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41. 发明授权

US5395990A Process for the production of alcohols and diols 失效
标题翻译：制备醇和二醇的方法
公开(公告)号：US5395990A
公开(公告)日：1995-03-07
申请号：US175542
申请日：1993-12-30
申请人： John Scarlett
发明人： John Scarlett
IPC分类号： B01J23/78 , B01J23/80 , B01J23/86 , B01J23/889 , B01J27/224 , C07B61/00 , C07C29/141 , C07C29/145 , C07C29/149 , C07C31/27 , C07C29/147 , C07C27/04 , C07C29/14
CPC分类号： C07C31/276 , C07C29/149 , C07C2101/14
摘要： A process is described for the production of a hydroxylic compound selected from alcohols and diols by hydrogenation of a hydrogenatable material selected from monoesters of carboxylic acids, monoesters of dicarboxylic acids, diesters of dicarboxylic acids, aldehydes, olefinically unsaturated aldehydes, and mixtures of two or more thereof, which process comprises the steps of:(a) providing a hydrogenation zone containing a charge of a granular hydrogenation catalyst which has a total surface area of at least about 15 m.sup.2 /g, a pore size distribution such that more than 50% of the pore volume is provided by pores in the size range less than about 40 nm, and a surface area distribution such that more than 50% of the total surface area is provided by pores in the size range of from about 7 nm to about 40 nm;(b) supplying to the hydrogenation zone a feed stream of a mixture containing hydrogen and the hydrogenatable material;(c) maintaining the hydrogenation zone under temperature and pressure conditions which are conducive to effecting hydrogenation of the hydrogenatable material; and(d) recovering from the hydrogenation zone a product stream comprising the hydroxylic compound.The process is exemplified by the hydrogenation of dimethyl 1,4-cyclohexanedicarboxylate to yield 1,4-cyclohexanedimethanol.
摘要翻译：描述了通过氢化可选择的羧酸单羧酸，二羧酸单酯，二羧酸二酯，醛，烯属不饱和醛的可氢化材料以及两种或两种以上的混合物来制备选自醇和二醇的羟基化合物的方法该方法包括以下步骤：（a）提供含有粒状氢化催化剂装料的氢化区，其具有至少约15m 2 / g的总表面积，孔径分布使得大于50％的孔体积由小于约40nm的尺寸范围的孔提供，并且表面积分布使得总表面积的大于50％由尺寸范围为约7nm至约40的孔提供 nm; （b）向氢化区供应含有氢和可加氢材料的混合物的进料流; （c）在有利于可氢化材料的氢化的温度和压力条件下保持氢化区; 和（d）从氢化区回收包含羟基化合物的产物流。该方法的实例是通过1,4-环己烷二羧酸二甲酯的氢化得到1,4-环己烷二甲醇。

42. 发明授权

US5286878A Catalytic reduction of organic carbonyls 失效
标题翻译：催化还原有机羰基
公开(公告)号：US5286878A
公开(公告)日：1994-02-15
申请号：US616892
申请日：1990-11-21
申请人： Stephen L. Buchwald , Kristina A. Kreutzer , Esther Spaltenstein
发明人： Stephen L. Buchwald , Kristina A. Kreutzer , Esther Spaltenstein
IPC分类号： C07B41/02 , C07B43/04 , C07C29/143 , C07C29/147 , C07C209/52 , C07D207/06 , C07D295/023 , C07D307/52 , C07P207/06 , C07C29/132 , C07C33/22 , C07P207/20
CPC分类号： C07D295/023 , C07B41/02 , C07B43/04 , C07C209/52 , C07C29/143 , C07C29/147 , C07D207/06 , C07D307/52 , C07B2200/07 , C07C2101/14
摘要： A process is provided whereby organic carbonyl substrates, including esters, ketones and amides, are reduced in a reaction with a silane reducing reagent and a catalyst. Effective catalysts broadly include those which consist of a group 4, 5 or 6 metal which either: a) is in less than its maximum oxidation state or is capable of being converted to a complex in less than its maximum oxidation state; and/or is a group 4, 5 or 6 metal hydride. Exemplary catalysts include titanium-containing catalysts such as (bis trimethylphosphine) titanocene, trimethyl phosphine adduct of a (hydrido) silyl complex of titanocene, titanocene dichloride and titanocene monochloride.
摘要翻译：提供了一种方法，其中与硅烷还原剂和催化剂的反应中还原有机羰基底物，包括酯，酮和酰胺。有效的催化剂广泛地包括由4,5或6族金属组成的催化剂，其中：a）小于其最大氧化态，或能够在小于其最大氧化态下转化为络合物; 和/或是4,5或6族金属氢化物。示例性催化剂包括含钛催化剂，例如（双三甲基膦）二茂钛，二茂钛（二氯）二氯化锆和二氯二氯化钛的（氢化）甲硅烷基配合物的三甲基膦加合物。

