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1. 发明申请

US20180245223A1 ELECTROCHEMICAL, CHLORINATION, AND OXYCHLORINATION SYSTEMS AND METHODS TO FORM PROPYLENE OXIDE OR ETHYLENE OXIDE 审中-公开
公开(公告)号：US20180245223A1
公开(公告)日：2018-08-30
申请号：US15963637
申请日：2018-04-26
申请人： Calera Corporation
发明人： Kyle Self , Michael Joseph Weiss , Ryan J Gilliam , Thomas Albrecht , Gal Mariansky
IPC分类号： C25B3/06 , C07D301/24 , C07D303/04 , C07C29/64 , C07C31/36
CPC分类号： C25B3/06 , C07C17/08 , C07C29/64 , C07C31/36 , C07D301/24 , C07D303/04 , C07C19/01 , C07C19/045
摘要： Disclosed herein are methods and systems that relate to various configurations of electrochemical oxidation, chlorine oxidation, oxychlorination, chlorination, and epoxidation reactions to form propylene oxide or ethylene oxide.

2. 发明授权

US10000432B2 Processes for the synthesis of chiral 1-alkanols 有权
公开(公告)号：US10000432B2
公开(公告)日：2018-06-19
申请号：US15111449
申请日：2015-01-09
申请人： PURDUE RESEARCH FOUNDATION
发明人： Ei-ichi Negishi
IPC分类号： C12P17/06 , C07C29/50 , C07C29/44 , C07F5/06 , C07C67/03 , C07C29/62 , C07C67/317 , C07C67/343 , C07C69/734 , C07C41/26 , C07C51/295 , C07C29/09 , C07C29/10 , C07D319/06 , C12P7/62
CPC分类号： C07C29/50 , C07B2200/05 , C07B2200/07 , C07C29/095 , C07C29/10 , C07C29/44 , C07C29/62 , C07C41/26 , C07C51/295 , C07C67/03 , C07C67/317 , C07C67/343 , C07C69/734 , C07C2601/14 , C07D319/06 , C07F5/06 , C12P7/62 , C07C31/125 , C07C31/12 , C07C69/14 , C07C53/128 , C07C33/18 , C07C69/732 , C07C31/1355 , C07C43/13 , C07C31/36
摘要： The invention relates to highly enantioselective processes for the synthesis of chiral 1-alkanols via Zr-catalyzed asymmetric carboalumination of alkenes.

3. 发明授权

US09744391B2 Use of metal-accumulating plants for implementing chemical reactions 有权
公开(公告)号：US09744391B2
公开(公告)日：2017-08-29
申请号：US14831987
申请日：2015-08-21
申请人： CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE , UNIVERSITE MONTPELLIER 2 SCIENCES ET TECHNIQUES
发明人： Claude Grison , Jose Escarre
IPC分类号： C07C321/00 , A62D3/35 , B01J23/06 , B01J23/72 , B01J23/755 , C07C29/62 , C07C2/86 , C07C17/16 , C07C41/30 , C07C45/00 , C07C67/02 , C07C67/347 , C07C209/32 , C07D239/22 , C07F1/08 , A62D101/04
CPC分类号： A62D3/35 , A62D2101/04 , B01J23/06 , B01J23/72 , B01J23/755 , C07C2/861 , C07C17/16 , C07C29/62 , C07C41/30 , C07C45/00 , C07C67/02 , C07C67/347 , C07C209/32 , C07C2523/04 , C07C2527/122 , C07C2527/128 , C07C2527/138 , C07D239/22 , C07F1/08 , C07C31/36
摘要： A method of implementing organic synthesis reactions uses a composition containing a metal catalyst originating from a calcined plant. The plants can be from the Brassicaceae, Sapotaceae and Convolvulaceae family, and the metal catalyst contains metal in the M(II) form such as zinc, nickel, manganese, lead, cadmium, calcium, magnesium or copper. Examples of the organic synthesis reactions include halogenations, electrophilic reactions, cycloadditions, transesterification reactions and coupling reactions, among others.

