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1. 发明申请

US20160177085A1 Epoxy Resin Containing Silicone-Modified Epoxy Resin and Polyvalent Carboxylic Acid Compound, and Cured Product Thereof 审中-公开
标题翻译：含有硅氧烷改性环氧树脂和多价羧酸化合物的环氧树脂及其固化产物
公开(公告)号：US20160177085A1
公开(公告)日：2016-06-23
申请号：US14973162
申请日：2015-12-17
申请人： Nippon Kayaku Kabushiki Kaisha , Shin-Etsu Chemical Co., Ltd.
发明人： Toshio Shiobara , Junichi Sawada , Miyuki Wakao , Tsutomu Kashiwagi , Naofusa Miyagawa , Yoshihiro Kawata , Chie Sasaki
IPC分类号： C08L63/00
CPC分类号： C08L63/00 , C08G59/3281 , C08G59/42 , C08G59/4215 , C08L2205/025 , G02B1/04 , H01L23/296 , H01L2924/0002 , H01L2924/00
摘要： A silicone-modified epoxy resin composition that offers a cured product excellent in low permeability to gas, mechanical strength, and heat resistance and transparency and further offers an optical semiconductor sealing material excellent in heat cycle resistance, and a cured epoxy resin product obtained by curing the composition. The epoxy resin composition comprises the following components (A) to (C): (A) a silicone-modified epoxy resin having a cyclic siloxane structure, (B) a silicone-modified epoxy resin having a branched siloxane structure, and (C) an epoxy resin curing agent containing a polyvalent carboxylic acid having a tricyclodecane structure and a carboxylic anhydride compound.
摘要翻译：一种硅氧烷改性环氧树脂组合物，其提供了低气体，机械强度，耐热性和透明性优异的固化产物，并且还提供了耐热循环性优异的光半导体密封材料和通过固化获得的固化环氧树脂产品组成。环氧树脂组合物包含以下组分（A）至（C）：（A）具有环状硅氧烷结构的硅氧烷改性环氧树脂，（B）具有支链硅氧烷结构的硅氧烷改性环氧树脂，和（C）含有具有三环癸烷结构的多元羧酸和羧酸酐化合物的环氧树脂固化剂。

2. 发明授权

US09139700B2 Method for preparing a polyorganosiloxane 有权
标题翻译：聚有机硅氧烷的制备方法
公开(公告)号：US09139700B2
公开(公告)日：2015-09-22
申请号：US14044962
申请日：2013-10-03
申请人： SHIN-ETSU CHEMICAL CO., LTD.
发明人： Takayuki Kusunoki , Yuusuke Takamizawa , Tsutomu Kashiwagi
IPC分类号： C08G77/08
CPC分类号： C08G77/08
摘要： One object of the present invention is to provide a method for preparing a polyorganosiloxane without using any catalyst having corrosivity and toxicity such as an alkaline earth metal catalyst in a condensation reaction of at least one organic silicon compound having a silanol group and/or an alkoxy silyl group. The present invention is a method for preparing a polyorganosiloxane, wherein the method includes a step of condensation reacting at least one organic silicon compound having at least one —OX group bonding to a silicon atom in the molecule, wherein X is a hydrogen atom, an alkyl group having 1 to 10 carbon atoms or an alkoxyalkyl group having 2 to 10 carbon atoms, in the presence of a catalyst, wherein the catalyst is at least one selected from the group having hydroxides or oxides of elements in Groups 3-15 of the periodic table.
摘要翻译：本发明的一个目的是提供一种在至少一种具有硅烷醇基的有机硅化合物和/或烷氧基的缩合反应中不使用任何具有腐蚀性和毒性的催化剂如碱土金属催化剂制备聚有机硅氧烷的方法甲硅烷基。本发明是一种制备聚有机硅氧烷的方法，其中该方法包括将至少一种至少一个具有至少一个-OX基团的有机硅化合物与分子中的硅原子键合的步骤，其中X是氢原子，在催化剂存在下，具有1至10个碳原子的烷基或具有2至10个碳原子的烷氧基烷基，其中所述催化剂是选自具有氢氧化物或第3-15族中的元素的氧化物的至少一种周期表。

