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    • 52. 发明申请
    • Device for the production of crystal rods having a defined cross-section and column-shaped polycrystallization structure by means of floating-zone continuous crystallization
    • 用于通过浮区连续结晶生产具有限定横截面和柱状多结晶结构的晶棒的装置
    • US20050188918A1
    • 2005-09-01
    • US10513320
    • 2003-05-06
    • Nikolai AbrosimovHelge Riemann
    • Nikolai AbrosimovHelge Riemann
    • B22D11/00B22D11/01C01B33/02C30B13/00C30B13/20C30B15/00C30B15/08H01L21/208C30B1/00
    • C30B13/20C30B15/08C30B29/06Y10T117/10Y10T117/1052Y10T117/1056
    • The invention relates to a device for the production of crystal rods having a defined cross-section and a column-shaped polycrystalline structure by means of floating-zone continuous crystallization, comprising at least one crucible filled with crystalline material, provided with a central deviation for transporting the contents of the crucible to a growing crystal rod arranged below the crucible, whereby the central deviation plunges into the melt meniscus, also comprising means for continuously adjustable provision of crystalline material to the crucible, and means for simultaneously feeding the melt energy and adjusting the crystallization front. In order to produce crystal rods having a defined diameter and a column-shaped polycrystalline structure using heating means which are technically less complex, while at the same time guaranteeing high crystallization rates and stable phase definition, the means for simultaneously feeding the melt energy and adjusting the crystallization front on the growing crystal rod (8) is a flat induction coil (5) which has an opening, said induction coil (5) being arranged at a distance from the crucible (4) and/or being vertically moveable in relation to the crystallization front.
    • 本发明涉及一种用于通过浮区连续结晶生产具有限定横截面的晶棒和柱状多晶结构的装置,包括至少一个填充有结晶材料的坩埚,该坩埚具有中心偏差 将坩埚的内容物输送到布置在坩埚下方的生长晶体杆上,由此中心偏离进入熔体弯月面,还包括用于连续调节地向坩埚提供结晶材料的装置,以及用于同时进料熔体能量和调节 结晶前沿。 为了制造具有规定直径的晶棒和使用技术上较不复杂的加热装置的柱状多晶结构,同时保证高结晶速率和稳定的相位定义,同时供给熔体能量并调节 生长晶棒(8)上的结晶前沿是具有开口的平坦感应线圈(5),所述感应线圈(5)布置在与坩埚(4)相距一定距离处和/或可相对于 结晶前沿。
    • 55. 发明授权
    • Method and apparatus for single crystal pulling downwardly from the
lower surface of a floating melt
    • 用于单晶从浮动熔体的下表面向下拉的方法和装置
    • US4824519A
    • 1989-04-25
    • US112499
    • 1987-10-22
    • Aleksandar G. Ostrogorsky
    • Aleksandar G. Ostrogorsky
    • C30B15/00C30B15/08C30B35/00
    • C30B15/08C30B29/40Y10S117/90Y10S117/907Y10S117/91Y10T117/1008Y10T117/1032Y10T117/106Y10T117/1068Y10T117/1072
    • An elemental or compound melt is floated on a denser encapsulent. The melt has two horizontal free surfaces (i.e., surfaces not in contact with a solid). A shaft including a seed crystal extends upwardly through the encapsulent to contact the lower free surface of the melt and then is withdrawn downwardly through the encapsulent to grow the crystal. During solidification mechanical stresses are not imposed on the crystal. The melt is heated from above so that the lower melt surface is colder than the upper melt surface which provides a strong stabilizing temperature gradient within the melt. Unsteady natural convective flows in the melt are eliminated. Steady natural convection is substantially decreased compared to the Czochralski process (CZ) and Liquid Encapsulated Czochralski process (LEC). The stoichiometric ratio in the melt is maintained by controlling the pressure of the volatile element over the upper free surface of the melt.
    • 元素或化合物熔体漂浮在更密封的密封剂上。 熔体具有两个水平的自由表面(即,与固体不接触的表面)。 包括晶种的轴向上延伸穿过密封件以接触熔体的下部自由表面,然后通过密封件向下抽出以使晶体生长。 在凝固期间,不会对晶体施加机械应力。 熔体从上方被加热,使得下部熔体表面比上部熔体表面更冷,这在熔体内提供了强烈的稳定温度梯度。 消除了熔体中不稳定的自然对流。 与Czochralski工艺(CZ)和液体封装Czochralski工艺(LEC)相比,稳定的自然对流显着降低。 通过控制挥发性元素在熔体的上自由表面上的压力来维持熔体中的化学计量比。
    • 56. 发明授权
    • Processes for the continuous preparation of single crystals
    • 连续制备单晶的方法
    • US4565600A
    • 1986-01-21
    • US492368
    • 1983-05-11
    • Jean Ricard
    • Jean Ricard
    • C30B15/08C30B15/34
    • C30B29/20C30B15/08Y10S117/91
    • Processes for the continuous preparation of single crystals having a predetermined shape and requiring little or no subsequent machining which processes comprise placing a single crystal-forming material in a crucible fitted in its lower portion with a capillary conduit having a length equal to or greater than the retention length of the molten material in the capillary at the selected temperature and pressure, heating the crystal-forming material to a temperature above its melting point, bringing a performed appropriately oriented crystal seed into contact with the pendant drop formed at the lower point of the capillary, and pulling the seed crystal away from the feed material in the crucible so that the amount of crystal-forming material fed per unit of time is at every instant substantially equal to the quantity of material pulled into single crystal form, together with novel apparatus comprising a capillary-containing crucible, heating means, feed means, enclosure, seed-supporting carrier, means for moving and rotating the carrier, and means for controlling the movement of the carrier.
    • 用于连续制备具有预定形状并且几乎不需要后续加工的单晶的方法,该方法包括将单晶形成材料放置在装配在其下部的坩埚中,毛细导管的长度等于或大于 在选择的温度和压力下熔融材料在毛细管中的保留长度,将晶体形成材料加热到高于其熔点的温度,使得所执行的适当取向的晶种与形成在 毛细管,并将晶种从坩埚中的进料中拉出,使得每单位时间供给的结晶形成材料的量基本上等于被拉入单晶形式的材料的数量,以及新颖的装置 包括含毛细管的坩埚,加热装置,进料装置,外壳,种子支撑 载体,用于移动和旋转载体的装置,以及用于控制载体的运动的装置。