4. 发明申请

US20170174593A1 PROCESS FOR PREPARING DICHLOROPROPANOL 有权
公开(公告)号：US20170174593A1
公开(公告)日：2017-06-22
申请号：US15263727
申请日：2016-09-13
申请人： CHANG CHUN PLASTICS CO., LTD.
发明人： Chien-Fu Huang , Cheng-Hui Chan
IPC分类号： C07C29/62 , C07C29/80
CPC分类号： C07C29/62 , C07C29/80 , C07C29/86 , C07C31/42 , C07C31/36
摘要： Provided is a process of preparing dichloropropanol, DCP. The process includes the step of: subjecting a three-carbon material to a first chlorination reaction with an aqueous hydrochloric acid solution in the presence of a carboxylic acid catalyst; adding the three-carbon material into the first mixture solution to undergo a second chlorination reaction and obtain a second mixture solution containing less than 13 wt % of hydrochloric acid; distilling the second mixture solution; and purifying the overhead product by oil-water separation to obtain DCP from the oil phase. By lowering the concentration of the hydrochloric acid contained in the mixture to be distilled, the DCP product can be straightly obtained via distillation and oil-water separation, thereby effectively simplifying the process of preparing DCP.

5. 发明申请

US20170166679A1 POLYURETHANE MATERIALS FORMED FROM UNSATURATED PLANT OILS VIA AN ALKYNE ZIPPER REACTION 有权
公开(公告)号：US20170166679A1
公开(公告)日：2017-06-15
申请号：US14965263
申请日：2015-12-10
申请人： International Business Machines Corporation
发明人： Scott B. King , Brandon M. Kobilka , Joseph Kuczynski , Jason T. Wertz
IPC分类号： C08G18/32 , C08G18/72 , G10K11/162 , C07C29/147
CPC分类号： C08G18/3206 , C07C29/14 , C07C29/143 , C07C29/147 , C07C29/56 , C07C29/58 , C07C29/62 , C07C45/26 , C08G18/72 , C08G2101/00 , C08G2350/00 , G10K11/162 , C07C33/025 , C07C33/02 , C07C31/36 , C07C33/042 , C07C33/04 , C07C47/19 , C07C49/185 , C07C31/20 , C07C31/22 , C07C31/24
摘要： A process of forming a polyurethane material includes forming an unsaturated alcohol from an unsaturated plant oil via a reduction reaction. The process includes forming an alkyne-terminated alcohol from the unsaturated alcohol and forming a polyol having two primary hydroxyl groups from the alkyne-terminated alcohol. The process further includes polymerizing a mixture that includes the polyol having the two primary hydroxyl groups to form a polyurethane material.

6. 发明申请

US20160347905A1 PRODUCTION METHOD FOR CARBONATE COMPOUND AND METHACRYLATE OR ESTER THEREOF 有权
标题翻译：碳酸酯化合物和甲基丙烯酸酯或其酯的生产方法
公开(公告)号：US20160347905A1
公开(公告)日：2016-12-01
申请号：US15233981
申请日：2016-08-11
申请人： Asahi Glass Company, Limited
发明人： Takashi OKAZOE , Masayuki MIYAZAKI , Kazuya OHARU , Tomoyuki FUJITA , Shinji WADA , Koichi MURATA , Naoko SHIROTA
IPC分类号： C08G64/30 , C07C68/00 , C07C17/361 , C08G64/06 , C07C29/38 , C07C67/317 , C07C51/377 , C07C51/16 , C07C45/63 , C07C68/06
CPC分类号： C08G64/307 , C07C17/361 , C07C29/38 , C07C45/63 , C07C49/16 , C07C51/16 , C07C51/377 , C07C57/04 , C07C67/00 , C07C67/14 , C07C67/317 , C07C68/00 , C07C68/06 , C08G64/00 , C08G64/06 , C07C69/96 , C07C31/36 , C07C69/63 , C07C69/54
摘要： The present invention relates to a method for producing a carbonate compound and methacrylic acid or an ester thereof, containing a step (a1) of obtaining hexachloroacetone and hydrogen chloride from acetone and chlorine molecule, a step (a2) of obtaining a dialkyl carbonate and chloroform from hexachloroacetone and an alkyl alcohol, a step (b1) of obtaining 1,1,1-trichloro-2-methyl-2-propanol from chloroform and acetone, a step (b2+b3 or b4) of obtaining methacrylic acid or an ester thereof and hydrogen chloride from 1,1,1-trichloro-2-methyl-2-propanol and water or an alcohol, and a step (c1 or c2) of obtaining chlorine molecule by reacting hydrogen chloride with oxygen molecule.
摘要翻译：本发明涉及含有从丙酮和氯分子得到六氯丙酮和氯化氢的步骤（a1）的碳酸酯化合物和甲基丙烯酸或其酯的制备方法，获得碳酸二烷基酯和氯仿的步骤（a2）由六氯丙酮和烷基醇制备由氯仿和丙酮获得1,1,1-三氯-2-甲基-2-丙醇的步骤（b1），获得甲基丙烯酸或酯的步骤（b2 + b3或b4）和来自1,1,1-三氯-2-甲基-2-丙醇和水或醇的氯化氢，以及通过使氯化氢与氧分子反应获得氯分子的步骤（c1或c2）。