3. 发明授权

US09117985B2 Silicone resin composition and an optical semiconductor device 有权
标题翻译：硅树脂组合物和光半导体装置
公开(公告)号：US09117985B2
公开(公告)日：2015-08-25
申请号：US14546569
申请日：2014-11-18
申请人： SHIN-ETSU CHEMICAL CO., LTD.
发明人： Yoshihira Hamamoto , Tsutomu Kashiwagi
IPC分类号： C08G77/08 , H01L33/56 , C08L83/14 , C08G77/52
CPC分类号： H01L33/56 , C08G77/52 , C08L83/04 , C08L83/14 , C08L83/00
摘要： One purpose is to provide a silicone resin composition which provides a cured product having a large Abbe's number and a high brightness. A silicone resin composition including (A-1) an organopolysiloxane having a three-dimensional crosslinked structure, at least two alkenyl groups, and at least one monovalent aromatic hydrocarbon group bonded to a silicon atom, (A-2) a linear organopolysiloxane having alkenyl groups at at least both terminals of a molecular chain and at least one monovalent aromatic hydrocarbon group bonded to a silicon atom, (B-1) a linear organohydrogen polysiloxane having at least one silphenylene skeleton in a molecular chain and hydrosilyl groups at least both terminals of the molecular chain, in an amount such that a ratio of the number of the hydrosilyl groups in component (B-1) to a total number of the alkenyl groups in components (A-1) and (A-2) is 0.5 to 2, and (C) a hydrosilylation catalyst in a catalytic amount.
摘要翻译：一个目的是提供一种提供具有大的阿贝数和高亮度的固化产物的硅树脂组合物。一种有机硅树脂组合物，其包含（A-1）具有三维交联结构的有机聚硅氧烷，至少两个烯基和至少一个与硅原子键合的一价芳香族烃基，（A-2）具有烯基的直链有机聚硅氧烷分子链的至少两个末端和至少一个与硅原子键合的一价芳香族烃基的基团（B-1）在分子链中具有至少一个亚苯基骨架的直链有机氢聚硅氧烷，至少两个末端是氢化甲硅烷基（B-1）中的氢化甲硅烷基数与组分（A-1）和（A-2）中的链烯基的总数的比率为0.5〜 2和（C）催化量的氢化硅烷化催化剂。

4. 发明授权

US09117978B2 Thermosetting silicone resin sheet and method for producing the same, and light-emitting apparatus using the thermosetting silicone resin sheet and method for producing the same 有权
标题翻译：热固性硅树脂片及其制造方法以及使用该热固性硅树脂片的发光装置及其制造方法
公开(公告)号：US09117978B2
公开(公告)日：2015-08-25
申请号：US14058871
申请日：2013-10-21
申请人： SHIN-ETSU CHEMICAL CO., LTD.
发明人： Tsutomu Kashiwagi , Toshio Shiobara
IPC分类号： H01L33/50 , B32B3/10 , B32B3/16 , C08L83/04 , C08K3/22
CPC分类号： H01L33/501 , B32B3/10 , B32B3/16 , C08K2003/221 , C08L83/04 , H01L2924/0002 , H01L2933/0041 , H01L2924/00
摘要： The present invention provides a thermosetting silicone resin sheet having a phosphor-containing thermosetting silicone resin layer formed in the form of an LED device and a method for producing the same, and a light-emitting apparatus using the thermosetting silicone resin sheet and a method for producing the same. The present invention was accomplished by the phosphor-containing thermosetting silicone resin sheet comprising a substrate film and a phosphor-containing thermosetting silicone resin layer that is a plastic solid or a semi-solid at room temperature composed of a single layer having no adhesive layer, formed by printing and molding a phosphor-containing thermosetting silicone resin composition on the substrate film in the form of an LED device.
摘要翻译：本发明提供一种具有以LED器件形式形成的含荧光体的热固性有机硅树脂层及其制造方法的热固性硅树脂片，以及使用该热固性硅树脂片的发光装置及其制造方法生产相同。本发明是通过含有基材膜的含磷光体的热固性有机硅树脂片和在室温下由不含粘合剂层的单层构成的塑料固体或半固体的含荧光体的热固性有机硅树脂层来实现的，通过以LED装置的形式将含荧光体的热固性硅树脂组合物印刷和模塑在基底膜上而形成。

