque vitreous silica portion 11b, and the material silica powder for the first opaque vitreous silica portion 11a includes more fine powder than that for the second opaque vitreous silica portion 11b.
摘要翻译：本发明提供一种可以在拉拔硅单晶时抑制坩埚在高温下的侧壁降低的石英玻璃坩埚，以及制造这种石英玻璃坩埚的方法。玻璃状石英玻璃坩埚10包括设置在坩埚的外表面侧并且含有大量气泡的不透明玻璃状石英层11和设置在内表面侧的透明氧化硅玻璃层12。不透明玻璃状石英层11包括设置在坩埚上部的第一不透明玻璃状石英部分11a和设置在坩埚下部的第二不透明玻璃状石英部分11b。第二不透玻璃状二氧化硅部11b的比重为1.7〜2.1，第一不透明玻璃状石英部11a的比重为1.4〜1.8，小于第二不透明玻璃状二氧化硅部的比重。用于第一不透明玻璃状石英部分11a的材料二氧化硅粉末的粒度分布比第二不透明玻璃状二氧化硅部分11b的粒度分布宽，并且用于第一不透明玻璃状石英部分11a的材料二氧化硅粉末包含比第二不透明玻璃状石英部分11b。

6. 发明申请

US20120141622A1 APPARATUS FOR MANUFACTURING VITREOUS SILICA CRUCIBLE 审中-公开
标题翻译：用于制造维生素二氧化硅可溶性的装置
公开(公告)号：US20120141622A1
公开(公告)日：2012-06-07
申请号：US13308308
申请日：2011-11-30
申请人： Toshiaki Sudo , Hiroshi Kishi , Takeshi Fujita , Minoru Kanda
发明人： Toshiaki Sudo , Hiroshi Kishi , Takeshi Fujita , Minoru Kanda
IPC分类号： B29C35/02
CPC分类号： C03B19/095
摘要： Provided is an apparatus for manufacturing a vitreous silica crucible which has a structure which can reduce gaps between a partition wall and electrodes inserted into through-holes formed in the partition wall while enabling electrodes to move to adjust a heating temperature of arc discharge. A plate-shaped partition wall 15 is placed above the rotating mold 10. Electrodes 13 for heating and fusing are inserted into through-holes 16 penetrating in a thickness direction, and are directed toward the rotating mold 10. A rocking unit 40 is provided on an upper side of the partition wall 15 and rocks the electrodes 13 around virtual rocking axes P, and the virtual rocking axes P pass through the through-holes 16.
摘要翻译：本发明提供一种制造石英玻璃坩埚的装置，其具有能够减少分隔壁与插入形成在隔壁中的通孔的电极之间的间隙的结构，同时使电极移动以调节电弧放电的加热温度。板状分隔壁15被放置在旋转模具10的上方。用于加热和熔合的电极13被插入穿透厚度方向的通孔16中，并被引导到旋转模具10上。摆动单元40设置在分隔壁15的上侧并围绕虚拟摇摆轴线P围绕电极13，并且虚拟摇摆轴线P穿过通孔16。

7. 发明授权

US08286447B2 Method for producing quartz glass crucible 有权
标题翻译：生产石英玻璃坩埚的方法
公开(公告)号：US08286447B2
公开(公告)日：2012-10-16
申请号：US12169838
申请日：2008-07-09
申请人： Hiroshi Kishi , Minoru Kanda
发明人： Hiroshi Kishi , Minoru Kanda
IPC分类号： C03B19/01 , C03B19/06
CPC分类号： C03B19/095 , C30B15/10 , C30B35/002
摘要： A method of producing a quartz glass crucible by arc melting a quartz powder molded product loaded on the inner side of a mold while performing vacuum suction, includes initiating the melting of quartz powder from the rim edge of a quartz powder molded product, subsequently lowering the arc electrode or raising the mold to heat and melt the sections on the downside of the rim edge. The method is preferably carried out such that the inner surface of the crucible is sealed within a time corresponding to 10% of the total arc time starting from the initiation of arc melting, and the seal thickness is 3 mm or less. The quartz glass crucible thus produced is useful for the pulling up of silicon single crystals and has a uniform glass layer with fewer internal bubbles.
摘要翻译：通过电弧熔融装载在模具内侧的石英粉末成形体同时进行真空抽吸来制造石英玻璃坩埚的方法包括从石英粉末成型品的边缘开始熔融石英粉末，随后将电弧电极或提升模具以加热和熔化边缘边缘的下侧的部分。该方法优选进行，使得坩埚的内表面在从电弧熔化开始起的总电弧时间的10％的时间内密封，并且密封厚度为3mm以下。由此制造的石英玻璃坩埚可用于提升硅单晶，并且具有均匀的具有较少内部气泡的玻璃层。