43. 发明授权

US5059720A Hydroxy containing fluorovinyl compounds and polymers thereof 失效
标题翻译：含羟基的氟化合物及其聚合物
公开(公告)号：US5059720A
公开(公告)日：1991-10-22
申请号：US592172
申请日：1990-10-09
申请人： Ming-Hong Hung
发明人： Ming-Hong Hung
IPC分类号： C08F2/06 , C07C29/147 , C07C41/01 , C07C43/178 , C08F2/04 , C08F16/14 , C08F16/24 , C08F16/26
CPC分类号： C07C43/178 , C07C29/147 , C08F16/24 , C08F16/26
摘要： Novel hydroxy containing fluorovinyl ethers, polymers of hydroxy containing fluorovinyl ethers, copolymers of selected hydroxy containing fluorovinyl ethers, a process for reducing ester containing fluorovinyl compounds to the corresponding alcohol with borohydrides, and a process for polymerizing hydroxy containing fluorovinyl ethers are disclosed.
摘要翻译：公开了含羟基的氟乙烯基醚，含羟基乙烯基醚的羟基聚合物，选择的含羟基乙烯基醚的选择性羟基乙烯基醚的共聚物，将含有氟乙烯基化合物的酯还原为与硼氢化物相应的醇的方法，以及聚合含羟基乙烯基醚的方法。

44. 发明授权

US4968668A Alcohols having 3-methyl or 3,5-dimethyl or 3,5-dimethylphenyl groups, a process for their preparation and a fragrance composition containing same 失效
标题翻译：具有3-甲基或3,5-二甲基或3,5-二甲基苯基的醇，其制备方法和含有它们的香料组合物
公开(公告)号：US4968668A
公开(公告)日：1990-11-06
申请号：US382646
申请日：1989-08-07
申请人： Walter Hafner , Walter Gebauer , Marlies Regiert , Wilhelm Friedrich , Erich Markl
发明人： Walter Hafner , Walter Gebauer , Marlies Regiert , Wilhelm Friedrich , Erich Markl
IPC分类号： A61K8/33 , A61Q13/00 , C07C27/00 , C07C29/14 , C07C29/141 , C07C29/143 , C07C29/147 , C07C29/149 , C07C29/17 , C07C29/36 , C07C29/38 , C07C29/40 , C07C29/58 , C07C29/80 , C07C33/20 , C07C33/46 , C07C67/00 , C11B9/00
CPC分类号： C07C33/20
摘要： 2-Methyl-3-(3-methylphenyl)-propan-1-ol, 2-methyl-3-(3,5-dimethylphenyl)-propan-1-ol, 1-(3-methylphenyl)-2-methylbutan-3-ol and 1-(3,5-dimethylphenyl)-2-methylbutan-3-ol, their preparation and use as fragrances.
摘要翻译： PCT No.PCT / EP88 / 00081 Sec。 371日期1989年8月7日 102（e）日期1989年8月7日PCT提交1988年2月4日PCT公布。出版物WO88 / 05770 日期1988年8月11日2-甲基-3-（3-甲基苯基） - 丙-1-醇，2-甲基-3-（3,5-二甲基苯基） - 丙-1-醇，1-（3-甲基苯基） -2-甲基丁-3-醇和1-（3,5-二甲基苯基）-2-甲基丁-3-醇，它们的制备和用作香料。