5. 发明授权

US08993794B2 Method for preparing a polyorganosiloxane 有权
标题翻译：聚有机硅氧烷的制备方法
公开(公告)号：US08993794B2
公开(公告)日：2015-03-31
申请号：US14021461
申请日：2013-09-09
申请人： Shin-Etsu Chemical Co., Ltd.
发明人： Takayuki Kusunoki , Tsutomu Kashiwagi
IPC分类号： C07F7/18 , C08G77/08
CPC分类号： C07F7/188 , C08G77/08
摘要： A method for preparing a polyorganosiloxane, wherein the method includes a step of subjecting at least one organic silicon compound having at least one —OX group bonding to a silicon atom in the molecule, wherein X is a hydrogen atom, an alkyl group having 1 to 10 carbon atoms or an alkoxyalkyl group having 2 to 10 carbon atoms, to a condensation reaction in the presence of a catalyst, wherein the catalyst is one obtained by surface treating at least one selected from the group consisting of hydroxides of elements in Group II of the periodic table, hydrates of hydroxides of elements in Group II of the periodic table and oxides of elements in Group II of the periodic table with a silane coupling agent.
摘要翻译：一种制备聚有机硅氧烷的方法，其中该方法包括使至少一种具有至少一个-OX基的有机硅化合物与分子中的硅原子键合的步骤，其中X是氢原子，具有1〜 10个碳原子或具有2至10个碳原子的烷氧基烷基，在催化剂存在下进行缩合反应，其中所述催化剂是通过表面处理从第II族中的元素的氢氧化物中选出的至少一种周期表，元素周期表II族元素氢氧化物的水合物和周期表第II族元素的氧化物与硅烷偶联剂。

6. 发明授权

US08809480B2 Silicone resin composition, luminous substance-containing wavelength-converting film, and cured product thereof 有权
标题翻译：硅树脂组合物，含发光物质的波长转换膜及其固化物
公开(公告)号：US08809480B2
公开(公告)日：2014-08-19
申请号：US13734515
申请日：2013-01-04
申请人： Shin-Etsu Chemical Co., Ltd.
发明人： Takayuki Kusunoki , Toshio Shiobara , Tsutomu Kashiwagi
IPC分类号： C08G77/20 , C08L83/04 , C08G77/04 , C08G77/12
CPC分类号： C08G77/04 , C08G77/12 , C08G77/20 , C08L83/04 , H01L2224/73204
摘要： There is disclosed a silicone resin composition includes (A-1) a ladder structure-containing polyorganosiloxane having a ladder structure and having two or more alkenyl groups in one molecule, (B-1) a ladder structure-containing hydrogen polyorganosiloxane having a ladder structure and having hydrogen atoms that are bonded to two or more silicon atoms in one molecule, and/or (B-2) a hydrogen polyorganosiloxane having two or more hydrogen atoms that are bonded to silicon atoms in one molecule. As a result, there is provided the silicone resin composition as a light-emitting device protective material having a high transparency, heat resistance, light resistance and gas barrier.
摘要翻译：公开了一种有机硅树脂组合物，其包含（A-1）具有梯形结构且在一个分子中具有两个或更多个烯基的含梯度结构的聚有机硅氧烷，（B-1）具有梯形结构的含梯度结构的氢聚有机硅氧烷并且具有与一个分子中的两个或更多个硅原子键合的氢原子和/或（B-2）具有在一个分子中与硅原子键合的具有两个或更多个氢原子的氢聚有机硅氧烷。结果，提供了具有高透明度，耐热性，耐光性和阻气性的发光装置保护材料的有机硅树脂组合物。

