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1. 发明授权

US4906702A Esters of unsaturated carboxylic acids, preparation of their oil-soluble homo- and copolymers and use thereof as pour point depressants 失效
标题翻译：不饱和羧酸的酯，它们的油溶性均聚物和共聚物的制备以及作为倾点下降剂的用途
公开(公告)号：US4906702A
公开(公告)日：1990-03-06
申请号：US187183
申请日：1988-04-28
申请人： Wolfgang Ritter , Wolfgang Zoellner
发明人： Wolfgang Ritter , Wolfgang Zoellner
IPC分类号： C07C69/527 , C08F20/28 , C10L1/196 , C10L1/198 , C10L1/236
CPC分类号： C10L1/1963 , C08F20/28 , C10L1/1983 , C10L1/2364
摘要： Polymeric pour point depressants are described which are prepared from new esters of .alpha.,.beta.-olefinically unsaturated carboxylic acids of the formulaR.sub.1 --CO--[--O--A--CO--]--.sub.n ORwhereinR.sub.1 --CO-- is an .alpha.,.beta.-olefinically unsaturated carboxylic acid residue containing from 3 to 6 carbon atoms,R is a saturated or unsaturated hydrocarbon radical containing from 10 to 24 carbon atoms,--[--O--A--CO--]-- is a residue of a hydroxycarboxylic acid having from 2 to 6 carbon atoms,A is an aliphatic radical having from 1 to 5 carbon atoms, andn is a number having a value of from 1 to 18.

2. 发明授权

US4567291A 2-Methyl-2-buten-1-yl tiglate 失效
标题翻译： 2-甲基-2-丁烯-1-基tiglate
公开(公告)号：US4567291A
公开(公告)日：1986-01-28
申请号：US560353
申请日：1983-12-12
申请人： Dietmar Lamparsky , Roman Kaiser
发明人： Dietmar Lamparsky , Roman Kaiser
IPC分类号： C07C69/533 , A23L27/20 , A61K8/37 , A61Q13/00 , C07C69/527 , C11B9/00
CPC分类号： C11B9/0019
摘要： The invention is concerned with a novel odorant and/or flavoring substance, namely, 2-methyl-2-buten-1-yl tiglate of the formula ##STR1## The invention is also concerned with a process for the manufacture of the compound of formula I, the compound of formula I as an odorant and/or flavoring substance and odorant and/or flavoring compositions containing the compounds of formula I.
摘要翻译：本发明涉及一种新颖的加味剂和/或调味物质，即式I的2-甲基-2-丁烯-1-基tiglate。本发明还涉及制备化合物的方法式I的化合物，作为气味剂和/或调味物质的式I化合物和含有式I化合物的加味剂和/或调味组合物。

3. 发明授权

US4533723A Semi-esters of polyisobutylenesuccinic acid, their synthesis and preparations containing these compounds which can be transformed by radiation into an adhesive 失效
标题翻译：聚异丁烯基琥珀酸的半酯，它们的合成和含有这些化合物的制剂，其可通过辐射转化成粘合剂
公开(公告)号：US4533723A
公开(公告)日：1985-08-06
申请号：US625712
申请日：1984-06-28
申请人： Christian Weitemeyer
发明人： Christian Weitemeyer
IPC分类号： C07C69/527 , C08F2/48 , C08F8/14 , C09J4/00 , C08G63/52
CPC分类号： C08F8/14 , C09J4/00 , C08F2810/20 , C08F2810/30
摘要： Semi-esters of polyisobutylenesuccinic acid having the formula ##STR1## in which R.sup.1 is a polyisobutylene radical with a molecular weight of 100 to 20,000,R.sup.2 andR.sup.3 are different from one another and one of these two radicals is a hydrogen radical and the other one of the groups ##STR2## in which R.sup.4, R.sup.5 is a hydrogen or methyl radical, andR.sup.6 is a methyl or ethyl radical.The invention furthermore relates to processes for synthesizing these compounds as well as to preparations which can be converted by radiation into adhesives.
摘要翻译：具有式Ⅰ的聚异丁烯琥珀酸的半酯，其中R1是分子量为100〜20,000的聚异丁烯基，R2和R3彼此不同，这两个基团中的一个是氢基，另一个是氢基团其中R4，R5为氢或甲基的基团，R6为甲基或乙基。本发明还涉及合成这些化合物的方法以及可通过辐射转化成粘合剂的制剂。