45. 发明授权

US4945187A Process for preparing enantiomerically pure propan-1,2-diols 失效
标题翻译：制备对映异构纯的丙-1,2-二醇的方法
公开(公告)号：US4945187A
公开(公告)日：1990-07-31
申请号：US379741
申请日：1989-07-14
申请人： Klaus R. Muller
发明人： Klaus R. Muller
IPC分类号： C07C29/10 , C07C27/00 , C07C29/132 , C07C29/147 , C07C29/56 , C07C31/10 , C07C67/00
CPC分类号： C07C29/147 , C07B2200/07
摘要： The invention relates to a process for preparing enantiomerically pure S(+)-propan-1,2-diol and R(-)-propan-1,2-diol from L(-)-lactide or D(+)-lactide, respectively.
摘要翻译：本发明涉及从L（ - ） - 丙交酯或D（+） - 丙交酯制备对映体纯的S（+） - 丙-1,2-二醇和R（ - ） - 丙-1,2-二醇的方法，分别。

46. 发明授权

US4849401A Alcohols containing 2-methylphenyl or 2-methoxyphenyl groups, and fragrances containing same 失效
标题翻译：含有2-甲基苯基或2-甲氧基苯基的醇和含有它们的香料
公开(公告)号：US4849401A
公开(公告)日：1989-07-18
申请号：US178272
申请日：1988-04-06
申请人： Wilhelm Friedrich , Helmut Gebauer , Walter Hafner , Marlies Regiert
发明人： Wilhelm Friedrich , Helmut Gebauer , Walter Hafner , Marlies Regiert
IPC分类号： A61K8/34 , A61K8/18 , A61Q13/00 , C07C27/00 , C07C29/147 , C07C33/20 , C07C41/00 , C07C43/23 , C07C67/00 , C11B9/00 , C11D3/50 , C11D9/44
CPC分类号： C11B9/0061 , C07C33/20 , C07C43/23
摘要： The invention discloses compounds of the general formula ##STR1## in which R represents a methyl radical or a methoxy radical when R.sup.1 is a hydrogen atom; orR represents a methyl radical when R.sup.1 is a methyl radical.The compounds of the invention are useful as fragrances.
摘要翻译：本发明公开了当R1是氢原子时，其中R代表甲基或甲氧基的通式为“IMAGE”的化合物; 或当R 1为甲基时R表示甲基。本发明的化合物可用作香料。

47. 发明授权

US4820402A Hydrocracking process with improved distillate selectivity with high silica large pore zeolites 失效
标题翻译：加氢裂化工艺，具有改善的馏出物选择性与高二氧化硅大孔沸石
公开(公告)号：US4820402A
公开(公告)日：1989-04-11
申请号：US56341
申请日：1987-05-27
申请人： Randall D. Partridge , Rene B. LaPierre
发明人： Randall D. Partridge , Rene B. LaPierre
IPC分类号： C07C29/147 , C07C45/30 , C07C51/347 , C07D207/34 , C07D209/94 , C07D487/04 , C10G47/02 , C10G47/18 , C10G47/20
CPC分类号： C07D487/04 , C07C255/00 , C07C29/147 , C07C45/305 , C07C51/347 , C07D207/34 , C07D209/94
摘要： A hydrocracking process in which improved selectivity for the production of distillate range (165.degree. C.-343.degree. C.) products is obtained by the use of a catalyst containing a highly siliceous large pore zeolite as the acidic component. Suitable zeolites include zeolites, Y, ZSM-20 and beta with structural silica:alumina ratios of at least 50:1.
摘要翻译：通过使用含有高度硅质的大孔沸石的催化剂作为酸性成分，可获得提高馏出物范围（165℃-73℃）产物的选择性的加氢裂化方法。合适的沸石包括沸石，Y，ZSM-20和β，结构二氧化硅：氧化铝比至少为50:1。

