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1. 发明授权

US09634251B2 Nanotube solution treated with molecular additive, nanotube film having enhanced adhesion property, and methods for forming the nanotube solution and the nanotube film 有权
公开(公告)号：US09634251B2
公开(公告)日：2017-04-25
申请号：US13416820
申请日：2012-03-09
申请人： David A. Roberts , Rahul Sen , Peter Sites , J. Thomas Kocab , Billy Smith , Feng Gu
发明人： David A. Roberts , Rahul Sen , Peter Sites , J. Thomas Kocab , Billy Smith , Feng Gu
IPC分类号： H01B1/04 , B82Y40/00 , H01L51/00 , B82Y30/00 , C01B31/02 , B82Y10/00 , H01L21/02
CPC分类号： C09D5/24 , B82Y10/00 , B82Y30/00 , B82Y40/00 , C01B31/026 , C01B31/0273 , C01B32/17 , C01B2202/02 , C01B2202/22 , C09D1/00 , H01L21/02532 , H01L21/02606 , H01L21/02628 , H01L51/0003 , H01L51/0048 , Y10S977/75 , Y10S977/845 , Y10S977/932
摘要： The present disclosure provides a nanotube solution being treated with a molecular additive, a nanotube film having enhanced adhesion property due to the treatment of the molecular additive, and methods for forming the nanotube solution and the nanotube film. The nanotube solution includes a liquid medium, nanotubes in the liquid medium, and a molecular additive in the liquid medium, wherein the molecular additive includes molecules that provide source elements for forming a group IV oxide within the nanotube solution. The molecular additive can introduce silicon (Si) and/or germanium (Ge) in the liquid medium, such that nominal silicon and/or germanium concentrations of the nanotube solution ranges from about 5 ppm to about 60 ppm.

2. 发明申请

US20130052449A1 METHODS FOR CONTROLLING DENSITY, POROSITY, AND/OR GAP SIZE WITHIN NANOTUBE FABRIC LAYERS AND FILMS 有权
标题翻译：用于控制纳米纤维层和薄膜中密度，孔隙度和/或尺寸的方法
公开(公告)号：US20130052449A1
公开(公告)日：2013-02-28
申请号：US13578691
申请日：2011-02-14
申请人： Rahul Sen , J. Thomas Kocab , Feng Gu
发明人： Rahul Sen , J. Thomas Kocab , Feng Gu
IPC分类号： H01B1/04 , B32B5/16 , B82Y30/00 , B82Y40/00
CPC分类号： B82Y30/00 , C01B32/158 , C01B2202/02 , C01B2202/06 , C01B2202/22 , C01B2202/34 , C01B2202/36 , G11C13/025 , Y10S977/751 , Y10S977/752 , Y10T428/249921
摘要： A method for controlling density, porosity and/or gap size within a nanotube fabric layer is disclosed. In one aspect, this can be accomplished by controlling the degree of rafting in a nanotube fabric. In one aspect, the method includes adjusting the concentration of individual nanotube elements dispersed in a nanotube application solution. A high concentration of individual nanotube elements will tend to promote rafting in a nanotube fabric layer formed using such a nanotube application solution, whereas a lower concentration will tend to discourage rafting. In another aspect, the method includes adjusting the concentration of ionic particles dispersed in a nanotube application solution. A low concentration of ionic particles will tend to promote rafting in a nanotube fabric layer formed using such a nanotube application solution, whereas a higher concentration will tend to discourage rafting. In other aspects, both concentration parameters are adjusted.
摘要翻译：公开了一种用于控制纳米管织物层内的密度，孔隙率和/或间隙尺寸的方法。在一个方面，这可以通过控制纳米管织物中漂流的程度来实现。一方面，该方法包括调节分散在纳米管应用溶液中的单个纳米管元件的浓度。单个纳米管元件的高浓度倾向于促进在使用这种纳米管施用溶液形成的纳米管织物层中的漂流，而较低浓度将倾向于阻止漂流。另一方面，该方法包括调节分散在纳米管应用溶液中的离子颗粒的浓度。低浓度的离子颗粒倾向于促进在使用这种纳米管施用溶液形成的纳米管织物层中的漂流，而较高的浓度将倾向于阻止漂流。在其他方面，调整浓度参数。