4. 发明授权

US4347176A Compounds and methods of making same 失效
标题翻译：化合物及其制备方法
公开(公告)号：US4347176A
公开(公告)日：1982-08-31
申请号：US140157
申请日：1980-04-14
申请人： Nariman B. Mehta
发明人： Nariman B. Mehta
IPC分类号： A61K31/135 , A61K31/165 , A61K31/195 , A61K31/22 , A61K47/48 , A61K51/04 , C07C45/00 , C07C45/54 , C07C45/56 , C07C67/00 , C07C225/16 , C07C231/00 , C07C235/08 , C07C239/00 , C07C251/58 , C07D263/04 , C07D263/10 , C07K19/00 , C07G7/00 , C07C69/527 , C07C101/30 , G01N33/54
CPC分类号： C07D263/10 , A61K47/4833 , A61K51/0406 , C07C255/00 , C07C45/00 , C07C45/54 , C07C45/56 , C07D263/04 , Y10S436/804 , Y10S436/822 , Y10S530/806
摘要： A radioimmunoassay procedure has been discovered for bupropion [(.+-.)-2-t-butylamino-3-chloropropiophenone], an antidepressant compound, in biological fluids. Novel compounds of formula ##STR1## wherein either R.sub.2 is oxygen and R.sub.1 is (CH.sub.2).sub.n --0--(CO).sub.m --(CH.sub.2).sub.p --COOH where n is an integer from 0 to 5, m is 0 or 1, and p is an integer from 1 to 4; or R.sub.1 is hydrogen and R.sub.2 is N--0--(CH.sub.2).sub.q --COOH where q is an integer from 1 to 3, and novel methods of making them and novel intermediates useful therein are disclosed. Novel immunogens for raising bupropion specific antisera, and novel methods of making them are disclosed comprising conjugates of the novel compounds and suitable carrier material. The drug is added to the antisera together with novel radiolabeled competitor of formula ##STR2## wherein R' is a suitable radioisotope as described above and R.sub.3 is hydrogen, R.sub.4 is Cl, and R.sub.5 is oxygen, orR' is hydrogen and either(a) R.sub.3 is H and R.sub.4 is Cl and R.sub.5 is NO(CH.sub.2).sub.q CO--X where q is as defined for formula I and X is a group having formula III ##STR3## wherein R.sub.6 is a suitable radioisotope as described above, R.sub.7 is hydroxyl, and s is an integer from 1 to 4;(b) R.sub.4 is Cl, R.sub.5 is oxygen, and R.sub.3 is (CH.sub.2).sub.n --0--(CO).sub.m --(CH.sub.2).sub.p --CO--X where n, m, and p are as defined for formula I and X is as defined above; or(c) R.sub.3 is hydroxy, R.sub.5 is oxygen and R.sub.4 is a suitable radioisotope as defined above.The measure of radioactivity of the antisera bound radiolabeled competitor provides a measure of the amount of drug in the assayed biological fluid sample. A standard curve can be constructed from which the amount of drug in the assay sample can be interpolated. A kit is disclosed for practicing the radioimmunoassay.
摘要翻译：已经发现了用于生物液体中的安非他酮[（+/-） - 2-叔丁基氨基-3-氯苯丙酮]（一种抗抑郁药）的放射免疫测定方法。新的式（IMAGE）化合物，其中R2是氧，R1是（CH2）n-O-（CO）m-（CH2）p-COOH，其中n是0-5的整数，m是0或1， p是1至4的整数; 或R1是氢，R2是N-O-（CH2）q-COOH，其中q是1至3的整数，并且公开了制备它们的新方法和可用于其中的新的中间体。公开了用于提高安非他酮特异性抗血清的新型免疫原及其制备方法，其包括新化合物和合适的载体材料的缀合物。将药物与新的放射性标记的式（IMAGE）竞争剂一起加入到抗血清中，其中R'是如上所述的合适的放射性同位素，R 3是氢，R 4是Cl，R 5是氧，或者R'是氢，）R3是H，R4是Cl，R5是NO（CH2）qCO-X，其中q如式I所定义，X是具有式III的基团，其中R6是如上所述的合适的放射性同位素，R7是羟基，s为1至4的整数; （b）R4是Cl，R5是氧，R3是（CH2）n-O-（CO）m-（CH2）p-CO-X，其中n，m和p如式I所定义，X是如上所述; 或（c）R3是羟基，R5是氧，R4是如上定义的合适的放射性同位素。抗血清结合的放射性标记的竞争者的放射性测量值提供测定的生物流体样品中药物的量的量度。可以构建标准曲线，由此可以插入测定样品中的药物量。公开了用于实施放射免疫测定的试剂盒。

