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1. 发明授权

US09969690B2 Cure accelerators for anaerobic curable compositions 有权
公开(公告)号：US09969690B2
公开(公告)日：2018-05-15
申请号：US15452768
申请日：2017-03-08
申请人： Henkel IP & Holding GmbH
发明人： Philip T. Klemarczyk
IPC分类号： C08F2/00 , C08F20/06 , C08F118/02 , C07D215/06 , C08F20/28 , C08K5/3437 , C07D209/08 , C08K5/3417 , C07C255/25 , C08K5/315 , C07C253/30 , C07C229/18 , C08K5/18 , C07C227/26
CPC分类号： C07D215/06 , C07C211/48 , C07C227/26 , C07C229/18 , C07C253/30 , C07C255/25 , C07D209/08 , C08F20/28 , C08F220/28 , C08K5/16 , C08K5/18 , C08K5/315 , C08K5/3417 , C08K5/3437 , C09J4/00
摘要： Cure accelerators for anaerobic curable compositions, such as adhesives and sealants, are provided, and which are defined with reference to the compounds shown in structure I where A is CH2 or benzyl, R is C1-10 alkyl, R′ is H or C1-10 alkyl, or R and R′ taken together may form a four to seven membered ring fused to the benzene ring, R″ is optional, but when R″ is present, R″ is halogen, alkyl, alkenyl, cycloalkyl, hydroxyalkyl, hydroxyalkenyl, alkoxy, amino, alkylene- or alkenylene-ether, alkylene (meth)acrylate, carbonyl, carboxyl, nitroso, sulfonate, hydroxyl or haloalkyl, and EWG is as shown, an electron withdrawing group, such as nitro, nitrile, carboxylate or trihaloalkyl.

2. 发明授权

US09873659B2 Solutions of trialkali metal salts of MGDA with an excess of L-enantiomer, their manufacture and use 有权
公开(公告)号：US09873659B2
公开(公告)日：2018-01-23
申请号：US15516589
申请日：2015-10-07
申请人： BASF SE
发明人： Marta Reinoso Garcia , Constanze Franzke , Armin Stamm
IPC分类号： C11D3/33 , C07C227/42 , C07C229/24 , C07C229/16 , C07C227/26 , C11D3/20 , C11D3/04 , C11D3/10
CPC分类号： C07C229/16 , C07C227/26 , C11D3/044 , C11D3/046 , C11D3/10 , C11D3/2079 , C11D3/2082 , C11D3/33
摘要： Aqueous solution containing in the range of from 60.5 to 75% by weight of a mixture of trialkalimetal salts of the L-and D-enantiomers of methyl glycine diacetic acid (MGDA), said mixture containing predominantly the respective L-isomer with an enantiomeric excess (ee) in the range of from 3 to 97%, wherein said trialkali metal salts have the general formula (I) [CH3—CH(COO)—N(CH2—COO)2]K3−xNax (I) wherein x is in the range of from zero to 2.9.

