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    • 3. 发明申请
    • Chemical powder deposition method for the manufacture of optical fiber preforms and optical fibers
    • 用于制造光纤预制棒和光纤的化学粉末沉积方法
    • US20040226319A1
    • 2004-11-18
    • US10440208
    • 2003-05-15
    • John Burnette MacChesneyThomas Edward StockertPatrick William WiskMan Fei Yan
    • C03B037/016
    • C03C13/00C03B37/0128C03C25/00
    • The specification describes the production of optical fibers and optical fiber preforms using Chemical Powder Deposition (CPD). In this process a slurry of silica powders and dopant powders in a liquid carrier is prepared and the inside surface of a silica glass starter tube is coated with the slurry, then dried. The coating is then consolidated and the tube collapsed as in the conventional MCVD process. Multiple coatings, and coatings with varying compositions, can be used to produce any desired profile. In an alternative embodiment, doped silica glass of the desired final composition is prepared, and then pulverized to form the powder for the slurry. In both embodiments, the use of powders of known composition in the slurry allows direct control over the final glass composition, as compared with conventional processes in which the composition in the final glass is indirectly controlled by control of the thermodynamics of a vapor phase reaction.
    • 该规范描述了使用化学粉末沉积(CPD)制造光纤和光纤预制棒。 在该方法中,制备液体载体中的二氧化硅粉末和掺杂剂粉末的浆料,并且将石膏玻璃起始管的内表面涂覆有浆料,然后干燥。 然后将涂层固化,并且管如同传统的MCVD工艺那样折叠。 可以使用具有不同组成的多个涂层和涂层来产生任何所需的轮廓。 在替代实施方案中,制备所需最终组合物的掺杂二氧化硅玻璃,然后粉碎以形成用于浆料的粉末。 在两个实施方案中,与其中通过控制气相反应的热力学间接控制最终玻璃中的组成的常规方法相比,在浆料中使用已知组合物的粉末允许直接控制最终的玻璃组合物。
    • 4. 发明授权
    • Method of making an optical fiber using preform dehydration in an environment of chlorine-containing gas, fluorine-containing gases and carbon monoxide
    • 在含氯气体,含氟气体和一氧化碳的环境中制备使用预成型脱水的光纤的方法
    • US06776012B2
    • 2004-08-17
    • US09891903
    • 2001-06-26
    • Kai H ChangDavid KalishThomas John Miller
    • Kai H ChangDavid KalishThomas John Miller
    • C03B37027
    • C03C25/607C03B37/0142C03B37/01446C03B2207/36C03B2207/38C03C13/047C03C25/00G02B6/02G02B6/4492Y02P40/57
    • Embodiments of the invention include a method for making optical fiber having reduced aging or hydrogen aging loss over the life of the fiber and optical fiber systems including such optical fibers. The method includes the steps of dehydrating an optical fiber glass core rod in a first environment including oxygen and at least one of chlorine-containing gases, fluorine-containing gases and carbon monoxide; and adjusting the oxygen stoichiometry of the first environment so that it is neither oxygen-rich nor oxygen-deficient. Improved silicon-oxygen stoichiometry during one or more preform manufacturing steps reduces the amount of Si defects generated in the optical fiber preform. Also, deuterium exposure of optical fiber drawn from the preform reduces the likelihood of having atomic defects such as Si defects in the optical fiber that, over time, attract and bond with hydrogen atoms to form molecules that contribute to increased water absorption loss. The inventive method produces optical fibers with improved transmission characteristics, e.g., optical fibers made by methods according to embodiments of the invention have transmission loss at 1385 nanometers that is less than 0.33 dB/km and the aging loss increase thereafter is less than 0.04 dB/km.
    • 本发明的实施例包括一种制造光纤的寿命中具有降低的老化或氢老化损耗的方法以及包括这种光纤的光纤系统。 该方法包括在包括氧和含氯气体,含氟气体和一氧化碳中的至少一种的第一环境中使光纤玻璃芯棒脱水的步骤; 并调节第一环境的氧化学计量,使其既不富氧也不氧缺乏。 在一个或多个预成型件制造步骤期间改进的硅 - 氧化学计量减少了在光纤预制件中产生的Si缺陷的量。 此外,从预成型件汲取的光纤的氘暴露减少了具有诸如光纤中的Si缺陷的原子缺陷的可能性,随着时间的推移,它们吸引并与氢原子键合形成有助于增加吸水损失的分子。 本发明的方法产生具有改进的传输特性的光纤,例如,通过根据本发明的实施例的方法制造的光纤具有小于0.33dB / km的1385纳米的传输损耗,此后的老化损耗增加小于0.04dB / 公里。
    • 9. 发明授权
    • Absolute fluid filter
    • 绝对流体过滤器
    • US4227899A
    • 1980-10-14
    • US939972
    • 1978-09-06
    • Allan H. MenyDennis L. Palmer
    • Allan H. MenyDennis L. Palmer
    • B01D39/14B01D46/00C03C25/00B01D39/16
    • B01D39/14B01D46/00C03C25/00
    • The novel filter, according to an embodiment thereof, comprises a filter matrix formed into a specific geometry and made of glass, metal, mineral and/or cellulostic fibers, or fibers or fiber-agglomerates molded from thermoplastic, thermoset plastic, elastoplasts, or related synthetic polymer materials, which have been coated, impregnated, or compounded, prior to forming, with a series of substances in order that the filter may be easily cleaned and reused, as well as protected against corrosive action by the fluid media, or to render substances in the filtration fluid media chemically unreactive, or to change the chemical state or structure of matter in the fluid media. The coating compounds, filler compounds, or impregnants, depending upon which thereof are employed, change the physical properties of the filter matrix and alters impaction-retention of filtered particles, and/or alters the electrostatic attraction of the matrix for matter in the fluid media, and/or imparts corrosion protection to the filter matrix, and/or renders matter in the fluid media chemically unreactive by changing its reactivity characteristics or chemical structure upon contact with the matrix.
    • 根据其实施例​​,该新型过滤器包括形成为特定几何形状并由玻璃,金属,矿物和/或纤维素纤维制成的过滤器基体,或由热塑性塑料,热塑性塑料,弹性体或相关材料模制的纤维或纤维聚集体 合成聚合物材料已经在形成之前用一系列物质进行了涂覆,浸渍或复合,以使得过滤器可以容易地被清洁和重复使用,并且防止流体介质的腐蚀作用,或者使得 过滤介质中的物质化学反应不良,或改变流体介质中物质的化学状态或结构。 取决于其使用的涂料化合物,填料化合物或浸渍剂改变过滤基质的物理性质并改变过滤颗粒的冲击保留,和/或改变基质在流体介质中的物质的静电吸引 ,和/或向过滤器基质施加腐蚀保护,和/或通过在与基体接触时改变其反应特性或化学结构,使流体介质中的物质在化学上不起作用。