5. 发明授权

US4167513A Synthesis of unsaturated esters and lactone from butadiene and carbon dioxide 失效
标题翻译：从丁二烯和二氧化碳合成不饱和酯和内酯
公开(公告)号：US4167513A
公开(公告)日：1979-09-11
申请号：US939793
申请日：1978-09-05
申请人： Alfredo Musco , Roberto Santi , Gian P. Chiusoli
发明人： Alfredo Musco , Roberto Santi , Gian P. Chiusoli
IPC分类号： C07C69/587 , B01J31/00 , C07B61/00 , C07C29/09 , C07C29/149 , C07C51/00 , C07C51/09 , C07C51/15 , C07C57/03 , C07C67/00 , C07C69/527 , C07D309/32 , C07D315/00 , C07D309/30 , C07C69/61
CPC分类号： C07D315/00 , C07C29/095 , C07C29/149 , C07C51/09
摘要： Octadienyl esters of 2-ethylidene-hepta-3,5-dienoic and 2-vinyl-hepta-3,5-dienoic acids of formula C.sub.8 H.sub.11 COOC.sub.8 H.sub.13 and .delta.-lactone of formula ##STR1## or 2-ethylidene-hepta-6-ene-5-olide, are prepared by reaction of 1,3-butadiene with CO.sub.2 at a temperature comprised between about 20.degree. and 150.degree. C. and at a total pressure between about 10 and 500 atm in the presence of a phosphinic complex of palladium having the formula Pd[P(R).sub.3 ].sub.x, wherein x is an integer from 2 to 4, and (R).sub.3 is a homogeneous or heterogeneous group consisting of alkyls, cycloalkyls having up to 8 carbon atoms and of phenyls, also substituted, in an inert atmosphere.The obtained products are "per se" new and are valuable intermediates for synthesis of chemicals (fungicides, pesticides, etc.) and in particular as effective plasticizers.
摘要翻译：式C 8 H 11 COOC 8 H 13的2-亚乙基 - 庚-3,5-二烯酸和2-乙烯基 - 庚-3,5-二烯酸的辛二烯基酯和式（II）的δ-内酯或2-亚乙基 - 七烯-5-醇通过1,3-二丁烯与CO 2在约20-150℃的温度下反应并在约10-500atm的总压下在次膦酸盐络合物具有式Pd [P（R）3] x的钯，其中x是2至4的整数，（R）3是由烷基，具有至多8个碳原子的环烷基和苯基组成的均相或异质基团也在惰性气氛中取代。