3. 发明申请

US20140323684A1 AMINO ACID PREPARATION METHOD COMPRISING A STEP OF HYDROFORMYLATION OF AN UNSATURATED FATTY NITRILE 审中-公开
标题翻译：含有不饱和脂肪酸的水解步骤的氨基酸制备方法
公开(公告)号：US20140323684A1
公开(公告)日：2014-10-30
申请号：US14362309
申请日：2012-12-03
申请人： ARKEMA FRANCE , CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE , UNIVERSITE DE RENNES 1
发明人： Jean-Luc Dubois , Jean-Luc Couturier , Jean-François Carpentier , Jérémy Ternel
IPC分类号： C08G69/08 , C07C227/26
CPC分类号： C08G69/08 , C07C227/04 , C07C227/26 , C07C253/22 , C07C253/30 , C07C229/08 , C07C255/19 , C07C255/17 , C07C255/07
摘要： A method for synthesizing a ω-amino acid compound having formula HOOC—R′—CH2NH2, where R is an alkyl radical including between 6 and 15 carbon atoms or an alkylene radical including between 6 and 15 carbon atoms and between 0 and 2 unsaturations. The method including the following steps: 1) hydroformylation of an unsaturated fatty nitrile selected from compounds having formula R1—CH═CH—[(CH2)q—CH═CH]m—(CH2)r—CN, said step consisting in reacting the nitrile with the carbon monoxide and dihydrogen such as to obtain at least one fatty nitrile aldehyde having formula HOC—R′—CN; 2) dioxygen oxidation, wherein the nitrile aldehyde obtained in step 1) is converted into fatty nitrile acid having formula HOOC—R′—CN; and 3) reduction, in which the nitrile acid obtained in step 2) is converted into co-amino acid having formula HOOC—R′—CH2NH2.
摘要翻译：一种合成具有式HOOC-R'-CH2NH2的ω-氨基酸化合物的方法，其中R是包含6至15个碳原子的烷基或包含6至15个碳原子的亚烷基和0至2个不饱和度。该方法包括以下步骤：1）选自具有式R1-CH = [ - （CH2）q-CH = CH-（CH2）r-CN的化合物的不饱和脂肪腈的羰基化，所述步骤包括具有一氧化碳和二氢的腈，以获得至少一种具有式HOC-R'-CN的脂肪腈醛; 2）二氧氧化，其中将步骤1）中得到的腈醛转化为具有式HOOC-R'-CN的脂肪腈酸; 和3）还原，其中将步骤2）中获得的腈酸转化为具有式HOOC-R'-CH2NH2的共氨基酸。

4. 发明授权

US07956195B2 Process for the preparation and isolation of the individual stereoisomers of 1-amino, 3-substituted phenylcyclopentane-carboxylates 有权
标题翻译：用于制备和分离1-氨基，3-取代的苯基环戊烷羧酸酯的单个立体异构体的方法
公开(公告)号：US07956195B2
公开(公告)日：2011-06-07
申请号：US12004582
申请日：2007-12-21
申请人： Thomas D. Gordon , Grier A. Wallace , Martin E. Hayes , Kirill A. Lukin , Lei Wang , Dilinie P. Fernando
发明人： Thomas D. Gordon , Grier A. Wallace , Martin E. Hayes , Kirill A. Lukin , Lei Wang , Dilinie P. Fernando
IPC分类号： C07D487/00 , C07D233/72 , C07D235/02 , C07C229/48
CPC分类号： C07D235/02 , C07B2200/07 , C07C45/69 , C07C227/18 , C07C227/24 , C07C227/26 , C07C227/34 , C07C253/00 , C07C253/34 , C07C2601/08 , C07C49/697 , C07C49/753 , C07C229/48 , C07C255/46
摘要： The present invention discloses processes for the preparation and isolation of the individual stereoisomers of 1-amino, 3-substituted phenylcyclopentane-carboxylates.
摘要翻译：本发明公开了1-氨基，3-取代的苯基环戊烷羧酸酯的各种立体异构体的制备和分离方法。

5. 发明授权

US06627772B2 Preparation of N-[2-(carboxymethoxy) ethyl]-N-(carboxymethyl) glycine 有权
标题翻译： N- [2-（羧基甲氧基）乙基] -N-（羧甲基）甘氨酸的制备
公开(公告)号：US06627772B2
公开(公告)日：2003-09-30
申请号：US10081200
申请日：2002-02-22
申请人： Phillip S. Athey , David A. Wilson
发明人： Phillip S. Athey , David A. Wilson
IPC分类号： C07C22922
CPC分类号： C07C255/25 , C07C227/26 , C07C229/12
摘要： Compounds represented by the formula wherein R and R1 independently represent H, —CH2CN or —CH2CO2X, with the proviso that R and R1 can not be both H or —CH2CO2X; and X represents hydrogen, an alkali metal or alkaline earth metal are disclosed. These compounds are useful as intermediate compounds in the preparation of N-[2-(carboxymethoxy)ethyl]-N-(carboxy-methyl)glycine. These intermediates can be formed by contacting 3-morpholinone with glycolonitrile under alkaline conditions to form an aminonitrile which can be hydrolyzed and contacted with additional glycolonitrile to form the nitrile intermediate which can be converted to N-[2-(carboxymethoxy)ethyl]-N-(carboxymethyl)glycine via hydrolysis.
摘要翻译：由式R和R 1表示的化合物独立地表示H，-CH 2 CN或-CH 2 CO 2 X，条件是R和R 1不能同时为H或-CH 2 CO 2 X; X表示氢，碱金属或碱土金属。这些化合物可用作制备N- [2-（羧基甲氧基）乙基] -N-（羧基 - 甲基）甘氨酸的中间体化合物。这些中间体可以通过在碱性条件下使3-吗啉酮与乙醇腈接触形成氨基腈，其可以水解并与另外的乙醇腈接触以形成腈中间体，其可以转化为N- [2-（羧基甲氧基）乙基] -N - （羧甲基）甘氨酸通过水解。

