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    • 94. 发明授权
    • Feedback controller in probe microscope utilizing a switch and a inverter
    • 探针显微镜中的反馈控制器利用开关和逆变器
    • US09140720B2
    • 2015-09-22
    • US13935706
    • 2013-07-05
    • Boise State University
    • Byung I. Kim
    • G01Q20/00G01Q20/02G01Q60/32G01Q60/36G01Q30/14G01Q60/38G01Q70/10B82Y35/00
    • G01Q20/02B82Y35/00G01Q30/14G01Q60/32G01Q60/36G01Q60/38G01Q70/10
    • A method of measuring properties of a sample, the method comprising: measuring a deflection of a cantilever of a COIFM; measuring a voltage at an actuator contacting the cantilever and configured to counteract the deflection of the cantilever; measuring a voltage at a scan signal source, wherein the scan signal source is communicably coupled to the piezotube and configured to move the piezotube along an X- and a Y-axis; measuring a voltage at a feedback controller, wherein the feedback controller is communicably coupled to the piezotube and configured to move the piezotube along a Z-axis; switching a switch from a first position to a second position; switching the switch to a third position; correlating at least one of the measurements to (i) a repulsive force, and (ii) an attractive force.
    • 一种测量样品性质的方法,所述方法包括:测量COIFM的悬臂的偏转; 测量与所述悬臂接触的致动器的电压并且构造成抵消所述悬臂的偏转; 测量扫描信号源处的电压,其中所述扫描信号源可通信地耦合到所述压电管并且被配置为沿X轴和Y轴移动所述压电管; 测量反馈控制器处的电压,其中所述反馈控制器可通信地耦合到所述压电管并且被配置为沿Z轴移动所述压电管; 将开关从第一位置切换到第二位置; 将开关切换到第三位置; 将至少一个测量值与(i)排斥力相关联,和(ii)吸引力。
    • 95. 发明授权
    • Scanning probe based apparatus and methods for low-force profiling of sample surfaces and detection and mapping of local mechanical and electromagnetic properties in non-resonant oscillatory mode
    • 基于扫描探针的仪器和方法,用于低强度样品表面分析,并以非共振振荡模式检测和映射局部机械和电磁特性
    • US09110092B1
    • 2015-08-18
    • US14247041
    • 2014-04-07
    • NT-MDT Development Inc.
    • Serguei MagonovSergey BelikovJohn David AlexanderCraig Gordon WallStanislav LeesmentViktor Bykov
    • G01N13/16G01B5/28G01Q10/00G01Q60/38G05D23/19
    • G05D23/19G01Q10/06G01Q60/32G05D23/1919
    • This invention relates to multi-purpose probe-based apparatus, and to methods for providing images of surface topography, and detection and quantitative mapping of local mechanical and electromagnetic properties in non-resonant oscillatory mode. These methods may include filtering of incoming probe signals. These incoming probe signals provide time deflection curves, parts of which are used for the control of scanning and collection of data that reflects sample adhesion, stiffness, elastic modulus and viscoelastic response, electric and magnetic interactions. These methods permit adaptive choice of an AFM's deflection set-point, which allows imaging at the contact repulsive force for precise surface profilometry, as non-resonant oscillation brings tip and sample into intermittent contact. These methods permit choosing a desired deformation model that allows an extraction of quantitative mechanical properties including viscoelastic response from deflection curves. These methods also permit local quantitative measurements of tip-sample current and detection of surface potential, capacitance gradients and piezoresponse in non-resonant oscillatory mode. The stable thermal environment reduces apparatus thermal drift and improves apparatus performance.
    • 本发明涉及基于多用途探针的装置,以及用于提供表面形貌图像的方法,以及非共振振荡模式中局部机械和电磁特性的检测和定量映射。 这些方法可以包括对输入探测信号的滤波。 这些传入的探头信号提供时间偏转曲线,其部分用于控制扫描和收集反映样品粘附,刚度,弹性模量和粘弹性响应,电和磁相互作用的数据。 这些方法允许自适应地选择AFM的偏转设定点,其允许以接触排斥力成像以进行精确的表面轮廓测量,因为非共振振荡使尖端和样品进入间歇接触。 这些方法允许选择所需的变形模型,其允许提取包括偏转曲线的粘弹性响应的定量机械性能。 这些方法还允许在非共振振荡模式下局部定量测量尖端样品电流和检测表面电位,电容梯度和压电应变。 稳定的热环境降低了设备的热漂移,提高了设备​​性能。