48. 发明授权

US4818747A Bicyclic aliphatic alcohols and their utilization as perfuming ingredients 失效
标题翻译：双环脂族醇及其作为加香成分的利用
公开(公告)号：US4818747A
公开(公告)日：1989-04-04
申请号：US169536
申请日：1988-03-17
申请人： Wolfgang K. Giersch , Gunther Ohloff
发明人： Wolfgang K. Giersch , Gunther Ohloff
IPC分类号： C11D3/50 , B01J23/86 , B01J27/12 , C07B61/00 , C07C27/00 , C07C29/147 , C07C29/149 , C07C31/137 , C07C67/00 , C11B9/00 , C11D9/44 , D06M13/02 , D06M13/144 , D06M23/00 , A61K7/46
CPC分类号： C07C31/137 , C11B9/0053
摘要： Bicyclic aliphatic alcohols or formula ##STR1## wherein substituents CH.sub.2 OH and CH.sub.3 are geminally bound to the carbon atom in position 2 or 3 of the hexanic ring and wherein the wavy line stands for a C-H bond of cis or trans configuration. Use of same as perfuming ingredients.
摘要翻译：双环脂族醇或式（I）其中取代基CH 2 OH和CH 3与己烷环的2或3位的碳原子结合，其中波浪线代表顺式或反式构型的C-H键。使用与加香成分相同。

49. 发明授权

US4746680A Therapeutic agents 失效
标题翻译：治疗剂
公开(公告)号：US4746680A
公开(公告)日：1988-05-24
申请号：US725206
申请日：1985-04-19
申请人： James E. Jeffery , Antonin Kozlik , Eric C. Wilmshurst
发明人： James E. Jeffery , Antonin Kozlik , Eric C. Wilmshurst
IPC分类号： C07D295/06 , A01N33/02 , A61K31/135 , A61K31/16 , A61K31/165 , A61K31/40 , A61K31/435 , A61K31/495 , A61P25/24 , A61P25/26 , C07C29/147 , C07C33/50 , C07C45/00 , C07C45/42 , C07C45/44 , C07C49/237 , C07C49/567 , C07C57/46 , C07C61/40 , C07C67/00 , C07C209/00 , C07C209/28 , C07C209/40 , C07C209/48 , C07C209/52 , C07C209/56 , C07C209/58 , C07C211/25 , C07C211/26 , C07C213/00 , C07C217/74 , C07C231/00 , C07C231/02 , C07C231/08 , C07C231/10 , C07C231/12 , C07C233/03 , C07C233/05 , C07C233/13 , C07C233/18 , C07C313/00 , C07C323/32 , C07D207/06 , C07D211/70 , C07D295/073 , C07D295/185
CPC分类号： C07D295/185 , C07C255/00 , C07C29/147 , C07C33/50 , C07C45/004 , C07C45/42 , C07C45/44 , C07C49/237 , C07C49/567 , C07C57/46 , C07C61/40 , C07D207/06 , C07D211/70 , C07D295/073 , C07C2101/04
摘要： Compounds of formula I ##STR1## in which R.sub.1 is C.sub.1-6 alkyl, C.sub.2-6 alkenyl, C.sub.2-6 alkynyl, C.sub.3-7 cycloalkyl, cycloalkylalkyl or optionally substituted phenyl; R.sub.2 is H or C.sub.1-3 alkyl; R.sub.3 and/or R.sub.4 are H, formyl, C.sub.1-3 alkyl, C.sub.3-6 alkenyl, C.sub.3-6 alkynyl, C.sub.3-7 cycloalkyl or R.sub.3 and R.sub.4 together with the nitrogen atom form a heterocyclic ring system; R.sub.5 and/or R.sub.6 are H, halo, CF.sub.3, C.sub.1-3 alkyl, C.sub.1-3 alkoxy, C.sub.1-3 alkylthio or R.sub.5 and R.sub.6 together with the carbon atoms to which they are attached form a second benzene ring show therapeutic activity in the treatment of depression. Pharmaceutical compositions and processes for preparing compounds of formula I are disclosed.
摘要翻译：式I的化合物其中R 1为C 1-6烷基，C 2-6烯基，C 2-6炔基，C 3-7环烷基，环烷基烷基或任选取代的苯基; R2是H或C1-3烷基; R 3和/或R 4是H，甲酰基，C 1-3烷基，C 3-6烯基，C 3-6炔基，C 3-7环烷基或R 3和R 4与氮原子一起形成杂环体系; R 5和/或R 6是H，卤素，CF 3，C 1-3烷基，C 1-3烷氧基，C 1-3烷硫基或R 5和R 6与它们所连接的碳原子一起形成第二苯环，治疗抑郁症。公开了制备式I化合物的药物组合物和方法。