3. 发明授权

US09617151B2 Methods for controlling density, porosity, and/or gap size within nanotube fabric layers and films 有权
公开(公告)号：US09617151B2
公开(公告)日：2017-04-11
申请号：US13578691
申请日：2011-02-14
申请人： Rahul Sen , J. Thomas Kocab , Feng Gu
发明人： Rahul Sen , J. Thomas Kocab , Feng Gu
IPC分类号： C01B31/02 , H01B1/04 , B82Y40/00 , B82Y30/00 , G11C13/02
CPC分类号： B82Y30/00 , C01B32/158 , C01B2202/02 , C01B2202/06 , C01B2202/22 , C01B2202/34 , C01B2202/36 , G11C13/025 , Y10S977/751 , Y10S977/752 , Y10T428/249921
摘要： A method for controlling density, porosity and/or gap size within a nanotube fabric layer is disclosed. In one aspect, this can be accomplished by controlling the degree of rafting in a nanotube fabric. In one aspect, the method includes adjusting the concentration of individual nanotube elements dispersed in a nanotube application solution. A high concentration of individual nanotube elements will tend to promote rafting in a nanotube fabric layer formed using such a nanotube application solution, whereas a lower concentration will tend to discourage rafting. In another aspect, the method includes adjusting the concentration of ionic particles dispersed in a nanotube application solution. A low concentration of ionic particles will tend to promote rafting in a nanotube fabric layer formed using such a nanotube application solution, whereas a higher concentration will tend to discourage rafting. In other aspects, both concentration parameters are adjusted.

4. 发明申请

US20130243954A1 NANOTUBE SOLUTIONS WITH HIGH CONCENTRATION AND LOW CONTAMINATION AND METHODS FOR PURIFIYING NANOTUBE SOLUTIONS 审中-公开
标题翻译：具有高浓度和低污染性的纳米级溶液和用于纯化纳米溶液的方法
公开(公告)号：US20130243954A1
公开(公告)日：2013-09-19
申请号：US13825070
申请日：2011-09-20
申请人： David A. Roberts , Rahul Sen , J. Thomas Kocab , Billy Smith , Feng Gu
发明人： David A. Roberts , Rahul Sen , J. Thomas Kocab , Billy Smith , Feng Gu
IPC分类号： H01L51/00
CPC分类号： H01L51/0048 , B01D21/262 , B01D37/00 , B01D2251/90 , B01D2251/902 , B05D1/005 , B05D1/02 , B82Y40/00 , C02F1/36 , C02F1/38 , C02F1/444 , C02F1/5236 , C02F1/683 , C02F2101/20
摘要： Solutions of carbon nanotubes and methods for purifying the solutions are provided. The methods include mixing, for example, at least one complexing agents, at least one ionic species, and/or at least one buffer oxide etch (BOE) with a liquid medium containing carbon nanotubes and different types of contaminants, such as metal impurities, amorphous carbon, and/or silica particles, and performing a filtration process to the liquid medium so as to remove or reduce the contaminants in the liquid medium. As a result, carbon nanotube solutions of low contaminants are produced. In some embodiments, the solutions of this disclosure include a high concentration of carbon nanotubes and are substantially free from metal, amorphous carbon, and/or silica impurities.
摘要翻译：提供了碳纳米管的解决方案和纯化溶液的方法。所述方法包括将例如至少一种络合剂，至少一种离子种类和/或至少一种缓冲氧化物蚀刻（BOE）与含有碳纳米管和不同类型污染物（例如金属杂质）的液体介质混合，无定形碳和/或二氧化硅颗粒，并且对液体介质进行过滤处理以除去或减少液体介质中的污染物。结果，产生了低污染物的碳纳米管溶液。在一些实施方案中，本公开的溶液包括高浓度的碳纳米管，并且基本上不含金属，无定形碳和/或二氧化硅杂质。

5. 发明授权

US10069072B2 Nanotube solutions with high concentration and low contamination and methods for purifiying nanotube solutions 有权
公开(公告)号：US10069072B2
公开(公告)日：2018-09-04
申请号：US13825070
申请日：2011-09-20
申请人： David A. Roberts , Rahul Sen , J. Thomas Kocab , Billy Smith , Feng Gu
发明人： David A. Roberts , Rahul Sen , J. Thomas Kocab , Billy Smith , Feng Gu
IPC分类号： B05D1/02 , H01L51/00 , B82Y40/00 , C02F1/68 , B05D1/00 , B01D37/00 , B01D21/26 , C02F1/36 , C02F1/38 , C02F1/44 , C02F1/52 , C02F101/20
摘要： Solutions of carbon nanotubes and methods for purifying the solutions are provided. The methods include mixing, for example, at least one complexing agents, at least one ionic species, and/or at least one buffer oxide etch (BOE) with a liquid medium containing carbon nanotubes and different types of contaminants, such as metal impurities, amorphous carbon, and/or silica particles, and performing a filtration process to the liquid medium so as to remove or reduce the contaminants in the liquid medium. As a result, carbon nanotube solutions of low contaminants are produced. In some embodiments, the solutions of this disclosure include a high concentration of carbon nanotubes and are substantially free from metal, amorphous carbon, and/or silica impurities.