7. 发明授权

US09315433B2 Method for producing 2,7-octadien-1-OL 有权
标题翻译： 2,7-辛二烯-1-OL的制备方法
公开(公告)号：US09315433B2
公开(公告)日：2016-04-19
申请号：US14778798
申请日：2014-03-26
申请人： KURARAY CO., LTD.
发明人： Tatsuya Yoshikawa , Tomoaki Tsuji
IPC分类号： C07C29/46 , C07C29/36 , C07C29/86 , C07C33/02 , C07C31/36
CPC分类号： C07C29/46 , C07C29/36 , C07C29/86 , C07C31/36 , C07C33/02
摘要： Provided is a simple and industrially advantageous method for producing 2,7-octadien-1-ol, in which an expensive palladium catalyst is recovered in high efficiency and the reaction rate per atom of palladium is enhanced. Specifically, provided is a method for producing 2,7-octadien-1-ol by subjecting butadiene and water to a telomerization in the presence of a palladium catalyst containing a water-soluble triarylphosphine having two or more sulfonate groups in the molecule and a palladium compound, a tertiary amine, and carbon dioxide, including a step of mixing the telomerization solution obtained by the telomerization with an organic solvent having a dielectric constant at 25° C. of 2 to 18, followed by carrying out phase separation in the presence of carbon dioxide, thereby obtaining 2,7-octadien-1-ol from an organic phase while recovering an aqueous phase including the palladium catalyst. By this production method, the selectivity for 2,7-octadien-1-ol is enhanced.
摘要翻译：提供了一种简单且工业上有利的生产2,7-辛二烯-1-醇的方法，其中以高效率回收昂贵的钯催化剂，并且每个钯原子的反应速率增强。具体地说，提供了在含有分子中具有2个以上磺酸酯基的水溶性三芳基膦的钯催化剂的存在下，使丁二烯和水进行调聚，得到2,7-辛二烯-1-醇的方法，化合物，叔胺和二氧化碳，包括将通过调聚获得的调聚溶液与介电常数在25℃下的有机溶剂混合2至18的步骤，然后在存在下进行相分离从而从有机相中获得2,7-辛二烯-1-醇，同时回收包括钯催化剂的水相。通过该制备方法，增强了对2,7-辛二烯-1-醇的选择性。

8. 发明授权

US09180384B2 Apparatus and process for using olefin as an azeotropic entrainer for isolating 1,3-DICHLORO-2-propanol from a 2,2′-oxybis (1-chloropropane) waste stream 有权
标题翻译：使用烯烃作为共沸夹带剂从2,2'-氧双（1-氯丙烷）废物流中分离1,3-二氯-2-丙醇的装置和方法
公开(公告)号：US09180384B2
公开(公告)日：2015-11-10
申请号：US13990356
申请日：2011-12-07
申请人： Mahesh Ratnakar Sawant , Edward D. Daugs , Mark R. Smit
发明人： Mahesh Ratnakar Sawant , Edward D. Daugs , Mark R. Smit
IPC分类号： C07C29/80 , C07C29/86 , C07C29/74 , C07C29/78 , B01D3/36 , C07C29/82
CPC分类号： B01D3/36 , C07C29/74 , C07C29/78 , C07C29/80 , C07C29/82 , C07C29/86 , C07C31/36
摘要： Disclosed are a process and an apparatus for using an olefin as an azeotropic entrainer to isolate a target organic compound from a waste stream. The olefin may be, for example, 1-decene, 1-dodecene, or 1-tetradecene. The target organic compound may be 1,3-dichloro-2-propanol in waste stream comprising a 2,2′-oxybis(1-chloropropane).
摘要翻译：公开了一种使用烯烃作为共沸夹带剂从废物流中分离目标有机化合物的方法和装置。烯烃可以是例如1-癸烯，1-十二碳烯或1-十四碳烯。目标有机化合物可以是包含2,2'-氧双（1-氯丙烷）的废物流中的1,3-二氯-2-丙醇。