7. 发明授权

US09963542B2 Silicone-modified epoxy resin, composition containing the epoxy resin, and cured product of same 有权
公开(公告)号：US09963542B2
公开(公告)日：2018-05-08
申请号：US15300645
申请日：2015-03-25
申请人： Shin-Etsu Chemical Co., Ltd. , Nippon Kayaku Kabushiki Kaisha
发明人： Toshio Shiobara , Junichi Sawada , Miyuki Wakao , Tsutomu Kashiwagi , Naofusa Miyagawa , Yoshihiro Kawada , Chie Sasaki , Naosuke Taniguchi
IPC分类号： C08G59/38 , C08G59/32 , C08G59/42
CPC分类号： C08G59/3281 , C08G59/20 , C08G59/38 , C08G59/4238 , C08G59/4269 , C08G59/4284
摘要： A silicone-modified epoxy resin which yields a cured product having low gas permeability and excellent strength; a composition of the silicone-modified epoxy resin; and an epoxy resin cured product obtainable by curing the composition, are provided.An epoxy resin represented by the following Formula (1): wherein R1 represents a hydrocarbon group having 1 to 6 carbon atoms; X represents an organic group having a norbornane epoxy structure, or a hydrocarbon group having 1 to 6 carbon atoms; n represents an integer from 1 to 3; plural R1s and plural Xs present in the formula may be respectively identical or different; and two or more of plural Xs represent an organic group having a norbornane epoxy structure.

8. 发明授权

US09944760B2 Silicone-modified epoxy resin, composition containing said epoxy resin, and cured product thereof 有权
公开(公告)号：US09944760B2
公开(公告)日：2018-04-17
申请号：US15120482
申请日：2015-02-18
申请人： Shin-Etsu Chemical Co., Ltd. , Nippon Kayaku Kabushiki Kaisha
发明人： Toshio Shiobara , Junichi Sawada , Miyuki Wakao , Tsutomu Kashiwagi , Naofusa Miyagawa , Yoshihiro Kawada , Chie Sasaki , Naosuke Taniguchi
IPC分类号： C08G77/50 , C08G77/14 , C08G77/38 , C08G59/34 , C08G59/40 , C08G59/02 , C08G59/30 , C08G59/32 , C09J183/14 , C08G59/42 , C08G59/68 , C08G77/20
CPC分类号： C08G77/50 , C08G59/027 , C08G59/306 , C08G59/3281 , C08G59/34 , C08G59/40 , C08G59/4215 , C08G59/4276 , C08G59/4284 , C08G59/50 , C08G59/688 , C08G77/14 , C08G77/20 , C08G77/38 , C09J183/14 , C08K5/11 , C08K5/12 , C08K5/17
摘要： The purpose of the present invention is to provide a silicone-modified epoxy resin which produces a cured product having excellent low gas permeability and strength; a composition of the resin; and an epoxy resin cured product obtainable by curing the composition.Disclosed is an epoxy resin represented by the following Formula (1): wherein R1 independently represents a monovalent aromatic hydrocarbon group having 6 to 12 carbon atoms; R2 independently represents a monovalent aliphatic hydrocarbon group having 1 to 12 carbon atoms; R3 independently represents a monovalent aliphatic hydrocarbon group having 1 to 12 carbon atoms or a monovalent aromatic hydrocarbon group having 6 to 12 carbon atoms; R4 represents an oxygen atom or a divalent hydrocarbon group having an aliphatic cyclic structure; R5 represents silicone chain having a norbornane epoxy structure at either end; and X represents an organic group having a norbornane epoxy group.