6. 发明授权

US5258550A Process for preparing glycine 失效
标题翻译：制备甘氨酸的方法
公开(公告)号：US5258550A
公开(公告)日：1993-11-02
申请号：US720825
申请日：1991-07-08
申请人： Kenji Fujiwara , Nobutaka Ueda , Yuuji Matsuu , Hiroshi Kato , Atsuhiko Hiai
发明人： Kenji Fujiwara , Nobutaka Ueda , Yuuji Matsuu , Hiroshi Kato , Atsuhiko Hiai
IPC分类号： C07C227/12 , C07C227/26 , C07C229/00
CPC分类号： C07C227/26 , C07C227/12
摘要： This invention relate to a process for producing glycine by reacting glycolonitrile, carbon dioxide and ammonia in the presence of water, comprising subjecting first water, glycolonitrile, carbon dioxide and ammonia to a pre-reaction at 80.degree.-120.degree. C. for 0.5-1 hour and then to the main reaction at 150.degree.-200.degree. C. and a process further comprising recycling the remaining mother liquor having separated the glycine from the reaction solution obtained by the above process to the system comprising water, glycolonitrile, carbon dioxide and ammonia to carry out the aforesaid pre-reaction and/or main reaction.
摘要翻译： PCT No.PCT / JP90 / 01576 Sec。 371日期：1991年7月8日 102（e）日期1991年7月8日PCT 1990年12月5日PCT PCT。出版物WO91 / 08194 日本6月13日，1991年。本发明涉及在水存在下使乙醇腈，二氧化碳和氨反应生产甘氨酸的方法，包括使第一水，乙醇腈，二氧化碳和氨在80℃下进行预反应， 120℃下进行0.5-1小时，然后在150-200℃进行主反应，并且进一步包括将从上述方法获得的反应溶液中分离出甘氨酸的剩余母液循环到包含水，乙醇腈，二氧化碳和氨，以进行上述预反应和/或主反应。