50. 发明授权

US4720587A Fluoranthene derivatives 失效
标题翻译：荧蒽衍生物
公开(公告)号：US4720587A
公开(公告)日：1988-01-19
申请号：US661674
申请日：1984-10-17
申请人： Kenneth W. Bair
发明人： Kenneth W. Bair
IPC分类号： C07D295/08 , A61K31/045 , A61K31/135 , A61K31/255 , A61K31/275 , A61K31/415 , A61K31/42 , A61K31/535 , A61K31/5375 , A61P31/00 , A61P35/00 , B01J27/135 , C07B61/00 , C07C29/147 , C07C33/46 , C07C63/44 , C07C63/70 , C07C66/02 , C07C67/00 , C07C69/76 , C07C205/15 , C07C213/00 , C07C213/02 , C07C215/06 , C07C215/08 , C07C215/10 , C07C215/20 , C07C215/28 , C07C215/38 , C07C215/42 , C07C215/44 , C07C217/48 , C07C217/58 , C07C253/00 , C07C255/56 , C07C255/58 , C07C313/00 , C07C315/04 , C07C317/32 , C07C317/36 , C07C319/20 , C07C323/32 , C07C323/36 , C07C323/38 , C07D213/02 , C07D233/61 , C07D263/52 , C07D263/62 , C07D263/64 , C07D295/10 , C07D295/12 , C07D295/135 , C07D309/12 , C07D317/32 , C07D319/06 , C07D498/04 , C07D521/00 , C07J63/00 , C07C87/64
CPC分类号： A61K31/045 , C07C205/15 , C07C215/10 , C07C215/28 , C07C215/42 , C07C217/48 , C07C217/58 , C07C255/58 , C07C317/32 , C07C323/32 , C07D231/12 , C07D233/56 , C07D249/08 , C07D263/52 , C07D263/64 , C07D295/135 , C07D309/12 , C07D319/06 , C07J63/008 , C07C2101/14 , C07C2103/24 , C07C2103/26 , C07C2103/40 , C07C2103/42 , C07C2103/48 , C07C2103/50 , Y10S514/908
摘要： The present invention relates to compounds of formula (I)ArCH.sub.2 R.sup.1 (I)or a monomethyl or a monoethyl ether thereof (the compound of formula (I) including these ethers may contain no more than 30 carbon atoms in total); ethers, esters thereof; acid addition salts thereof; wherein Ar is a fluoranthene or substituted fluoranthene ring system; R.sup.1 contains not more than eight carbon carbon atoms and is a group ##STR1## wherein m is 0 or 1;R.sup.5 is hydrogen;R.sup.6 and R.sup.7 are the same or different and each is hydrogen or C.sub.1-3 alkyl optionally substituted by hydroxy;R.sup.8 and R.sup.9 are the same or different and each is hydrogen or C.sub.1-3 alkyl; ##STR2## is a five- or six-membered saturated carbocyclic ring; R.sup.10 is hydrogen, methyl or hydroxymethyl;R.sup.11, R.sup.12 and R.sup.13 are the same or different and each is hydrogen or methyl;R.sup.14 is hydrogen, methyl, hydroxy, or hydroxymethyl.

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