8. 发明授权

US08163083B2 Silica glass crucible and method for pulling up silicon single crystal using the same 有权
标题翻译：二氧化硅玻璃坩埚和使用其同时提升硅单晶的方法
公开(公告)号：US08163083B2
公开(公告)日：2012-04-24
申请号：US12169828
申请日：2008-07-09
申请人： Hiroshi Kishi , Minoru Kanda
发明人： Hiroshi Kishi , Minoru Kanda
IPC分类号： C30B11/00 , C30B15/00 , C30B21/06 , C30B27/02 , C30B28/10 , C30B30/04 , C30B19/00 , C30B9/00 , C30B17/00 , C30B21/02 , C30B28/06
CPC分类号： C30B15/10 , C30B29/06 , Y10T117/1032
摘要： A silica glass crucible causing fewer pinholes in silicon single crystals is provided by a method of preventing pinholes by performing the pulling up of a silicon single crystal while restraining the dissolution rate of the crucible inner surface to 20 μm/hr or less, using a silica glass crucible for the pulling up of silicon single crystals, wherein the area of crystalline silica formed by crystallization of amorphous silica is restricted to 10% or less of the crucible inner surface area, or the density of pits formed from open bubbles on the crucible inner surface is restricted to 0.01 to 0.2 counts/mm2.
摘要翻译：通过使用二氧化硅将硅坩埚内表面的溶解速度抑制为20μm/小时以下，通过进行硅单晶的拉拔来防止针孔的方法来提供硅单晶中的针孔少的石英玻璃坩埚用于提取硅单晶的玻璃坩埚，其中由无定形二氧化硅结晶形成的结晶二氧化硅的面积限制在坩埚内表面积的10％以下，或坩埚内部由开放气泡形成的凹坑的密度表面限制在0.01〜0.2个/ mm2。

9. 发明授权

US08936685B2 Vitreous silica crucible for pulling silicon single crystal and method of manufacturing the same 有权
标题翻译：用于拉硅单晶的玻璃状硅石坩埚及其制造方法
公开(公告)号：US08936685B2
公开(公告)日：2015-01-20
申请号：US13394284
申请日：2010-08-20
申请人： Toshiaki Sudo , Makiko Kodama , Minoru Kanda , Hiroshi Kishi
发明人： Toshiaki Sudo , Makiko Kodama , Minoru Kanda , Hiroshi Kishi
IPC分类号： C30B15/10 , C03B19/09 , C30B29/06 , C30B35/00 , C30B29/18
CPC分类号： C03B19/095 , C30B15/10 , C30B29/06 , C30B29/18 , C30B35/002 , Y02P40/57 , Y10T117/1032
摘要： The present invention provides a vitreous silica crucible which can suppress the sidewall lowering of the crucible under high temperature during pulling a silicon single crystal, and a method of manufacturing such a vitreous silica crucible. The vitreous silica crucible 10 includes an opaque vitreous silica layer 11 provided on the outer surface side of the crucible and containing numerous bubbles, and a transparent vitreous silica layer 12 provided on the inner surface side. The opaque vitreous silica layer 11 includes a first opaque vitreous silica portion 11a provided on the crucible upper portion, and a second opaque vitreous silica portion 11b provided on the crucible lower portion. The specific gravity of the second opaque vitreous silica portion 11b is 1.7 to 2.1, and the specific gravity of the first opaque vitreous silica portion 11a is 1.4 to 1.8, and smaller than that of the second opaque vitreous silica portion. The particle size distribution of the material silica powder for the first opaque vitreous silica portion 11a is wider than that of the second opaque vitreous silica portion 11b, and the material silica powder for the first opaque vitreous silica portion 11a includes more fine powder than that for the second opaque vitreous silica portion 11b.
摘要翻译：本发明提供一种可以在拉拔硅单晶时抑制坩埚在高温下的侧壁降低的石英玻璃坩埚，以及制造这种石英玻璃坩埚的方法。玻璃状石英玻璃坩埚10包括设置在坩埚的外表面侧并且含有大量气泡的不透明玻璃状石英层11和设置在内表面侧的透明氧化硅玻璃层12。不透明玻璃状石英层11包括设置在坩埚上部的第一不透明玻璃状石英部分11a和设置在坩埚下部的第二不透明玻璃状石英部分11b。第二不透玻璃状二氧化硅部11b的比重为1.7〜2.1，第一不透明玻璃状石英部11a的比重为1.4〜1.8，小于第二不透明玻璃状二氧化硅部的比重。用于第一不透明玻璃状石英部分11a的材料二氧化硅粉末的粒度分布比第二不透明玻璃状二氧化硅部分11b的粒度分布宽，并且用于第一不透明玻璃状石英部分11a的材料二氧化硅粉末包含比第二不透明玻璃状石英部分11b。

10. 发明授权

US08196430B2 Method and apparatus for manufacturing vitreous silica crucible 有权
标题翻译：石英玻璃坩埚的制造方法和装置
公开(公告)号：US08196430B2
公开(公告)日：2012-06-12
申请号：US12303994
申请日：2008-11-28
申请人： Hiroshi Kishi , Minoru Kanda , Masaki Morikawa
发明人： Hiroshi Kishi , Minoru Kanda , Masaki Morikawa
IPC分类号： C03B19/01 , C03B19/09 , C03B19/06
CPC分类号： C03B19/095 , C30B15/10 , Y02P40/57
摘要： A method of manufacturing a vitreous silica crucible by a rotary mold method, which includes performing arc melting in a state in which electrodes are provided so as to be shifted from a mold central line, wherein, by this eccentric arc, the glass temperature difference during melting of a straight body portion, a curved portion and a bottom of the crucible is controlled to 300° C. or below and the thickness of a transparent layer of the straight body portion and the bottom is controlled to 70 to 120% of the thickness of a transparent layer of the curved portion.
摘要翻译：一种通过旋转模具法制造石英玻璃坩埚的方法，其包括在设置电极以使其从模具中心线偏移的状态下进行电弧熔化，其中，通过该偏心弧，玻璃温度差在将坩埚的直体部分，弯曲部分和底部的熔化控制在300℃以下，直体部分和底部的透明层的厚度被控制在厚度的70〜120％的弯曲部分的透明层。

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