9. 发明申请

US20150243899A1 Fluorene Compound, Light-Emitting Element, Light-Emitting Device, Electronic Device, Lighting Device, and Organic Compound 有权
标题翻译：芴化合物，发光元件，发光装置，电子装置，照明装置和有机化合物
公开(公告)号：US20150243899A1
公开(公告)日：2015-08-27
申请号：US14668239
申请日：2015-03-25
申请人： Semiconductor Energy Laboratory Co., Ltd.
发明人： Harue Osaka , Takako Takasu , Hiromi Nowatari , Satoko Shitagaki , Nobuharu Ohsawa , Satoshi Seo , Kyoko Takeda , Sachiko Kawakami , Tsunenori Suzuki
IPC分类号： H01L51/00 , C07C31/36 , C07C49/163 , C07D333/76 , C07D307/91
CPC分类号： H01L51/0058 , C07C25/02 , C07C25/22 , C07C31/36 , C07C33/46 , C07C33/50 , C07C49/163 , C07C49/333 , C07C49/80 , C07C2603/18 , C07C2603/24 , C07C2603/50 , C07D307/91 , C07D333/76 , C07D409/10 , C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1088 , C09K2211/1092 , H01L51/0052 , H01L51/0054 , H01L51/006 , H01L51/0072 , H01L51/0073 , H01L51/0074 , H01L51/0081 , H01L51/0085 , H01L51/5004 , H01L51/5016 , H01L51/5056 , H01L51/508 , H01L51/5088 , H01L51/5092 , H01L51/5206 , H01L51/5221 , H01L2251/301 , H01L2251/308 , H01L2251/552 , H05B33/10 , Y10S428/917
摘要： A substance having a hole-transport property and a wide band gap is provided. A fluorene compound represented by a general formula (G1) is provided. In the general formula (G1), α1 and α2 separately represent a substituted or unsubstituted arylene group having 6 to 13 carbon atoms; Ar1 represents a substituted or unsubstituted aryl group having 6 to 18 carbon atoms, a substituted or unsubstituted 4-dibenzothiophenyl group, or a substituted or unsubstituted 4-dibenzofuranyl group; n and k separately represent 0 or 1; Q1 represents sulfur or oxygen; and R1 to R15 separately represent hydrogen, an alkyl group having 1 to 12 carbon atoms, or an aryl group having 6 to 14 carbon atoms.
摘要翻译：提供具有空穴传输性和宽带隙的物质。提供由通式（G1）表示的芴化合物。在通式（G1）中，α1和α2分别表示取代或未取代的碳原子数为6〜13的亚芳基。 Ar1表示取代或未取代的碳原子数为6〜18的芳基，取代或未取代的4-二苯并噻吩基或取代或未取代的4-二苯并呋喃基; n和k分别表示0或1; Q1表示硫或氧; R1〜R15分别表示氢，碳原子数1〜12的烷基或碳原子数6〜14的芳基。

10. 发明授权

US08969630B2 Method for preparing chlorohydrins and method for preparing epichlorohydrin using chlorohydrins prepared thereby 有权
标题翻译：氯氢化物的制备方法和由此制备的氯代醇制备表氯醇的方法
公开(公告)号：US08969630B2
公开(公告)日：2015-03-03
申请号：US13805750
申请日：2011-06-08
申请人： Won Seob Song , Sung Yul Woo , Boo Weon Song , Seong Han Park , Myoung Suk Kwon
发明人： Won Seob Song , Sung Yul Woo , Boo Weon Song , Seong Han Park , Myoung Suk Kwon
IPC分类号： C07C31/34 , C07D301/02 , C07C29/62 , C07D303/08
CPC分类号： C07C29/62 , C07D303/08 , C07C31/36
摘要： A method of preparing chlorohydrins and a method of preparing epichlorohydrin by using chlorohydrins prepared using the method are provided. The method of preparing chlorohydrins by reacting polyhydroxy aliphatic hydrocarbon with a chlorination agent in the presence of a catalyst includes at least one combination of a series of unit operations including a first reaction step, a water removal step, and a second reaction step, in that respective order, wherein the method further includes purifying chlorohydrins from a reaction mixture discharged from a final reaction step of the plurality of reaction steps. The method of preparing epichlorohydrin includes reacting chlorohydrins prepared using the method of preparing chlorohydrins, with an alkaline agent.
摘要翻译：提供了一种制备氯代醇的方法和一种使用该方法制备的使用氯代醇制备表氯醇的方法。通过在催化剂存在下使多羟基脂族烃与氯化剂反应制备氯代醇的方法包括一系列单元操作的组合，包括第一反应步骤，除水步骤和第二反应步骤，其中其中所述方法还包括从多个反应步骤的最终反应步骤排出的反应混合物中纯化氯代醇。制备表氯醇的方法包括使用制备氯代醇的方法制备的氯代醇与碱性试剂反应。

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