9. 发明授权

US09751901B2 Method for preparing a polyorganosiloxane and a polyorganosiloxane 有权
公开(公告)号：US09751901B2
公开(公告)日：2017-09-05
申请号：US15376830
申请日：2016-12-13
申请人： SHIN-ETSU CHEMICAL CO., LTD.
发明人： Takayuki Kusunoki , Tsutomu Kashiwagi
IPC分类号： C08G77/12 , C07F7/18 , C08G77/04
CPC分类号： C07F7/1804 , C07F7/025 , C07F7/188 , C08G77/045 , C08G77/12 , C08G77/80
摘要： A polyorganosiloxane resin represented by the following general formula (5): (R3SiO1/2)1′(R2SiO2/2)m′(RSiO3/2)n′(SiO4/2)o′ (5) wherein R is, independently of each other, a hydrogen atom or a monovalent hydrocarbon group having 1 to 18 carbon atoms, and optionally having an oxygen, halogen, nitrogen or sulfur atom; l′, m′ and o′ are, independently of each other, an integer of from 0 to 10,000; n′ is an integer of from 1 to 10,000; a total of l′, m′ and n′ is from 2 to 30,000; and at least one R is a hydrogen atom and at least one R is an —OX group in the molecule, wherein X is an alkyl group having 1 to 10 carbon atoms or an alkoxyalkyl group having 2 to 10 carbon atoms; and at least one hydrogen atom and at least one —OX group bond to one and the same silicon atom.

10. 发明授权

US09340649B2 Method for preparing a polyorganosiloxane and a polyorganosiloxane 有权
标题翻译：聚有机硅氧烷和聚有机硅氧烷的制备方法
公开(公告)号：US09340649B2
公开(公告)日：2016-05-17
申请号：US14790549
申请日：2015-07-02
申请人： SHIN-ETSU CHEMICAL CO., LTD.
发明人： Takayuki Kusunoki , Tsutomu Kashiwagi
IPC分类号： C07F7/18 , C08G77/04
CPC分类号： C07F7/1804 , C07F7/025 , C07F7/188 , C08G77/045 , C08G77/12 , C08G77/80
摘要： A polyorganosiloxane resin represented by the following general formula (5): (R3SiO1/2)l′(R2SiO2/2)m′(RSiO3/2)n′(SiO4/2)o′ (5) wherein R is, independently of each other, a hydrogen atom or a monovalent hydrocarbon group having 1 to 18 carbon atoms, and optionally having an oxygen, halogen, nitrogen or sulfur atom; l′, m′ and o′ are, independently of each other, an integer of from 0 to 10,000; n′ is an integer of from 1 to 10,000; a total of l′, m′ and n′ is from 2 to 30,000; and at least one R is a hydrogen atom and at least one R is an —OX group in the molecule, wherein X is an alkyl group having 1 to 10 carbon atoms or an alkoxyalkyl group having 2 to 10 carbon atoms; and at least one hydrogen atom and at least one —OX group bond to one and the same silicon atom.
摘要翻译：由以下通式（5）表示的聚有机硅氧烷树脂：（R3SiO1 / 2）1'（R2SiO2 / 2）m'（RSiO3 / 2）n'（SiO4 / 2）o'（5）氢原子或具有1至18个碳原子的一价烃基，并且任选地具有氧，卤素，氮或硫原子; 1'，m'和o'彼此独立地为0至10,000的整数; n'为1〜10000的整数; 共有1'，m'和n'为2至30,000; 并且至少一个R是氢原子，并且至少一个R是分子中的-OX基团，其中X是具有1至10个碳原子的烷基或具有2至10个碳原子的烷氧基烷基; 和至少一个氢原子和至少一个-OX基团与一个和相同的硅原子键合。

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