7. 发明授权

US4677224A Continuous process for synthesizing an .alpha.-amino acid by chemical catalytic hydrolysis 失效
标题翻译：通过化学催化水解合成α-氨基酸的连续方法
公开(公告)号：US4677224A
公开(公告)日：1987-06-30
申请号：US740803
申请日：1985-06-03
申请人： Auguste Commeyras , Jacques Taillades , Jean Brugidou , Louis Mion , Regine Sola , Robert Pascal , Monique Lasperas , Alain Rousset
发明人： Auguste Commeyras , Jacques Taillades , Jean Brugidou , Louis Mion , Regine Sola , Robert Pascal , Monique Lasperas , Alain Rousset
IPC分类号： C07B61/00 , B01J31/00 , B01J31/06 , C07C67/00 , C07C227/00 , C07C227/20 , C07C227/26 , C07C227/28 , C07C229/02 , C07C229/08 , C07C313/00 , C07C319/20 , C07C323/58 , C07C99/10
CPC分类号： C07C227/26
摘要： The device for carrying out the continuous process for synthesizing an .alpha.-amino acid incorporates: (a) a vessel (10) for feeding .alpha.-amino-nitrile, or one of its salts; (b) a connecting pipe (12), in which a pump (14) is mounted, connecting the feed vessel (10) to (c) a catalysis column (16) containing a carbonyl-containing polymeric resin (18) which is insoluble in basic aqueous medium; (d) a connecting pipe (20) from the catalysis column (16) to (e) a hydrolysis reactor (22), acting simultaneously as a reservoir for the .alpha.-amino acid salt formed, and equipped with (f) means for feeding hydroxide ions, comprising a feed vessel (24), a pipe (26) and a pump (28); and (g) a pipe (30) for drawing off the .alpha.-amino acid salt formed.
摘要翻译：用于进行用于合成α-氨基酸的连续方法的装置包括：（a）用于供给α-氨基腈或其盐之一的容器（10）（b）其中安装有泵（14）的连接管（12），其将进料容器（10）连接到（c）含有含羰基的聚合物树脂（18）的催化塔（16），其不溶于在碱性水介质中; （d）从催化塔（16）到（e）水解反应器（22）的连接管（20），同时作为形成的α-氨基酸盐的储存器，并配备有（f）进料装置氢氧根离子，包括进料容器（24），管道（26）和泵（28）; 和（g）用于抽出形成的α-氨基酸盐的管道（30）。

8. 发明申请

US20100222610A1 GLUTAMIC ACID N,N-DIACETIC AMIDE, GLUTAMIC ACID N-ACETIC AMIDE N-ACETONITRILE, ALKALI METAL SALTS THEREOF, PROCESS TO PREPARE THEM AND THEIR USE 有权
标题翻译：谷氨酸N，N-二酰胺，谷氨酸N-乙酰胺N-乙酸酯，其碱金属盐，其制备方法及其用途
公开(公告)号：US20100222610A1
公开(公告)日：2010-09-02
申请号：US12673683
申请日：2008-08-14
申请人： Tjerk Oedse Boonstra , Martin Heus , Axel Carstens , Jim Lepage
发明人： Tjerk Oedse Boonstra , Martin Heus , Axel Carstens , Jim Lepage
IPC分类号： C07C231/06
CPC分类号： C11D3/33 , C07C227/26 , C07C229/24 , C07C237/06 , C07C255/25 , C09K8/86 , C11D7/3245 , D21C9/10
摘要： The present invention relates to glutamic acid N,N-diacetic amide, potassium or sodium glutamate N,N-diacetic amide, glutamic acid N-acetic amide N-acetonithle, potassium or sodium glutamate N-acetic amide N-acetonitrile, to processes to prepare such compounds and the use thereof.
摘要翻译：本发明涉及谷氨酸N，N-二乙酰胺，谷氨酸钾或谷氨酸钠N，N-二乙酸酰胺，谷氨酸N-乙酰胺N-乙腈，谷氨酸钾或谷氨酸N-乙酰胺N-乙腈，以处理制备这些化合物及其用途。