6. 发明授权

US4028387A (1-Methyl-2-vinyl)4,6-heptadienyl-3,8-nonadienoate and a method of manufacturing the same 失效
标题翻译：（1-甲基-2-乙烯基）4,6-庚二烯基-3,8-壬二烯酸酯及其制造方法
公开(公告)号：US4028387A
公开(公告)日：1977-06-07
申请号：US612082
申请日：1975-09-10
申请人： Satoru Enomoto , Hitoshi Takita , Hisayuki Wada , Yutaka Mukaida , Mikiro Yanaka
发明人： Satoru Enomoto , Hitoshi Takita , Hisayuki Wada , Yutaka Mukaida , Mikiro Yanaka
IPC分类号： C07C69/527 , C08F36/22 , C11C3/02 , C07C69/52
CPC分类号： C08F36/22
摘要： Reaction of (1-methyl-2-vinyl)4,6-heptadiene-1-ol with butadiene and carbon monoxide in the presence of a catalyst comprising palladium compounds and phosphine compounds provides a novel substance of (1-methyl-2-vinyl)4,6-heptadienyl-3,8-nonadienoate. This product can be made into a polymer at temperatures of 100.degree. to 250.degree. C.
摘要翻译：（1-甲基-2-乙烯基）4,6-庚二烯-1-醇与丁二烯和一氧化碳在包含钯化合物和膦化合物的催化剂存在下的反应提供了（1-甲基-2-乙烯基）4,6-庚二烯基-3,8-壬二烯酸酯。该产品可以在100-250℃的温度下制成聚合物。

7. 发明授权

US3961051A Juvenile hormones stabilized with acrylonitrile U.V. absorbers 失效
标题翻译：用丙烯腈紫外线稳定的少年激素吸收体
公开(公告)号：US3961051A
公开(公告)日：1976-06-01
申请号：US508015
申请日：1974-09-20
申请人： Alexander Emodi
发明人： Alexander Emodi
IPC分类号： A01N25/22 , C07C69/527 , C07D303/22 , C07D303/32 , C07D303/42 , C07D317/64 , C07D333/12 , C07D333/38 , A01N9/28
CPC分类号： C07D333/38 , A01N25/22 , C07D303/22 , C07D303/32 , C07D303/42 , C07D317/64 , C07D333/12 , Y10S424/12 , Y10S514/972
摘要： A method of stabilizing juvenile hormones against deterioration from air and sunlight by combining the juvenile hormones with substituted acrylonitrile or substituted benzotriazole ultraviolet light absorbers and/or with substituted phenolic anti-oxidants, and the resulting stabilized, insecticide compositions.
摘要翻译：通过将少年激素与取代的丙烯腈或取代的苯并三唑紫外光吸收剂和/或与取代的酚类抗氧化剂组合，以及所得稳定的杀虫剂组合物，将少年激素稳定化以防止空气和阳光下的变质。

8. 发明授权

US3867415A Propenyl and propynyl esters of chloro substituted 2-octenoic and 2-nonenoic acids 失效
标题翻译：氯取代的2-辛烯和2-壬烯酸的丙烯基和丙炔基酯
公开(公告)号：US3867415A
公开(公告)日：1975-02-18
申请号：US23503072
申请日：1972-03-15
申请人： HOFFMANN LA ROCHE
发明人： CHODNEKAR MADHUKAR SUBRAYA , PFIFFNER ALBERT , RIGASSI NORBERT , SCHWIETER ULRICH , SUCHY MILOS
IPC分类号： C07C29/147 , C07C51/363 , C07C57/52 , C07C69/527 , C07C69/62 , A01N9/24
CPC分类号： C07C57/52 , C07B2200/09 , C07C29/147 , C07C51/363 , C07C33/423
摘要： Propenyl and propynyl esters of chloro and dichloro substituted, 2-octenoic, 2-nonenoic, 2-dodecenoic and 2-tridecenoic acids and propenyl and propynyl ethers of chloro and dichloro substituted, 2-octenyl, 2-nonenyl, 2-dodecenyl and 2-tridecenyl alcohols, and insecticide compositions that include at least one of the propenyl or propynyl esters or ethers and that can also include a conventional insect-poison.
摘要翻译：氯和二氯取代的2-辛烯，2-壬烯，2-十二碳烯酸和2-十三碳烯酸的丙烯基和丙炔基酯和氯代和二氯取代的2-辛烯基，2-壬烯基，2-十二碳烯基和2 - 十二碳烯基的丙烯基和丙炔基醚 - 十三碳烯醇，以及包含至少一种丙烯基或丙炔基酯或醚的杀虫剂组合物，并且还可以包括常规昆虫毒素。