6. 发明申请

US20140329430A1 Low Defect Nanotube Application Solutions and Fabrics and Methods for Making Same 有权
标题翻译：低缺陷纳米管应用解决方案和织物及其制作方法
公开(公告)号：US20140329430A1
公开(公告)日：2014-11-06
申请号：US14265602
申请日：2014-04-30
申请人： J. Thomas Kocab , Thomas R. Bengtson , Sanjin Hosic , Rahul Sen , Billy Smith , David A. Roberts , Peter Sites
发明人： J. Thomas Kocab , Thomas R. Bengtson , Sanjin Hosic , Rahul Sen , Billy Smith , David A. Roberts , Peter Sites
IPC分类号： D06B23/20 , D04H1/732
CPC分类号： B01D19/0005 , B01D19/0031 , B01D19/0036 , B01D19/0057 , B01D19/0078 , B05D1/005 , B05D3/002 , B05D3/12 , B05D7/24 , D04H1/4242 , D04H1/732 , Y10T442/60
摘要： The present disclosure provides methods for removing defects nanotube application solutions and providing low defect, highly uniform nanotube fabrics. In one aspect, a degassing process is performed on a suspension of nanotubes to remove air bubbles present in the solution. In another aspect, a continuous flow centrifugation (CFC) process is used to remove small scale defects from the solution. In another aspect, a depth filter is used to remove large scale defects from the solution. According to the present disclosure, these three methods can be used alone or combined to realize a low defect nanotube application solutions and fabrics.
摘要翻译：本公开提供了用于去除缺陷纳米管应用解决方案并提供低缺陷，高度均匀的纳米管织物的方法。在一个方面，对纳米管的悬浮液进行脱气处理以除去溶液中存在的气泡。另一方面，使用连续流离心（CFC）方法从溶液中除去小规模的缺陷。在另一方面，深度滤波器用于从溶液中去除大规模的缺陷。根据本公开，这三种方法可以单独使用或组合使用以实现低缺陷纳米管应用解决方案和织物。

7. 发明授权

US10654718B2 Scalable nanotube fabrics and methods for making same 有权
公开(公告)号：US10654718B2
公开(公告)日：2020-05-19
申请号：US14033158
申请日：2013-09-20
申请人： Rahul Sen , Billy Smith , J. Thomas Kocab , Ramesh Sivarajan , Peter Sites , Thomas Rueckes , David A. Roberts
发明人： Rahul Sen , Billy Smith , J. Thomas Kocab , Ramesh Sivarajan , Peter Sites , Thomas Rueckes , David A. Roberts
IPC分类号： B82Y30/00 , H01H1/00 , D21H21/52 , D21H15/02 , D21H13/50 , D04H1/732 , D04H1/4242 , H01L23/532 , G11C13/02
摘要： The present disclosure provides scalable nanotube fabrics and methods for controlling or otherwise adjusting the nanotube length distribution of a nanotube application solution in order to realize scalable nanotube fabrics. In one aspect of the present disclosure, one or more filtering operations are used to remove relatively long nanotube elements from a nanotube solution until nanotube length distribution of the nanotube solution conforms to a preselected or desired nanotube length distribution profile. In another aspect of the present disclosure, a sono-chemical cutting process is used to break up relatively long nanotube elements within a nanotube application solution into relatively short nanotube elements to realize a pre-selected or desired nanotube length distribution profile.