9. 发明授权

US06916761B1 Polymer-supported Lewis acid catalyst 失效
标题翻译：聚合物负载的路易斯酸催化剂
公开(公告)号：US06916761B1
公开(公告)日：2005-07-12
申请号：US09889406
申请日：2000-10-23
申请人： Shu Kobayashi
发明人： Shu Kobayashi
IPC分类号： C07D263/10 , B01J23/10 , B01J31/06 , B01J31/10 , B01J31/12 , B01J31/14 , B01J31/16 , B01J31/22 , B01J31/26 , B01J31/34 , B01J31/36 , B01J31/38 , B01J31/40 , C07B37/00 , C07B37/02 , C07B61/00 , C07C29/40 , C07C33/025 , C07C33/30 , C07C45/64 , C07C45/72 , C07C49/835 , C07C67/31 , C07C69/732 , C07C253/00 , C07C255/42 , C07C327/22 , B01J23/83 , B01J27/02 , B01J27/053 , C08F4/02
CPC分类号： B01J31/10 , B01J31/0227 , B01J31/1658 , B01J31/2226 , B01J31/4015 , B01J2231/326 , B01J2231/342 , B01J2231/343 , B01J2231/44 , B01J2531/35 , B01J2531/37 , B01J2531/38 , C07B37/02 , C07B2200/07 , C07C29/38 , C07C67/343 , C07C227/26 , C07C253/00 , C07C253/08 , C07C327/22 , C07C2601/14 , C07D263/38 , Y02P20/584 , C07C69/732 , C07C255/42 , C07C33/14 , C07C33/30
摘要： In order to provide a novel Lewis acid catalyst, which shows high reaction activity in aqueous medium, is easily recovered, and is excellent in reusability, a Lewis acid group expressed by the general formula (I): MXn (I) (wherein M represents a polyvalent element, X represents an anionic group, and n is an integer representing the valence of M) is linked and supported on a polymer membrane via an SO3 or SO4 group.
摘要翻译：为了提供在水性介质中显示高反应活性的新颖的路易斯酸催化剂，易于回收，并且具有优异的可重复使用性，由通式（I）表示的路易斯酸基团：<？在线配方说明书 =“在线公式”end =“lead”？> MX （I）<？in-line-formula description =“In-line Formulas”end =“tail”？>（其中 M表示多价元素，X表示阴离子基团，n表示M价数的整数）通过SO 3或SO 4连接并负载在聚合物膜上， SUB>组。

10. 发明授权

US6008176A Use of glycine-N, N-diacetic acid derivatives as biodegradable complexing agents for alkaline earth metal ions and heavy metal ions 失效
标题翻译：甘氨酸-N，N-二乙酸衍生物作为碱土金属离子和重金属离子的可生物降解络合剂
公开(公告)号：US6008176A
公开(公告)日：1999-12-28
申请号：US73244
申请日：1998-05-06
申请人： Juergen Schneider , Birgit Potthoff-Karl , Alexander Kud , Richard Baur , Alfred Oftring , Thomas Greindl
发明人： Juergen Schneider , Birgit Potthoff-Karl , Alexander Kud , Richard Baur , Alfred Oftring , Thomas Greindl
IPC分类号： C07D307/54 , A23C7/02 , A61K8/44 , A61Q11/00 , C07B61/00 , C07C227/00 , C07C227/02 , C07C227/18 , C07C227/26 , C07C229/16 , C07C229/26 , C07C229/30 , C07C229/34 , C07C229/36 , C07C255/24 , C07C255/25 , C07D207/337 , C07D211/74 , C07D213/55 , C07D263/32 , C07D277/30 , C07D307/24 , C07D333/24 , C11D3/33 , C11D11/00 , C11D17/06 , D06L1/14 , D06L3/02 , D06L3/10 , D06M11/40 , D21C9/10 , D21C9/16 , G03C5/305 , G03C5/38 , G03C5/44 , G03C7/42
CPC分类号： G03C7/42 , A23C7/02 , A61K8/44 , A61Q11/00 , C07C227/18 , C07C227/26 , C07C229/16 , C07C229/26 , C07C255/25 , C11D11/0023 , C11D11/0041 , C11D17/065 , C11D3/33 , D06L3/021 , D06L3/10 , D21C9/1042 , G03C5/3053 , G03C5/38 , G03C5/44 , A61K2800/51
摘要： Glycine-N,N-diacetic acid derivatives and their alkali metal, alkaline earth metal, ammonium and substituted ammonium salts are used as complexing agents for alkaline earth metal and heavy metal ions with the exception of .alpha.-alanine-N,N-diacetic acid as textile detergent builders in powder detergent formulations and as calcium sequestrants in oral hygiene products.
摘要翻译：使用甘氨酸-N，N-二乙酸衍生物及其碱金属，碱土金属，铵和取代的铵盐作为碱土金属和重金属离子的络合剂，除了α-丙氨酸-N，N-二乙酸作为粉末洗涤剂配方中的纺织洗涤剂助洗剂和口腔卫生产品中的钙螯合剂。

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