9. 发明授权

US3796746A Unsaturated ester of halogenated alkenes 失效
公开(公告)号：US3796746A
公开(公告)日：1974-03-12
申请号：US3796746D
申请日：1971-11-15
申请人： ALELIO G D
发明人： D ALELIO G
IPC分类号： B27K3/15 , C07C69/527 , C08F20/22 , C08F20/40 , D06M14/00 , C07C69/54
CPC分类号： D06M14/00 , B27K3/15 , B27K2240/30 , C08F20/22 , C08F20/40 , C08K5/02 , C08L61/06 , C08L97/02
摘要： THIS INVENTION DEALS WITH NEW UNSATURATED ESTERS OF A,B-UNSATURATED CARBOXYLIC ACIDS DERIVED FROM HALOGENATED ALCOHOLS OF THE FORMULAS

HO-R-C(-X)=C(-X)-R'' AND HO-R-C(-X)2-C(-X)2-R''

WHEREIN R IS A DIVALENT HYDROCARBON MOIETY HAVING AT LEAST ONE AND NO MORE THAN 10 CARBON ATOMS, X IS A MEMBER SELECTED FROM THE CLASS OF OF BROMINE AND CHLORINE, AND R'' IS A MEMBER SELECTED FROM THE CLASS OF HYDROGEN, X AND A MOLOVALENT HYDROCARBON CONTAINING AT LEAST ONE AND NO MORE THAN 20 CARBON ATOMS. TYPICAL ESTERS ARE THE ACRYLATES, METHACRYLATES, MALEATES, FURMARATES, ITACONATES AND CINNAMATES. THE MONOMERS POSSESS FIRERETARDANT PROPERTIES AND ARE USEFUL FOR THE SYNTHESIS OF POLYMERS AND COPOLYMERS.

10. 发明授权

US3671577A Process for producing 1, 4-diacyloxy-2-butene 失效
标题翻译：生产1,4-二氨基-2-丁烯的方法
公开(公告)号：US3671577A
公开(公告)日：1972-06-20
申请号：US3671577D
申请日：1970-03-13
申请人： TOYO SODA MFG CO LTD
发明人： ONO ISAO , FUKABORI KENTARO , SHIMOMURA SEIICHI
IPC分类号： C07C69/025 , B01J23/00 , B01J27/00 , B01J31/00 , C07B61/00 , C07C69/16 , C07C69/527 , C07C67/04
CPC分类号： C07C67/055 , C07C69/16 , C07C69/28 , C07C69/593 , C07C69/08
摘要： 1,4-DIACYLOXY-2-BUTENE IS PRODUCED BY PASSING A GASEOUS MIXTURE OF BUTADIENE, AN ALIPHATIC MONOCARBOXYLIC ACID AND AN OXYGENCONTAINING GAS OVER A CATALYST COMPRISING AT LEAST ONE OF PALLADIUM, IRIDIUM, PLATINUM, RHODIUM AND RUTHENIUM AND CARBOXYLATE AND INORGANIC ACID SALT THEREOF.
摘要翻译： 1,4-二氧化二-2-丁烯是通过引入丁二烯的气体混合物，二氧化硅单羧酸和含氧气体，通过包含至少一种钯，铱，铂，铑和钌以及羧酸和无机物的催化剂生产的其酸盐。

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