8. 发明授权

US06855476B2 Photoacid generators for use in photoresist compositions 有权
标题翻译：用于光致抗蚀剂组合物的光酸发生剂
公开(公告)号：US06855476B2
公开(公告)日：2005-02-15
申请号：US10117693
申请日：2002-04-05
申请人： Lawrence Ferreira , Andrew J. Blakeney , Gregory Dominic Spaziano , Ognian Dimov , J. Thomas Kocab , John P. Hatfield
发明人： Lawrence Ferreira , Andrew J. Blakeney , Gregory Dominic Spaziano , Ognian Dimov , J. Thomas Kocab , John P. Hatfield
IPC分类号： C07C309/10 , C07C321/28 , C07C323/20 , C07C381/12 , C07D207/40 , C07D209/94 , C07D333/46 , G03F7/004 , G03F7/039 , G03F7/038 , G03F7/26
CPC分类号： C07C381/12 , C07C309/10 , G03F7/0045 , G03F7/0395 , Y10S430/114 , Y10S430/115 , Y10S430/122 , Y10S430/123
摘要： A photoacid compound having the following general structure: R—O(CF2)nSO3X wherein n is an integer between about 1 to 4; R is selected from the group consisting of: substituted or unsubstituted C1-C12 linear or branched alkyl or alkenyl, substituted or unsubstituted araalkyl, substituted or unsubstituted aryl, substituted or unsubstituted bicycloalkyl, substituted or unsubstituted tricycloalkyl, hydrogen, alkyl sulfonic acid, substituted or unsubstituted perfluoroalkyl, the general structure F((CF2)pO)m(CF2)q— wherein p is between about 1 to 4, m is between about 0 to 3 and q is between about 1 to 4, and substituted or unsubstituted partially fluorinated alkyl, halofluoroalkyl, perfluoroalkylsulfonic, or glycidyl; and X is selected from the group consisting of: organic cations and covalently bonded organic radicals.
摘要翻译：一种具有以下一般结构的光酸化合物：其中n是约1至4之间的整数; 取代或未取代的芳基，取代或未取代的双环烷基，取代或未取代的三环烷基，氢，烷基磺酸，取代或未取代的芳基，取代或未取代的芳烷基，未取代的全氟烷基，通式F（（CF 2）p O）m（CF 2）q - ，其中p为约1至4，m为约0至3，q为约1至4，取代或未取代的部分氟化烷基，卤氟烷基，全氟烷基磺酸或缩水甘油基; 并且X选自：有机阳离子和共价键合的有机基团。

9. 发明授权

US07416821B2 Thermally cured undercoat for lithographic application 有权
标题翻译：用于光刻应用的热固化底漆
公开(公告)号：US07416821B2
公开(公告)日：2008-08-26
申请号：US11075518
申请日：2005-03-09
申请人： Binod B De , Sanjay Malik , J. Thomas Kocab , Thomas Sarubbi
发明人： Binod B De , Sanjay Malik , J. Thomas Kocab , Thomas Sarubbi
IPC分类号： G03C3/00
CPC分类号： G03F7/094 , C09D133/14 , Y10S430/11 , Y10S430/111 , Y10S430/128
摘要： Thermally curable undercoat composition comprising for producing a bilayer relief image comprising: a) a polymer of Structure I comprising repeating units of Structure II, III, and IV b) a phenolic crosslinker; c) a thermal acid generator (TAG); and d) a solvent.
摘要翻译：包含用于制备双层浮雕图像的可热固化底涂层组合物，其包含：a）结构I的聚合物，其包含结构II，III和IV的重复单元b）酚交换剂; c）热酸生成器（TAG）; 和d）溶剂。

10. 发明授权

US06911297B2 Photoresist compositions 有权
标题翻译：光刻胶组合物
公开(公告)号：US06911297B2
公开(公告)日：2005-06-28
申请号：US10465000
申请日：2003-06-19
申请人： David Brzozowy , J. Thomas Kocab , John P. Hatfield , Lawerence Ferreira , Andrew Blakeney
发明人： David Brzozowy , J. Thomas Kocab , John P. Hatfield , Lawerence Ferreira , Andrew Blakeney
IPC分类号： G03F7/004 , G03F7/038 , G03F7/039 , G03F7/38 , G03F7/40 , H01L21/027
CPC分类号： G03F7/0046 , G03F7/0045 , G03F7/0392 , G03F7/0397 , G03F7/40
摘要： Radiation sensitive compositions for use in producing a patterned image on a substrate comprise: a) a first photoacid generator compound which comprises one or more compounds of the structure (A); b) a second photoacid generator compound which comprises one or more compounds of the structure (B); c) a polymer component comprising an alkali soluble resin component whose alkali solubility is suppressed by the presence of acid sensitive moieties and whose alkali solubility is returned by treatment with an acid and, optionally, heat; wherein said polymer comprises one or more polymers comprising the monomer unit (C); and d) a solvent.
摘要翻译：用于在衬底上生产图案化图像的辐射敏感组合物包括：a）包含一种或多种结构（A）化合物的第一光致酸发生剂化合物; b）包含一种或多种结构（B）的化合物的第二光酸产生剂化合物; c）包含碱溶性树脂组分的聚合物组分，其碱溶解度通过酸敏感部分的存在而被抑制，并且其碱溶解度通过用酸处理和任选地加热而返回; 其中所述聚合物包含一种或多种包含单体单元（C）的聚合物; 和d）溶剂。

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